低成本纳米复合材料70％ CeO2·30％ NiO的合成及其催化性能的研究

分别选用水热,浸渍,柠檬酸络合燃烧,共沉淀方法合成了多种前驱体,再经过600 ℃煅烧处理4h,成功合成出纳米复合材料70％ CeO2·30％ NiO,对这些复合材料进行系统的XRD、BET、H2-TPR、O2-TPD表征和CO催化氧化性能测试.     

碘化N-正丁基氟哌啶醇对大鼠缺氧复氧心肌细胞钠钙交换体电流的抑制作用

碘化N-正丁基氟哌啶醇(N-n-butyl haloperidol iodide,F2)为本研究室改造合成的新化合物。前期研究发现F2作为L-型钙通道拮抗剂,能剂量依赖地拮抗缺血再灌注所导致的大鼠心脏损伤。研究F2对缺氧复氧(hypoxia/reoxygenation,H/R)大鼠心肌细胞钠钙交换体电流的作用并探讨其保护机制。采用Langendorff灌流系统灌流SD大鼠心脏,标准酶解法消化分离得到单个心室肌细胞。正常台式液灌流5min,立即灌流充90%N2-10%CO2的缺氧液,建立体外心肌细胞H/R模型,采用全细胞膜片钳技术记录对照、模型以及不同浓度F2(0.1、1、10μmol/L)对心肌细胞钠钙交换体电流,观察H/R状态F2对心肌细胞钠钙交换体电流的影响。结果显示:缺氧抑制钠钙交换体电流主要是抑制外向电流;H/R引起钠钙交换体电流增大,尤其是外向电流的增大。F2呈浓度依赖地抑制钠钙交换体电流,钠钙交换体电流I-V曲线上移。以上表明:F2能抑制钠钙交换体电流,尤其是外向电流,防止H/R时心肌细胞的钙超载,保护心肌细胞。     

电阻绝缘检测中低压脉冲信号注入法的算法改进

在有源式低压脉冲信号注入法的基础上,重新推导了计算电阻值的数学模型,并设计了一种运用该模型的有源式动力电池绝缘电阻监测系统,该系统可以有效地解决部分无源式和有源式绝缘检测法无法有效精确测量同时下降的正负端绝缘电阻与正负端单侧绝缘电阻的问题.此外,通过台架实验验证了该监测系统的有效性,在改进电动汽车动力电池监测系统方面具有一定的应用价值.     

UPLC-MS/MS法同时检测小花鬼针草中6种单体成分的含量

建立了一种应用UPLC-MS/MS同时测定小花鬼针草中6种单体成分原儿茶酸、芦丁、金丝桃苷、槲皮苷、槲皮素和山奈酚含量的方法。小花鬼针草药材粉碎后，经甲醇超声提取稀释后进样，采用负离子多反应监测（MRM）模式同时测定提取物中6种单体成分的含量，并以芍药苷为内标。色谱柱为Agilent SB C18 （50 mm × 2.1 mm, 1.8 μm），流动相为乙腈-0.1%甲酸水溶液，梯度洗脱，流速为0.4 mL/min，柱温为35 ℃。结果表明，该方法所测6种成分在相应的质量浓度范围内，峰面积与浓度线性关系良好，r＞0.999 0；平均加样回收率（n=6）为92.1% ～95.5%，相对标准偏差≤4.50%。该方法简单快捷、灵敏度高、专属性强，可同时测定小花鬼针草中6种单体成分。     

On implementing the symbolic preprocessing function over Boolean polynomial rings in Gröbner basis algorithms using linear algebra

Some techniques using linear algebra was introduced by Faugère in F4 to speed up the reduction process during Gr?bner basis computations.These techniques can also be used in fast implementations of F5 and some other signature-based Gr?bner basis algorithms.When these techniques are applied,a very important step is constructing matrices from critical pairs and existing polynomials by the Symbolic Preprocessing function(given in F4).Since multiplications of monomials and polynomials are involved in the Symbolic Preprocessing function,this step can be very costly when the number of involved polynomials/monomials is huge.In this paper,multiplications of monomials and polynomials for a Boolean polynomial ring are investigated and a specific method of implementing the Symbolic Preprocessing function over Boolean polynomial rings is reported.Many examples have been tested by using this method,and the experimental data shows that the new method is very efficient.     

