反应精馏过程设计研究

介绍连续反应精馏过程设计的两种研究方法：静态分析法和有限元正交搭配OEFE法，静态分析法是对反应精馏图进行热力学和拓扑学分析，鉴定反应精馏过程的基本可能性，此方法不需要依靠确定的对象的特性，要求最少最反应混合物的物理化学特性，有限元正交配技术应用了把整级评估模型转变成连续的模型。OCFE能精确地吻俣逐板模型的优化设计，而只是使用一套较小的模型公式和避免使用与塔级数有关的总决策变量，用静态分析寻找一个最大转化率稳定态，用OCFE确定反应精馏塔的级数（塔级数）及进行精级（塔板）位置。     

基于人工标引的中文学术期刊文献自动分类算法

为了解决期刊电子化的自动分类问题 ,提出了一种基于中文学术期刊人工标引的自动分类算法。这种算法主要利用自动分词得到各文献的特征词向量空间 ,并考虑到人工标引在分类中的关键作用 ,得到综合了特征词 TF和 IDF权重的分类准则。通过适当训练建立分类库 ,计算待分类样本与已知分类的相似性 ,判别各分类。实验表明 :该分类算法可以获得 85 %的分类识别率     

茴香醛席夫碱衍生物的极谱波行为及分析应用

研究茴香醛的极谱波行为并建立了测定微量茴香醛的示波极谱分析方法。在硫酸介质中 ,对氨基苯磺酸与茴香醛反应生成席夫碱 ,该席夫碱在示波极谱仪上于 - 1.0 7V(vs.SCE)产生一个灵敏极谱波 ,用于间接测定茴香醛 ,其浓度在 2× 10 - 6 ～ 1.5× 10 - 4mol/ L范围内与导数波高呈线性关系。极谱波性质被证明为吸附波。该法具有灵敏、快速简便、结果准确等特点 ,用于食品中微量茴香醛的测定 ,结果满意     

中间照明水平下视锐度的亮度响应特性研究

在中间照明水平下测量人眼的视锐度与亮度和对比度的变化关系，分析在明视觉下所建立的阿吉恩视锐度模型（Adrian‘s Visual Acuity Model)在中间视觉下的适应程度，建立中间视觉下的视锐度模型，并分析其在夜间交通照明的应用。     

一种新型的计算机温度检测系统

论述了一种新型的两级总线型电子冷藏箱生产线系统 ,介绍了该系统的技术性能和特点 ,指出了其应用推广的价值     

异步电动机的无功就地动态补偿

详细论述了运用数字电子技术对异步电动机无功就地动态补偿的理论依据和实施步骤。异步电动机的功率因数随负载的变动而变化 ,欲使异步电动机功率因数保持0 .95,需要及时投切补偿电容器。无功补偿电容量与不同负载时定子相电流与相电压的相位差角有一一对应的关系 ,只要测得不同负载时定子相电流与相电压的相位差角 ,就可以确定相应的无功补偿电容量的大小。采用七位加法计数器测得线电压和线电流过零值点的时间差 ,由此就可以确定相电流与相电压的相位差角 ,从而及时投切相应的补偿电容。     

The reaction of acenaphthene with nitrobenzene

The reaction of acenaphthene with nitrobenzene was investigated in the presence of AlCl₃. The results showed that the reaction proceeded via carboncation-electrophilic substitution reaction and free radical substitution reaction pathway. The products of acenaphthenyl phenylamine and biacenaphthyl could be synthesized by this reaction. The influence of the amount of AlCl₃ and the temperature on the components of products were also studied in this reaction. Foundation item: Supported by the National Nature Science Foundation of China (No. 29676045) Biography: Wu Lin (1965-), male, Postdictor, research direction: PAHs catalytic conversion and its biologic toxicity.     

Construction of multivalent DNA vaccines forMycobacterium tuberculosis and its immunogenicity

The coding regions of Ag85B MPT-64, and ESAT-6 secreted proteins were cloned initially into the eukaryotic expression vector pJW4303, then transformed to E. coli Top 10 strain for plasmid DNA extraction and further analysis. Plasmids containing the right insertion were sequenced to confirm their identity. COS7 cells were transfected with a mixture containing serially diluted plasmid DNA encoding three secreted proteins and Lipofectin (Gibco). The supernatants and pellets prepared from various cell lines were run on SDS-PAGE gel and the expression of these proteins in COS7 cells were demonstrated by immunoblot using polyclonal or monoclonal antiserum of M.TBH37Rv. 21 days after first vaccination of C57BL-6 mice by all three recombinant eukaryotic expressing vectors, antibody titer for Ag85B reached 1∶3200. 21 days after second vaccination, the antibody titer reached 1∶102400. The highest antibody levels induced by multivalent vaccines after the second injection were equal to or even greater than the highest antibody levels of single DNA vaccine reported in literature after third injections. Antibody titer of MPT-64 was 1∶50 after the first injection and it reached 1∶200 after the second injection. No antigen-specific antibody against ESAT-6 was detected in sera harvested from immunized mice 21 days after both injections. Antigen-specific IFN-g level of Ag85B was 110 pg/mL while no antigen-specific IFN- g level of ESAT-6 and MPT-64 was detected even after third injections. To our knowledge, it is the first time that studies of polyvalent recombinant DNA vaccines against TB were carried out in C57BL-6 mice. Our results indicated that multiple DNA vaccines could be used to enhance protective responses against M.TB.     

Satellite SAR interferometric observations of displacements associated with urban subsidence in Suzhou, Eastern China

SAR interferometry (InSAR) has a high potential for surface displacement mapping in the range from millimeter to meter. In this paper the potential of ERS-1/2 SAR interferometry for mapping subtle land subsidence has been investigated. A time series of ERS-1/2 SAR data from February 1993 to February 2000 is collected from measurements taken in Suzhou city, Jiangsu Province, China, eight ERS-1/2 SAR images are used to create seven interferograms, and three differential interferograms are produced using the three-pass method, which clearly show the spatial extent of land subsidence. The deformation maps are validated by leveling surveys, the correlation coefficient and standard deviation between them are 0.943 and 0.1706 respectively. Based on seven benchmarks, the subsidence rates are estimated, the overall trends are in close agreement with InSAR results. The results of study show that for the mapping of land subsidence in urban environments InSAR has a strong potential due to its cost-saving, high resolution and accuracy.     

超氧化物歧化酶及其模拟研究

超氧化物歧化酶 (SOD)作为一种生物活性酶 ,在治疗由氧化应激所导致的疾病方面有着非常广阔的应用前景 .本文综述了国内外近年来有关 SOD的存在和结构、SOD活性的测定及模拟等方面的研究进展 .