江西皿蛛科蜘蛛区系结构研究

列出了江西皿蛛科18种蜘蛛名录、地理分布,分析了物种结构和生态类群的特点,并就国内分布已基本查清的17种蜘蛛,根据中国动物地理区划,将其作出归纳,得知江西17种皿蛛科蜘蛛属华中区,与西南区共有种最多,与青藏区共有种最少;与邻省比较,与浙江共有种最多,而与广东、福建共有种最少。     

同位素内标法对水产品中硝基呋喃代谢物液相色谱-串联质谱法测定

建立了水产品中硝基呋喃类代谢物残留量的同位素内标定量液相色谱-串联质谱法测定。样品经稀盐酸水解,邻硝基苯甲醛衍生,乙酸乙酯提取净化后,用液相色谱-串联质谱法通过正离子扫描多反应监测模式检测,稳定同位素内标定量。本方法的线性范围为1.25～10μg/kg,4种硝基呋喃代谢物的线性相关系数均在0.993 2以上,4种化合物...     

独立学院大学生创业观的塑造

针对独立学院创业教育的现状、优势和存在的问题,提出在大学生创业观上必须正确处理好自身条件与社会需求、个人就业观与家庭期望、学校创业教育与个人专业学习三大关系。     

Eu（bpy）2（NO3）3（H2O）2/Nafion修饰于金电极上的电化学发光性质研究（英文）

本文合成了铕-联吡啶的二元配合物Eu(bpy)2(NO3)3(H2O)2,用元素分析、红外及紫外光谱对配合物进行了表征.采用循环伏安法,研究了用Nafion将Eu(bpy)2(NO3)3(H2O)2修饰于金电极上的电化学发光行为.讨论了介质、pH对该体系电化学发光性质的影响,推测了Eu(bpy)2(NO3)3(H2O)2电化学发光的机理.结果表明:在没有共反应试剂存在的条件下,Eu(bpy)2(NO3)3(H2O)2在pH 8.0的硼砂缓冲溶液中可以产生较强的电化学发光,其发光体可能为Eu*(bpy)2(NO3)3(H2O)2.     

金属有机骨架材料上气体吸附存储与分离的研究进展

对金属有机骨架(MOFs)材料的结构及合成方法做了简要概述;结合国内外研究现状详细介绍了MOFs材料在吸附存储与分离领域的研究进展,并对MOFs材料在该领域的应用进行了展望.     

Photonic integrated technology for multi-wavelength laser emission

We summarized the design, fabrication challenges and important technologies for multi-wavelength laser transmitting photonic integration. Technologies discussed include multi-wavelength laser arrays, monolithic integration and modularizing coupling and packaging. Fabrication technique requirements have significantly declined with the rise of reconstruction-equivalent-chirp and second nanoimprint mask technologies. The monolithic integration problem between active and passive waveguides can be overcome with Butt-joint and InP array waveguide grating technologies. The dynamic characteristics of multi-factors will be simultaneously measured with multi-port analyzing modules. The performance of photonic integration chips is significantly improved with the autoecious factors compensation packaging technique.     

Evaluating the reliability of microsatellite genotyping from low-quality DNA templates with a polynomial distribution model

Molecular studies using trace DNA, such as from museum specimens, ancient or forensic samples and samples obtained noninvasively, often have a common problem of low quality of DNA templates. Amplification errors, such as allelic dropout and false allele, may arise during polymerase chain reaction (PCR) using such samples. A mathematical model which treats homozygotes and heterozygotes discriminately has been developed to measure sample quality and compute the confidence level of using multipletube approaches. We use plucked hair samples collected from 26 individual Sichuan snub-nosed monkeys (Rhinopithecus roxel- lana) to test the model. In this case, a confidence level of 99% can be achieved by three positive PCRs. If the sample quality is very poor and requires many PCR replicates, an alternative multiplestep genotyping method is recommended. This model enables researchers to optimize experimental protocols through pilot studies and obtain reliable genetic information using noninvasive sampling method.     