Facile synthesis of flake-like dihydrate zinc oxalate particles

Monodispersed dihydrated zinc oxalate(ZnC_2O_4·2H_2O) particles with characteristic morphology were synthesized by aging a mixed solution of zinc nitrate(Zn(NO_3)_2) and sodium oxalate(Na_2C_2O_4) in the presence of a citrate ligand, with an average flat size of approximately 10–15 μm. The important parameters, including the solution pH values and the concentration of the zinc ions and citrate ligand, were investigated using a series of experiments. It is verified that the citrate ligand significantly affects the morphology of zinc oxalate particles, probably via its multiple roles of chelating, dispersing, and selective absorption. Thermodynamic equilibrium of the distribution of zinc species in an aqueous solution of Zn(Ⅱ)-citrate-oxalate-H_2O was estimated to explain the experimental results and to clarify the size and morphological evolution mechanism of the precipitated particles.     

Secure Two-Party Distance Computation Protocol Based on Privacy Homomorphism and Scalar Product in Wireless Sensor Networks

Numerous privacy-preserving issues have emerged along with the fast development of the Internet of Things. In addressing privacy protection problems in Wireless Sensor Networks(WSN), secure multi-party computation is considered vital, where obtaining the Euclidian distance between two nodes with no disclosure of either side’s secrets has become the focus of location-privacy-related applications. This paper proposes a novel Privacy-Preserving Scalar Product Protocol(PPSPP) for wireless sensor networks. Based on PPSPP, we then propose a Homomorphic-Encryption-based Euclidean Distance Protocol(HEEDP) without third parties. This protocol can achieve secure distance computation between two sensor nodes. Correctness proofs of PPSPP and HEEDP are provided, followed by security validation and analysis. Performance evaluations via comparisons among similar protocols demonstrate that HEEDP is superior; it is most efficient in terms of both communication and computation on a wide range of data types, especially in wireless sensor networks.     

Underdetermined DOA estimation and blind separation of non-disjoint sources in time-frequency domain based on sparse representation method

This paper deals with the blind separation of nonstation-ary sources and direction-of-arrival （DOA） estimation in the under-determined case, when there are more sources than sensors. We assume the sources to be time-frequency （TF） disjoint to a certain extent. In particular, the number of sources presented at any TF neighborhood is strictly less than that of sensors. We can identify the real number of active sources and achieve separation in any TF neighborhood by the sparse representation method. Compared with the subspace-based algorithm under the same sparseness assumption, which suffers from the extra noise effect since it can-not estimate the true number of active sources, the proposed algorithm can estimate the number of active sources and their cor-responding TF values in any TF neighborhood simultaneously. An-other contribution of this paper is a new estimation procedure for the DOA of sources in the underdetermined case, which combines the TF sparseness of sources and the clustering technique. Sim-ulation results demonstrate the validity and high performance of the proposed algorithm in both blind source separation （BSS） and DOA estimation.     

实践转向与中国特色当代美学构建

建设中国特色当代美学几乎已成为中国当代美学界的一种共识.这种共识实际上是马克思主义的“现代实践转向”和20世纪90年代的“后现代实践转向”的共同结果.“现代实践转向”在中国奠定了以马克思主义实践观为基础的实践美学,并且,在20世纪80年,代实践美学成了中国当代美学的主导流派.随着20世纪90年代后现代主义思潮传入中国,“后现代实践转向”又打破了实践美学的唯我独尊的地位,形成了中国当代美学的多元共存的开放局面.在实践美学与后实践美学的论争中,实践美学发展到新的阶段,新实践美学依然一枝独秀,可能成为中国特色美学中的核心流派,并以“后现代实践转向”的发散性思维和多元共存的实践,建设中国特色当代美学.其中,以中国传统美学的优秀遗产为根基,以马克思主义实践观为指导,以西方美学发展为参照系,建设新实践美学,就是一个主要维度或多元共存中的主要“一元”.