碱处理结合盐辅助分散液液微萃取GC-MS/MS检测即食鱼制品中7种N-亚硝胺

为提高N-亚硝胺的相关检测效率,建立了碱处理结合盐辅助分散液液微萃取(SADLLME)气相色谱-串联质谱法(GC-MS/MS)检测即食鱼制品中7种N-亚硝胺的新方法。样品经氢氧化钡溶液热处理,转移目标物至水溶液中,在辅助盐硫酸钠近饱和条件下,以二氯甲烷为萃取剂进行SADLLME,应用GC-MS/MS进行检测。方法检出限为0.10~0.19μg/kg, 定量限为0.28~0.56μg/kg;加标水平为1、5、10μg/kg时,加标回收率为79.19%~117.40%,相对标准偏差为1.06%~10.30%。结果表明:此方法灵敏、可靠,选择性好,样品前处理简单,能够满足相关食品中N-亚硝胺检测的需要。     

非线性过程求最大熵谱定阶的一个经验表述

由非线性短时间序列的模拟数据对求最大熵谱的取阶区间进行了归纳及用数学表达式吻合，从而得到一个在求最大熵谱时定阶的经验公式，并将若干重大天文事件求最大熵谱时，所使用的阶数或阶数范围与本公式估计比较，其结果基本一致。此公式尤其适用于非线性过程中，从１￣４倍周期内的短时间数据序列求最大熵谱。     

Non-gyroscope DR and adaptive information fusion algorithm used in GPS/DR device

1 .INTRODUCTIONWith the development of intelligent transport sys-tem(ITS) ,the real-ti me navigation is being givenmore and more attention. One of the key technolo-gies in vehicle navigationis to get the vehicles’po-sition continuously and accurately . Nowadays ,most of the vehicle position devices in use employGPS. However , the satellite signal is frequentlyscreened or disturbed when vehicles running amonghigh buildings , in tunnels or under viaducts ,which makes GPS receiver unable…     

基于主成分分析和支持向量机的效能评定

简述了武器系统效能评定的各种方法,并分析了其特点。建立武器系统参数效能模型,首先要挑选特征参数,提出了采有主成分分析方法选择武器的特征参数。利用支持向量机建立了武器系统参数效能模型,通过实例与神经网络法的结果进行了比较,结果表明支持向量机方法比较精确和简单。     

甲烷、二氧化碳和氧化转化制备合成气——IX.热力学平衡值计算及其与实验值对比

研究了甲烷二氧化碳和氧化转化反应的热力学特性，计算了反应平衡常数及平衡组成。采用固定床流动反应装置考察了Ｎｉ／Ａｌ２Ｏ３催化剂对甲烷、二氧化碳和氧气转化反应的催化活性。     

Application of multi-resolution analysis in sonar image denoising

Sonar images have complex background, low contrast, and deteriorative edges; these characteristics make it difficult for researchers to dispose the sonar objects. The multi-resolution analysis represents the signals in different scales efficiently, which is widely used in image processing. Wavelets are successful in disposing point discontinuities in one dimension, but not in two dimensions. The finite Ridgelet transform （FRIT） deals efficiently with the singularity in high dimension. It presents three improved denoising approaches, which are based on FRIT and used in the sonar image disposal technique. By experiment and comparison with traditional methods, these approaches not only suppress the artifacts, but also obtain good effect in edge keeping and SNR of the sonar image denoising.     

STUDY ON THE BIODEGRADATION OF CELLULOSE FIBER/BASALTIC FIBER COMPOSITE PAPERBOARD

INTRODUCTIONThe Biodegradation of cellulose fiber/basaltic fiber composite paperboard prepared by reference [1] was studied experimentally and the influence factors on the biodegradation velocity were researched. EXPERIMENTALExperimentalEquipmentThe equipment of the biodegradation experiment is shown in figure 1. The carbon dioxide gas was removed when the compressed air generated by air pump passed through the taper bottle filled with sodium hydroxide solution, and then, the air tra…     

中国人口城镇、乡村分布现状及未来趋势预测

中国人口城镇、乡村分布现状及未来趋势预测狄昂照，李正平（国家科委科技促进发展研究中心，北京１０００３６）ＴｈｅｈｉｓｔｏｒｙａｎｄｃｕｒｒｅｎｔｄｉｓｔｒｉｂｕｔｉｏｎｏｆＣｈｉｎａ’ｓｕｒｂａｎａｎｄｒｕｒａｌｐｏｐｕｌａｔｉｏｎａｎｄｔｈｅｐｒｄ...     

对200AGeV~(32)S与核乳胶相互作用产生的靶核碎片的研究

本文对200AGeV~(32)S 与核乳胶相互作用产生的靶核碎片进行鉴别.对靶核碎片多重数及角分布进行了测量。测出黑、灰粒子质子能谱。分析测出的黑粒子质子能谱,认为黑粒子主要是从激发的剩余靶核蒸发出来的,但有相当数量的黑粒子是从核内级联碰撞产生的。