Influence of acid leaching and calcination on iron removal of coal kaolin

Calcination and acid leaching of coal kaolin were studied to determine an effective and economical preparation method of calcined kaolin. Thermogravimetric-differential thermal analysis (TG-DTA) and X-ray diffraction (XRD) demonstrated that 900℃ was the suitable temperature for the calcination. Leaching tests showed that hydrochloric acid was more effective for iron dissolution from raw coal kaolin (RCK), whereas oxalic acid was more effective on iron dissolution from calcined coal kaolin (CCK). The iron dissolution from CCK was 28.78wt%, which is far less effective than the 54.86wt% of RCK under their respective optimal conditions. Through analysis by using M?ssbauer spectroscopy, it is detected that nearly all of the structural ferrous ions in RCK were removed by hydrochloric acid. However, iron sites in CCK changed slightly by oxalic acid leaching because nearly all ferrous ions were transformed into ferric species after firing at 900℃. It can be concluded that it is difficult to remove the structural ferric ions and ferric oxides evolved from the structural ferrous ions. Thus, iron removal by acids should be conducted prior to calcination.     

一种掺铒离子化合物的上转换发光的研究

合成了一种新型掺Er 离子化合物的上转换发光材料,测量了此材料在短波段的上转换发光光谱和激发光谱,初步研究了它们在短波段的上转换发光过程:短波段的上转换发光分别为三光子或四光子过程.还比较了掺杂敏化剂和不掺敏化剂两种情况下的上转换发光的变化情况     

Simulation of wind gust structure in the atmospheric boundary layer with Lattice Boltzmann Method

Cold fronts occur in northern East Asia during winter and spring.After cold frontal passage,airflow is downward and accompa-nying strong winds fluctuate significantly;this is termed wind gusts.Analysis of observation data shows that wind gust structure has coherent characteristics.This is important for entrainment of spring dust storms into the upper boundary layer,where they are transported great distances.The Lattice Boltzmann Method(LBM) is a computational fluid technique based on the Boltzmann transport equation.The LBM has been used to study complex motion such as turbulence,because it describes motion at the micro level.In this paper,Large eddy simulation is introduced in the LBM,enabling simulation of turbulent flow in the atmospheric boundary layer.The formation and development of wind gusts are simulated,and a coherent structure with a combination of wave and vortex is obtained.This explains the mechanism of soil erosion and sand entrainment by the coherent structure of wind gusts.     

利福定对果蝇寿命的影响

本文研究利福定喂饲果蝇对其寿命的影响。试验组液体饲料分别含利福定10、5和2.5ppm,结果发现这三个浓度的利福定对果蝇均有延寿效应,其中,10ppm的利福定对雄果蝇的延寿效果最好,平均寿命延长22.4％(p<0.05),5ppm的利福定对雌果蝇的延寿效果最好,平均寿命延长19.2％(p<0.05)。而且,它们的最高寿命也有显著延长,提示利福定是一种较好的抗衰老药物。     

考虑固结路径影响的天然沉积土不排水剪切试验研究

针对传统等向固结剪切试验不能反映实际工程中的非等向变形和强度特性的局限,采用GDS应力路径三轴试验仪,对天然沉积结构性软黏土进行了不同固结条件下的不排水剪切试验,探讨不同应力路径对天然沉积土不排水剪切特性的影响.结果表明:相同的平均有效固结应力下土体偏压固结后剪切阶段应力-应变关系曲线的峰值强度大于等向固结的峰值强度;固结过程偏应力的存在提高了土体的总应力强度指标,当控制固结压力终值的剪应力相同时,偏压固结的强度包线相对于等向固结将平行上移;等向固结下当固结压力大于结构屈服压力时,有效应力路径与屈服面具有相似性,剪切屈服破坏后有效应力路径沿着临界状态线下滑;偏应力固结后剪切过程中有效应力路径的走向相对于等向固结发生了向右偏转.     

高压除鳞喷嘴内部流场数值模拟与仿真分析

针对目前工厂广泛使用的高压除鳞喷嘴,应用前处理软件Gambit建立其内部流畅的三维模型,采用Fluent软件提供的Laminar层流模型对不同结构参数的喷嘴内部不可压缩、稳态、层流流场进行了数值模拟,并分析了各参数对其流场速度分布、压力分布和出口轴心速度的影响.仿真值与理论计算值十分接近,数值模拟结果表明,喷嘴收缩角和直径对其内部流场影响较大,而扩张角对其内部流场影响相对较小,但各参数都存在最优值,且各参数之间也存在着最优搭配使射流打击效果最好.     

复合电流滤序器的谐波特性及其对相差高频保护的影响

谐波对电力系统继电保护的影响是电力部门十分关注的问题.本文就稳态谐波对复合电流滤序器和相差高频保护的影响作了计算与分析,并指出谐波对于相差高频保护影响的严重性.文中的计算、分析和结论可供电力系统继电保护工作者在设计、研究和运行分析时参考.     

Wigner-Ville distribution and cross Wigner-Ville distribution of noisy signals

The Wigner-Ville distribution （WVD） and the cross Wigner-Ville distribution （XWVD） have been shown to be efficient in the estimation of instantaneous frequency （IF）. But the statistical result of the IF estimation from XWVD peak is much better than using WVD peak. The reason is given from a statistical point of view. Theoretical studies show that XWVD of the analyzed signal can be estimated from XWVD of the noise-contaminated signal. The estimation is unbiased, and the variance is equal to that of noise. In this case, WVD cannot be estimated from W-VD of the noise-contaminated signal. Therefore, higher SNR is required when WVD is used to analyze signals.     

多群体优良模式自学习遗传算法

针对经典遗传算法存在的问题,提出了多群体优良模式自学习遗传算法.引入了迁移与学习算子,以提高遗传算法的有效性与收敛性.通过对Goldstein和Price函数的优化计算,说明了该方法具有良好的全局搜索能力和较快的收敛速度.     

特大规模组合电路测试数据产生方法研究

针对特大规模组合电路和全扫描设计电路提出了一种高速测试生成方法。该方法采用有限回溯测试模式产生方法生成测试码,采用ｎ（机器字长）个测试码并行的单故障传播方法模拟验证测试覆盖。测试生成与故障模拟为ｎ对１紧耦合集成方式。该方法运行１０个Ｂｅｎｃｈｍａｒｋ电路,取得了低测试长度、高故障覆盖、高效率的良好效果。