煤矿井下主排水设备的计算机辅助设计

本文阐述了煤矿井下排水设备的计算机辅助设计中选型程序的编制及绘图,介绍了程序的功能,若干技术问题的处理和绘图方法与要点.     

THE TRANSFER BEHAVIOUR OF SOME CATIONS AT WATER／NITROBENZENE INTERFACE BY SEMIDIFFERENTIAL CYCLIC VOLTAMMETRY

The transfer of Sr~(2+) and Ba~(2+) ion, facilitated by 18-Crown-6 present in the aqueous phase, and of succinylcholine ion at w/nb interface were investigated by semi-differential cyclic voltammetry. A good polarographic curve of succinylcholine ion dissolved in water was obtained in the system of 0.01 mol/l LiCl (w)——0.01 mol/l TBATPB (nb). The peak current is directly proportional to the concentration of SC~(2+) ion. It can be used for the determination of SC and the detection limit is 1.05×10~(-5) mol/l.The apparent D~w and D~(nb) have been estimated. The transfer of Sr~(2+) and of Ba~(2+) at the interface are facilitated by 18-Crown-6 present in the aqueous phase and the peak current is directly proportional to the concentration of 18-Crown-6 in water. This method can be used for the determination of the complexing agent and for the stability constant of the complex formed in the aqueous phase.All the experimental results are in keeping with the theoretical.     

杂环基二硅烷的合成与波谱表征

由2—噻吩基锂和N-吡咯格氏试剂分别与氟五甲基二硅烷反应,制得了2—噻吩基、五甲基二硅烷(Ⅰ)和N-吡咯基五甲基二硅烷(Ⅱ)。两种二硅烷都是无色液体。Ⅰ在室温下空气中是稳定的,Ⅱ在空气中逐渐转变成绿褐色。元素分析,IR,~1H MR和MS分析证实了其结构。Ⅰ和Ⅱ的最大紫外吸收峰分别为242.0nm和220.1nm。     

典型结构减速箱轴结构设计CAD

本文提出了一种轴结构设计的知识表示方法，实现了轴的结构设计，并绘制出轴的结构图     

浅析血型与体操运动员的选材

本文通过与遗传密切有关的血型来探讨体操选材,为准确选拔体操运动员,提供一些理论依据.     

三氮烯类化合物作为酸碱指示剂的研究及应用

本文报道了三氮烯类化合物作为酸碱指示剂的研究及应用.以我们新近合成的此类试剂之一——2-氯一4一硝基苯基重氮氨基偶氮苯为研究主要对象,分别讨论了有无表面活性剂存在、以及不同类型表面活性剂存在下,试剂的离解常数及变色区域.在TritonX-100存在下,其试剂的pKa=9.25±0.01,变色区域为pH8.40(黄)～10.0(紫);在CTMAB存在下,pKa=7.35士0.03,变色区域pH6.85～7.90;在混合表面活性剂TritonX-100-CTMAB存在下,pKa=8.20±0.05,变色域pH7.45～9.00(黄～紫).特别是在阳离子表面活性剂存在下,滴定终点颜色变化十分敏锐清晰,是一种优于酚酞和甲基橙的指示剂.最后并对此类试剂与表面活性剂的相互作用作了简单探讨.     

存在的尴尬与神奇的魅力--解读后殖民主义作家奈保尔

本文通过对维.苏.奈保尔成功的一生和主要作品的解读,揭示其尴尬的生存处境所形成的独特批判锋芒和对后殖民地人民深厚的关怀,以及独特的文学表达形式,展示了他不同凡响的艺术风采与魅力。     

数学课中结课艺术的研究

选择恰当的结课方式,诱发学生的学习兴趣与学习动机,激活学生的思维,提高课堂效率。     

科斯社会成本问题与政府管制的效率实现

科斯在其社会成本一文中提出经济行为具有相互性,并很好地将交易成本理论运用在经济行为中,通过交易成本为零的理想世界到交易成本为正的现实世界进行条件转换分析,提出了外在性存在的根源及解决途径主要包括自愿协商(市场)、企业、政府和法律四种;提出由市场解决不好的问题,不一定政府就解决的很好;提出应从社会净收益最大化的角度来看,关键在于避免较严重的损害的观点,即如何使损失最小化或使社会经济运行效率最大化。他的这些思想,使经济学家注意到了交易成本的各种后果,大大地提高了经济的解释力。为政府更有效地进行管制提供了理论支撑。     

SIMULTANEOUS REACTION AND LIQUID-LIQUID EXTRACTION IN THE HYDROGEN PEROXIDE PRODUCTION

The gas-liquid-liquid reactive extraction system for preparing hydrogen peroxide via anthraquinone was investigated. The oxidation reaction of hydrogenated working solution was combined with the extraction of hydrogen peroxide from working solution in a sieve plate column. The reaction of 2-ethylanthrahydroquionone with oxygen and the liquid-liquid extraction of hydrogen peroxide take place simultaneously. The oxygen was introduced with hydrogenated working solution through a nozzle in the bottom of the column, which worked as agitated air as well as oxidation reagent. The results showed the oxidation and extraction do not hamper each other, on the contrary, the presence of oxidation gas in the column can promote the transfer of hydrogen peroxide from organic phase to aqueous phase, thus the reaction efficiency and extraction efficiency increased with increasing gas superficial velocity. Furthermore, the oxidation efficiency is almost 100% and the extraction efficiency is higher than 90% in this process.