稀土硝酸盐与5-溴水杨醛缩-4-氨基氨替吡林、邻菲罗林三元配合物的合成与表征

由5-溴水杨醛缩-4-氨基氨替吡林(以L表示)、邻菲罗林(以L’表示)与稀土硝酸盐合成了三种新型三元配合物,并对合成的配合物进行了元素分析、红外光谱、紫外光谱和摩尔电导分析,确定了配合物的组成为:LnL L’(NO3)3·H2O。     

环芬化合物膜修饰电极对8-氮鸟嘌呤的电催化研究

用循环伏安法在石墨碳电极上制备环芳化合物膜修饰电极 ,研究该修饰电极的性质及电催化性能。该电极在pH <9的PBS溶液中能稳定存在 ,膜的循环伏安图上有两对氧化还原峰 ,峰电位随pH值的增大而负移。在pH =7.9的PBS中 ,氧化峰电流与扫速平方根υ1/ 2 在 10 0～ 5 0 0mV·S-1范围内成正比 ,表明电荷在膜中的传递受扩散影响。在pH =7.9的弱碱性溶液中该修饰电极对 8-氮鸟嘌呤有明显的电催化作用 ,且有一质子和一电子参与反应。在 1.0× 10 -4～1.0× 10 -2 mol·L-1范围内峰电流与 8-氮鸟嘌呤浓度呈线性关系。     

新型桌面吸气罩的研究与设计

文章针对目前化学实验室广范使用的喇叭型桌面吸气罩和半圆柱型桌面吸气罩存在的缺点,对桌面吸气罩进行分析研究,设计出一种性能优良的新型桌面吸气罩,因其有良好的技术经济性,值得推广。     

基于PRO/ENGINEER的WFCAD系统菜单的开发

运用Pro Engineer软件开发了WFCAD(WeldingFixturesandJigsComputerAidedDesign)系统的菜单 ,以第一、二类杠杆 铰链焊接工装夹具为设计对象 ,就如何采用Pro Engineer的用户化工具包Pro Toolkit的开发步骤和使用方法进行了介绍 ,实现了第一、二类杠杆 铰链焊接工装夹具的计算机辅助设计 .     

C－isotope composition and significance of the Sinian on the Tarim plate

102 samples of limestones,mudrocks shales and tillites from the Sinian in Kuluketage have been analyzed ,Four formations in the Sinian belong to glacial deposits in which the differences in δ^13C are distinct (-14.7‰- 4.2‰),Distinctly negative δ^13C excursions for three times support the viwe of three glacial deposits in this area suggested by previous authors,except for the durations of them ,δ^13C values are generally positive in the Beiyixi Formation of lower part of the Lower Sinian ,representing probably the rock records of a continental rift related to break-up of the Rodinian supercontinent,There are three times of distinct excursions of δ^13C curve in all strata,The first one is from positive values at the bottom to about -5‰ at the top of the Beiyixi Formation ,The second one,from 0‰-3‰ in the Arletonggou Formation of upper part of the Lower Sinian to -3.4‰---14.4‰ in the Teruiaiken Formation.The third one,from positive values in the Zhamoketi Formation of lower part of the Upper Sinian to negative values in glacial varves at the top of the Hankeerqiaoke Formation.     

Inhibitory effect of the adenovirus type 5 E1A protein expressed in the yeast system

The human adenovirus type 5 E1A, a tumor- suppressor gene[1], codes for two major related proteins of 243 amino acids (12S) and 289 amino acids (13S) by al-ternative splicing in two exons[2]. Studies have been shown that E1A can regulate expression of many genes and cell cycle[3]. Both in vitro and in vivo experiments indicated that E1A could induce tumor cells differentia-tion, convert tumor cells into an epithelial phenotype, in-hibit tumor cell growth and metastasis and strongly en-ha…     

Therapeutical effect of Shengmaisan is determined by the interaction among the three herbs

Shengmaisan is a recipe of traditional Chinese medicine, which is composed of three herbs. The interaction among the components from the three herbs of Shengmaisan is investigated using FT-IR, Matrix Assistant Laser Desorption/Ionization Time of flight mass spectrometry (MALDI TOF MS) and TEM observation. Interactions among various components from different herbs cause enhancement of the solubility of some component and suppression of the solubility of others. Results from MALDI-TOF MS show that some components found in the decoction from a single herb disappear when different herbs are decocted together. On the other hand, new substances are produced when two and/or three herbs of Shengmaisan are decocted together. TEM showed that vacuoles formed in the decoction from two and/or three herbs of Shengmaisan but did not occur in any decoction from a single herb. This result provides us direct evidence that the solubilized structure is formed by the interaction among the components from different herbs. This knowledge helps us to understand the therapeutical effects of traditional Chinese medicine.     

在系统可编程模拟器件在智能雷预处理电路中的应用

在系统可编程模拟器件是近期出现的新型可编程模拟器件，它的问世将在系统可编程技术的应用由数字电路领域拓展至模拟电路领域。介绍了在系统可编程模拟器件的结构特点和工作原理，并利用isp—PAC10设计出智能雷探测系统的预处理电路。仿真结果表明，采用ispPAC10设计的预处理电路频率特性比较理想，系统的稳定性与可靠性高。ispPAC还可反复编程，电路修改方便。     

模糊综合评价法在企业R＆D能力评价中的应用

依据影响企业R＆D能力的诸多不确定因素，运用模糊综合评价法从整体上评价各个影响因素，综合评价企业R＆D能力。