落球法测定液体粘滞系数实验设备的操作技巧

通过对落球法粘滞系数测定仪的分析而获得实验误差来源，通过提高实验技巧而克服仪器的弊端，使小球沿容器中心轴线准确下落，从而提高了实验成功率。     

The RCT approach for cell coverage prediction (II): Experiment and early results

We study on the implementation flow of the radio computerized tomography (RCT) prediction method. A case in real cellular mobile radio (CMR) system together with the prediction results are also presented. As shown by the results, the RCT prediction method is marked for its convenience and rapidity, as well as its relative high precision even when the prediction procedure is highly simplified. Since it is developed according to the characteristics of wireless communication environments of our country and has concurrently merits from both statistical and deterministic prediction models, the RCT prediction method is in good agreement with engineering practices in cellular mobile communication in cities at home. Optimized by combining with other techniques, further improvement could be achieved in the stability and precision of the RCT prediction method which now serves as the core part of a software tool for commercial use in CMR system analysis and optimization. Biography: Yu Sheng-bing (1974-), male, Ph. D candidate, research interest: theory analysis and application development of radio propagation in wireless communication systems.     

西门子DCS系统在大型焦炉中的应用

介绍了西门子DCS系统软件的特征,阐述了西门子DCS系统软件PCS7在现代大型焦--7.63 m焦炉控制系统中的应用.     

烷氧基稀土钠簇合物SmNa8（O^t Bu）10（OH）的合成及催化性能初探

用定量加入NaOH的方法高产率地合成了烷氧基稀土钠簇合物SmNa8（O^t Bu）10（OH），并对其进行了X射线晶体结构鉴定．此外，将其对芳醛的Tishchenko反应的催化活性进行了初探．     

高校辅导员要注重人文关怀

高校辅导员作为高校一线学生管理人员，注重人文关怀是做好工作的有效途径．人文关怀也成为高校实施有效管理的新理念．应用好这一新理念，对高校思想政治工作的顺利开展，促进大学生健康全面的成长有着重要的作用．     

车削颤振稳定性预测软件研究与开发

针对金属加工过程中颤振预测软件实现的工程需求,设计了车削加工颤振稳定性叶瓣图实验测试软硬件系统,研究了软件实现算法中的关键问题.首先,搭建了由采集卡、加速度传感器、模态力锤组成的硬件系统,开发了具有频响函数测试和稳定性叶瓣图生成功能的系统软件.其次,设计了交互式软件采集及分析界面,研究了基于C#编程语言频响函数测试过程中多通道高速同步触发采集的实现算法,开发了具有由频域分析方法获得颤振稳定性叶瓣图功能的C#类.最后,对CJ0625车床加工系统进行稳定性预测,结果表明软件预测结果与实验结果相吻合.     

Atomic layer deposition on Pd nanocrystals for forming Pd-TiO2 interface toward enhanced CO oxidation

Pd typically exhibits relatively low catalytic activity in CO oxidation, as CO is apt to be adsorbed on Pd to poison the surface for O2 activation. In this Letter, we report that this limitation can be overcome by integrating Pd with TiO2. The TiO2 was coated on Pd nanocubes with a controllable thickness using atomic layer deposition (ALD) method. Given the different work functions of TiO2 and Pd, the electrons in TiO2 semiconductor will flow toward Pd. With the electron density increased on Pd, the adsorption of CO to Pd will be weakened while the oxygen activation can be facilitated. Meanwhile, the interface-confined sites at Pd-TiO2 may further enhance the oxygen activation. As the species adsorption and activation are strongly correlated with electron density, the performance of Pd-TiO2 in CO oxidation turns out to depend on the TiO2 thickness, which determines the number of transferred electrons, within a certain range (<1.8 nm). This work provides a new strategy for enhancing catalytic performance through tailoring charge densities in hybrid catalysts.     

河南省产业集聚发展与环境污染关系的实证研究

产业集聚发展与其所在区域内环境污染之间的影响关系一直备受关注.本文选取河南省4个经济区域内产业集聚区2005-2014的面板数据,通过VEC模型对河南省产业集聚发展与环境污染之间的影响关系以及这种影响的区域异质性进行实证分析.研究结果表明:河南省不同经济区域内的产业集聚程度与该区域产业集聚区单位产值的环境污染程度之间存在长期的稳定关系,但二者之间不具有必然的因果关系;由于区域产业集聚类型和产业发展阶段存在差异,二者之间的影响程度也存在明显的区域异质性.最后,从产业集聚健康发展和保护区域生态环境的角度提出相关建议.     

鄢陵腊梅香气成分的固相微萃取-气质联用分析

采用顶空固相微萃取(SPME)吸附采集鄢陵腊梅花的香气成分,通过气相色谱-质谱联用(GC-MS)分析鉴定,以GC-MS总离子流色谱峰的峰面积归一化定量分析鄢陵腊梅花的香气成分,鉴定出含有芳樟醇、乙酸苄酯、吲哚、苯甲醇、反乙位罗勒烯、壬醛、丁香酚、桂醇和甲琥胺等60种挥发性物质.结果表明,固相微萃取-气相色谱-质谱(SPME-GC-MS)法是一种简单、可靠、适用于鲜花香气成分分析的方法.     

Annealing-induced interfacial toughening using a molecular nanolayer

Self-assembled molecular nanolayers (MNLs) composed of short organic chains and terminated with desired functional groups are attractive for modifying surface properties for a variety of applications. For example, organosilane MNLs are used as lubricants, in nanolithography, for corrosion protection and in the crystallization of biominerals. Recent work has explored uses of MNLs at thin-film interfaces, both as active components in molecular devices, and as passive layers, inhibiting interfacial diffusion, promoting adhesion and toughening brittle nanoporous structures. The relatively low stability of MNLs on surfaces at temperatures above 350-400 degrees C (refs 12, 13), as a result of desorption or degradation, limits the use of surface MNLs in high-temperature applications. Here we harness MNLs at thin-film interfaces at temperatures higher than the MNL desorption temperature to fortify copper-dielectric interfaces relevant to wiring in micro- and nano-electronic devices. Annealing Cu/MNL/SiO2 structures at 400-700 degrees C results in interfaces that are five times tougher than pristine Cu/SiO2 structures, yielding values exceeding approximately 20 J m(-2). Previously, similarly high toughness values have only been obtained using micrometre-thick interfacial layers. Electron spectroscopy of fracture surfaces and density functional theory modelling of molecular stretching and fracture show that toughening arises from thermally activated interfacial siloxane bridging that enables the MNL to be strongly linked to both the adjacent layers at the interface, and suppresses MNL desorption. We anticipate that our findings will open up opportunities for molecular-level tailoring of a variety of interfacial properties, at processing temperatures higher than previously envisaged, for applications where microlayers are not a viable option-such as in nanodevices or in thermally resistant molecular-inorganic hybrid devices.