Aero-optical wavefront measurement technique based on BOS and its applications

A collimated light beam will be refracted if it propagates through a flow-field with index-of-refraction variations,and its wavefront will be distorted.If we measure the deflection angle of the light beam,the gradient of the wavefront can be obtained using the Malus law,and the wavefront aberration can be computed with a reconstruction algorithm.Two characteristics of background oriented schlieren(BOS) are conducive to wavefront aberration measurement:BOS can be used to measure the deflection angle of a light beam by measuring the displacement field between the reference image and the experiment image.Moreover,in a BOS system of Schlieren mode,only the ray perpendicular to the background image can be captured with a camera.This is helpful to measure wavefront aberrations that occur after a planar wavefront has passed through the flow-field.Based on these characteristics of BOS of Schlieren mode,a new wavefront measurement technique,which is called the BOS-based wavefront technique(BOS-WT),is proposed in this paper.It works by constructing the relationship between the displacement of the background image and the aero-optical wavefront gradient and uses the Southwell wavefront reconstruction algorithm.A BOS-WT system was assembled,and its temporal resolution was found to be 6 ns,and its temporal-correlation resolution reached 0.2 μs.A BOS-WT can measure the time-correlation transient wavefront quantitatively.It is simple and easy to operate.In this paper,we also present a study of the aero-optical performance of supersonic mixing layer based on our BOS-WT transient wavefronts at an interval of 5 μs.The results showed the wavefront was transient and distorted after it had passed through the mixing layer.Through the analysis of the data at the 5 μs interval,the temporal evolution of wavefront can be obtained.     

Improved acetone sensing properties of flat sensors based on Co-SnO2 composite nanofibers

Co-SnO2 composite nanofibers were synthesized by an electrospinning method and characterized by X-ray diffraction, field emission scanning electron microscopy, and transmission electron microscopy. Gas sensors were fabricated by spinning these nanofibers onto flat ceramic substrates, which had signal electrodes and heaters on their top and bottom surfaces, respectively. Compared with sensors loaded with pure SnO2 nanofibers, the Co-SnO2 nanofiber sensors exhibited improved acetone sensing properties with high selectivity and rapid response and recovery times. The response was 33 when the sensors were exposed to 100 μL/L acetone at 330°C, and the corresponding response with 100 μL/L of ethanol was only 6. The response and recovery times to acetone were about 5 and 8 s, respectively. These results indicate Co-SnO2 composite nanofibers are good candidates for fabrication of high performance acetone sensors for practical application.     

Carbon and hydrogen isotopic compositions and their evolutions of gases generated by herbaceous swamp peat at different thermal maturity stages

Coalbed methane (CBM) accumulation models include continuous gas accumulation and staged gas accumulation.However,studied on the geochemical characteristics and indices to evaluate staged accumulation CBM are lacking.This study for the first time obtained the carbon and hydrogen isotopic compositions of methane and ethane generated at different evolution stages using thermal simulation of samples prepared by treating an herbaceous swamp peat at different temperatures.The results showed that the carbon isotopic compositions of methane and ethane were obviously affected by the thermal evolution level of the starting sample,while the hydrogen isotopic compositions were closely related to the maturity of gases.The carbon and hydrogen isotopic compositions of gases generated by coal-forming organic matter with Ro values from 1.2%,1.7%,2.4%,3.2% and 3.7% to 5.2% were determinated.The relationship between Ro values and the carbon and hydrogen isotopic compositions of gases generated by coal-forming organic matter at different evolution stages as well as the carbon or hydrogen isotopic relationships between methane and ethane were established.The results provide a scientific basis for studying the genesis of CBM generated at different maturity intervals and understanding the geochemical characteristics of staged accumulation CBM.These results were applied to a case study on CBM from the southern Qinshui basin,and it was found that the CBM accumulated after the Middle Jurassic and was characteristic of staged gas accumulation.This is consistent with the result of geological studies,and further showed that the results of thermal simulation experiments are very important for evaluating the genesis of natural CBM.