Optical homogeneity of ADP crystals from rapid growth

ADP (NH₄H₂PO₄) crystals were grown through the traditional method and rapid growth technology. The optical homogeneity of rapid grown ADP crystals was analyzed by laser interferometry and X-ray topography. Laser interferometry revealed sector boundaries at which optical homogeneity decreased dramatically. The main defects that seriously reduced the optical homogeneity of the rapid grown ADP crystal were sector boundaries, growth bands and inclusions. The concentration of Fe and Cr impurities was tested by a plasma emission spectrometer. It was found that the preferential incorporation of metallic impurities into the prismatic faces resulted in high density of growth bands and inclusions, thus reducing optical homogeneity of the prismatic sector.     

ZnO microsheet modified TiO<Subscript>2</Subscript> nanoparticle composite films for dye-sensitized solar cells

Randomly oriented ZnO microsheets were successfully self-assembled on TiO₂ nanoparticle (TN) film to act as the scattering layer via a cathodic electrodeposition process. The light scattering properties of ZnO microsheets were studied by UV-Vis spectrometer in the 400–800 nm wavelength range. It was found that ZnO microsheets exhibited excellent ability to scatter the incident light for ZnO microsheet-TiO₂ nanoparticle (ZT) composite films. The results showed that dye-sensitized solar cells (DSSCs) fabricated with ZT composite films showed higher short-circuit density (J_sc) and conversion efficiency than TN-based DSSCs, due to the light scattering properties of ZnO microsheets.     

A parallel approach to direct resolution of albuterol

A library consisting of a series of O,O′-diaryzoyl-L-(–)-tartaric acids (2) was designed and synthesized. The substituent on the aromatic ring of 2 significantly affects the diastereomeric excess and efficiency of the resolution of racemic albuterol (1). Excellent resolving reagent 2a was selected for the resolution of rac-1 via the parallel approach. However, a family of three resolving reagents failed to improve the resolution efficiency of rac-1.     

竹炭基活性炭电容去离子性能的研究

电容去离子技术可以通过施加静电场,强制离子向带有相反电荷的电极迁移,使其被电极表面产生的双电层吸附并从溶液中去除,从而达到水净化的目的.以活性炭作电极材料制备了电容去离子模拟装置,考察了该装置在通直流电的情况下的去离子性能,详细研究了处理水流速、处理水量、电极片距离与电极片对数等因素对水净化的影响及电极的反洗效果.结果表明,当流速为60mL/min,处理水量为4800mL,电极片间距为2cm,电极片对数为4对时,活性炭电极电去离子模拟装置的去离子效果最好,并表现出较好的循环利用性.对不同重金属的去除效果分别为:Pb2+Cu2+Cr3+Cd2+.此工作为活性炭型电容去离子技术提供了重要的参考价值.     

浙江瑞安红双林场种子植物区系分析

统计分析了瑞安红双林场种子植物区系组成以及属的分布区类型．该区共有种子植物124科,454属,909种（含种下分类群）．种子植物454属可归纳为14个分布区类型,其中以泛热带分布为最多,达24．6％,其次是北温带分布和东亚分布,分别达16．1％和13．3％．红双林场种子植物种类较丰富,区系起源古老,分布类型多样,地理成分复杂,在生物多样性保护中有重要地位．     

制冷陈列柜性能优化策略的应用

利用改进的双流体(MTF)模型对立式敞开型陈列柜冷风幕及其四周气体流动和传热进行数值模拟,从而确定陈列柜的漏风量.通过MTF得到的结果训练并验证针对漏风量的自适应支持向量机(ASVM)算法,建立陈列柜性能的优化函数.实验测试验证结果表明,优化后的陈列柜融霜后的凝结水质量和单位展示面积每日耗电量分别减少39.2%和19.3%,明显改善了漏风.     

BDI指数与上证综指的相关性

波罗的海干散货指数(BDI)和上海证券综合指数(上证综指)在2007—2009年的走势反映了金融危机背景下世界经济的变化趋势.选取2007—2009年BDI指数和上证综指的周均值作为实证研究的样本数据,对曲线图、散点图进行描述性分析,并进行相关性和波动趋势分析.结果显示:BDI指数与上证综指呈现正相关;上证综指一定程度上揭示了中国和世界经济的走势,确切反映了中国经济与世界航运市场的变化状况;上证综指的可借鉴性优于BDI.金融危机的爆发证明上证综指具有解释中国和世界航运市场变化的指向标的作用.     

Palaeoclimatic evolution recorded by multidicipline in sediments in gahai lake, qaidam basin since late last deglacial

Based on the analyses of Loss-on-Ignition (LOI), carbonate content and sediment characteristics, this paper reconstructs the climatic and environmental evolution of the Gahai Lake area since the late Last Deglacial Period.The results cover the late Last Deglacial Period and the Holocene.The climate was very unstable and rather arid during the late Last Deglacial Period.The Holocene can be divided into three pe-riods:the early Holocene (11360-8240 cal aB.P.), which was dry but unstable and featured rising tem-peratttres, the mid-Holocene (8240-3200 cal aB.P.), which was warm and wet and the late Holocene (since 3200 cal aBP), which was cold and dry.Results also show a warm-wet event around 1500 cal aB.P.     

定性分析和定量分析在海事风险评估中的应用

本文讨论定性分析和定量分析的定义、特点,并结合实例分析他们的优点、缺点及在海事风险评估中的实际应用.     

浅析自动气象站雷电保护

自动气象站作为一种集合了传感器、数据采集及处理、数据通信等技术的自动化电子设备,其抵御雷电兵贵损害的脆弱性是不言而喻的,因此预防雷电损害是自动气象站网可靠性设计的极其重要部分.本文从直击雷、感应雷及雷击电磁脉冲保护入手,提出了相应的解决办法,对做好自动气象站的雷击防护进行了探讨.