再生丝素固体的微细结构

研究了蚕丝丝素水溶液经不同方式干燥后，所得到的再生丝素固体的微细结构，以及存放过程中丝素的结构变化，指出经30℃热风干燥或经高于－20℃冷冻干燥后，所得到的丝素固体的结构是无定形和Silk I共存，在室内温度湿度环境中存放后，部分无定形结构转化为Silk I；蚕丝丝素水溶液经－80－－20℃冷冻干燥后，所得到的丝素膜的结构主要是无定形，含少量Silk II，存放过程中部分无定形结构转化为SilkI；室温放所自然形成的丝素凝胶中，丝素的结构是无定形和Silk Ⅱ共存；丝素水溶液表面膜中甘氨酸和丙氨酸的含量较高，表面膜的结构主要是Silk I和Tilk Ⅱ结晶度高。     

河成石灰华成因──掺气效应研究

本文通过对有大量碳酸钙沉积河段的水质分析、野外观测，发现河水流动过程中将空气带入水中形成大量气泡，引起水体物化方面的迅速变化，包括碳酸钙大量沉积，笔者称之为掺气效应。通过野外实验，对掺气效应及掺气效应中水体物化变化和碳酸钙沉积速度进行了论证和研究，在此基础上提出：掺气效应是河流中碳酸钙大量集中沉积的一个主要因素。     

TV跟踪系统光电轴一致性研究

本文论述复合制导系统 ＴＶ光电设备光电轴一致性问题，并给出新的处理方法。研究结果表明：本方法具有较高的精度与应用价值。     

高应变率扭转SHB实验技术

介绍自制分离式霍布金生扭杆试验设备；详细推导出按扭转ＳＨＢ方法测量材料的动态剪应力和剪应变关系的基本方程；对软铝进行高应变率试验得到动态剪应力和剪应变关系曲线。     

固沙植物白沙蒿化学成份的研究[Ⅰ]

从固沙植物白沙蒿中分到五个成份,经鉴定:1.亚(麻)油酸乙酯Ethyl linoleate。2.樱草素Sakuranetin,3.异樱草素Isosakuranetin,4.木波罗双氢黄酮Arto-carpanone,5、金合欢素Acacetin。亚(麻)油酸乙酯是冠心病类药物的主要成份,所以白沙蒿的发现为此类药物提供了新药源。     

适用于一般提法的埃尔米特插值多项式的差商构造公式

利用差商的非构造性定义建立了适用于一般提法的埃尔米特(Henmite)插值多项式的差商构造公式,并给出了插值余项估计。     

THE TRANSFER BEHAVIOUR OF SOME CATIONS AT WATER／NITROBENZENE INTERFACE BY SEMIDIFFERENTIAL CYCLIC VOLTAMMETRY

The transfer of Sr~(2+) and Ba~(2+) ion, facilitated by 18-Crown-6 present in the aqueous phase, and of succinylcholine ion at w/nb interface were investigated by semi-differential cyclic voltammetry. A good polarographic curve of succinylcholine ion dissolved in water was obtained in the system of 0.01 mol/l LiCl (w)——0.01 mol/l TBATPB (nb). The peak current is directly proportional to the concentration of SC~(2+) ion. It can be used for the determination of SC and the detection limit is 1.05×10~(-5) mol/l.The apparent D~w and D~(nb) have been estimated. The transfer of Sr~(2+) and of Ba~(2+) at the interface are facilitated by 18-Crown-6 present in the aqueous phase and the peak current is directly proportional to the concentration of 18-Crown-6 in water. This method can be used for the determination of the complexing agent and for the stability constant of the complex formed in the aqueous phase.All the experimental results are in keeping with the theoretical.     

偏最小二乘紫外分光光度法同时测定萘，1－甲基萘和蒽

用偏最小二乘法（ＰＬＳ）进行校正和预测，不经分离同时测定了混合体系中的萘，１－甲基萘和蒽。萘，１－甲基萘和蒽的浓度分别在０～２８ｍｇ／Ｌ，０～４０ｍｇ／Ｌ和０～４０ｍｇ／Ｌ的浓度范围服从比耳定律。对合成样品中这三种组分进行分析，结果令人满意。     

利福平菌丝体厌氧生化处理的研究

制药厂生产利福平过程中产生大量的利福平菌丝体,可严重污染环境。用厌氧消化法处理利福平菌丝体,消化温度40℃,反应器容积负荷2KgCOD/m~3·d,液料滞留期(SRT)14～20天,取得了良好的处理效果。COD去除率稳定在90％左右,BOD_5去除率达到95％以上,产气率达到0.49m~3/去除KgCOD。     

THE INFLUENCE OF SPINNING CONDITION ON STRUCTURE & PROPERTIES OF MASS-DYED SUPERFINE PP AS-SPUN FILAMENTS

The effect of colorant additive on the rheology of PP polymer melt and the influence of spinning conditions on the crystalline and orientation structure of mass-dyed as-spun PP filament are reported. The △E~~~ value for all colored chips is higher than that of blank chip to a varying degree. The crystallinity and orientation degree of dyed PP as-spun filament decrease with increasing melt temperature, decreasing spinning speed and increasing denier per filament (dpf), while the crystallinity of dyed as-spun filament increases with the content of colorant additive as a nucleation agent.