菊三七根部主要化学成分研究

目的：研究菊三七根部主要化学成分,为菊三七质量标准的制定提供理论依据与参考．方法;运用正相层析柱色谱和制备高效液相色谱对其化学成分进行分离,通过MS和NMR技术进行结构鉴定。结果：从菊三七的根部分离得到4个主要化合物,分别为千里光菲灵碱（Seneciphylline,1）、千里光宁碱（Senecionine,2）、Seneciphyllicacid（3）、Senecinicacid（4）．结论：化合物4首次从菊三七中分离得到．     

菊三七根中化合物seneciphyllicacid和senecinicacid的含量测定

目的：采用HPLC法测定菊三七根部seneciphyllicacid和senecinicacid的含量．方法：建立HPLC法测定菊三七根部seneciphyllicacid和senecinicacid的含量．色谱柱为AcclaimC18色谱柱（4．6mm×250mm,5μm）,流动相为甲醇-0．1％甲酸水（40：60,v·v-1）,流速为1．0mL·min-1,柱温为30℃,紫外检测波长为220nm．线性范围：Seneciphyllicacid为0．1～0．8mg·mL-1（相关系数r=0．9997）;senecinicacid为0．1～1．5mg·mL。（相关系数r=0．9998）．结果：测得菊三七根部seneciphyllicacid和senecinicacid的含量分别为2．9613mg·g-1、0．9542mg·g-1;RSD分别为1．34％、1．28％;平均回收率为98．84％、99．16％,RSD为1．94％、1．51％．结论：该方法快速、简便、准确度高,可为开发利用菊三七提供研究基础．     

数学思想方法在解析几何课堂教学中的应用

本文结合教学实践,举实例探讨了知识系统化思想、数形结合思想、类比思想、向量法这四种数学思想方法在解析几何课堂教学中的应用。     

X80管线钢中氮化物和碳化物析出热力学分析

基于规则熔体理论和平衡反应基础,对连铸工序X80管线钢中碳化物、氮化物析出进行热力学分析,研究Ti、Nb及Al的碳化物、氮化物析出规律。结果表明,固液两相区,TiC0.005N0.995和TiN分别在1785K和1784K时开始析出;奥氏体相区,碳化物、氮化物析出先后顺序为NbC0.64N0.36、NbC、NbN、AlN、TiC,相应析出温度为1457、1404、1354、1267、1226K;γ→α相变过程中,TiC发生相间析出,Nb主要以NbC形式析出,AlN析出量较少。     

Dynamic broadcast encryption scheme with revoking user

Currently, there still lacks an efficient methodology to revoke user’s ability to decrypt ciphertext in broadcast encryption with the uncertain number of ciphertext recipients. To solve this problem, here, we present a dynamic broadcast encryption scheme with the following properties: First, the length of the ciphertext has a linear relationship with the number of revocable users, but it has no association with the total number of ciphertext recipients. Second, the scheme also works when users dynamically join. Especially, compared with methods published up to date, our scheme is more efficient with a large number of ciphertext recipients. Third, the broadcaster can revoke user’s ability to decrypt ciphertext if necessary. Fourth, the private key of users is composed of three elements in Elliptic curve group of prime order. Last, if q-Decisional Multi-Exponent Bilinear Diffie-Hellman assumption holds, our scheme is secure in the standard model when a polynomial time adversary selectively attacks it.     

A new estimate of global soil respiration from 1970 to 2008

Soil respiration(Rs)is one of the key processes that underline our understanding of carbon cycle in terrestrial ecosystems.Great uncertainty remains in the previous global Rs estimates with a difference of 70 Pg C a 1between the highest and lowest estimates.Thus,the present study aimed to estimate the global annual Rs and investigate the interannual and spatial variability in global annual Rs using a semi-mechanistic,empirically-based model which included climatic factors(temperature and precipitation)and topsoil(0–20 cm)organic carbon storage.About 657 published studies of annual Rs from 147 measurement sites were included in this meta-analysis.The global data sets from 1970 to 2008 on climate,surface air temperature,and soil properties were collected.The Monte Carlo method was used to propagate the simulation errors to global Rs.The results indicated that the mean annual global Rs was 94.4 Pg C a 1,increasing at roughly 0.04 Pg C a 1(~0.04%a 1)from 1970 to 2008.The Rs rate increased from colder,drier and less soil carbon-rich regions to warmer,moister and more carbon-rich regions.Highest Rs rates appeared in the tropical forest,while the lowest ones were in polar and desert regions.The annual Rs correlated directly with global temperature anomalies,suggesting that the interannual variability in temperature was responsible for the interannual variations in predicted global Rs.The global Rs increased from high-latitude zones to low-latitude zones.Further studies are recommended to explore the relationship between soil respiration and vegetation characters.     

稳健正交最小二乘拟合法

针对一般的最小二乘法忽略自变量的误差这一缺点,提出一种新的正交最小二乘法.该方法以正交距离残差平方和最小为衡量准则,并通过一定的算法剔除粗差和异常值,从而获得最佳的拟合曲线.算例结果表明稳健正交最小二乘拟合法结果更为可靠.     

基于订阅划分的多维索引并行匹配算法

针对基于内容的发布/订阅系统匹配算法中的计数算法和树形算法在多操作符匹配结构中效率不高的问题,提出了一种基于订阅划分的多维索引并行匹配算法(SPMP-match).该算法利用二叉树原理对订阅进行分组,然后组织成树形索引结构,采用一种边匹配谓词边观察的策略,及时终止无成功匹配订阅的情形.该算法仅对可能和一个事件匹配成功的所有订阅进行匹配,不会产生无价值的时间消耗,并且在查找匹配成功的订阅时,只须要查看所有可能和某事件匹配成功的订阅表,避免了扫描整个订阅集合.     

云环境下基于RBAC的权限渗透问题

针对基于角色的访问控制模型在云计算跨域访问方面安全性不足的问题,在基于角色映射技术的基础上引入网络中跳数的定义,提出一种基于跳数的访问控制策略以解决在角色映射过程中所产生的权限渗透问题.从访问过程和形式化定义两方面对该策略进行了研究,并进行了仿真性能实验.与其他策略进行了比较,该策略通过在角色集和用户集中添加相应的字段来实现对跨域访问距离的细粒度控制,因此并未产生新的集合,进行跨域访问时也无须建立任何的镜像角色.实验结果表明该策略与传统跨域访问策略相比具有更高的效率以及更低的存储消耗.     

铁酸铋陶瓷的制备及其磁电性能研究

采用低温固相法制备BiFeO_3前驱体,经煅烧得到BiFeO_3粉体,并在不同温度下烧结制得BiFeO_3陶瓷。分析前驱体的热分解过程、粉体和陶瓷的物相组成及陶瓷的磁性能和介电性能。结果表明,采用低温固相法制备的BiFeO_3前驱体,经700℃煅烧可制得基本为单相的BiFeO_3粉体,再经800℃烧结可以制得体积密度较大的BiFeO_3陶瓷,其在室温下不表现宏观磁性;BiFeO_3陶瓷的介电常数和介电损耗均随其烧结温度的升高而下降。