基于FPGA的8K点FFT的设计与实现

采用4K点复数FFT实现8K实数点FFT;数据存储单元采用双口乒乓RAM结构;采用级联结构流水线的设计方式,基4蝶形结构完成前6级的运算,双基2蝶形结构完成最后一级运算;使用块浮点溢出检测.实验结果表明,在时钟周期为8.74ns的正常状态下,采用FFT处理器实现8K实数点FFT仅需要35.799μs,达到了高速运算的目的.     

Solvent effects on photophysical properties of copper and zinc porphyrins

The photophysics of Zn（tetraphenylporphyrin,TPP）, Zn（tetra-2,4,6-trimethylphenyl porphyrin, TMP）, Zn （tetra-（o-dichlorophenyl） porphyrin, TPPCI8）, Cu（tetraphenylporphyrin,TPP）, Cu（tetra-2,4,6-trimethyl- phenyl porphyrin,TMP）, and Cu（tetra-（o-dichlorophenyl） porphyrin, TPPCIE, TPPCI8） in several solvents have been investigated on steady state and time-resolved spectroscopy. The Cu（TPPCI8 ） is normal and shows no evidence of CT transition in the visible or near UV regions in nonpolar solvent. However, Cu（TPPCI8）shows a blue shift in the absorption spectrum and intramolecular CT bands at absorption spectra in polar solvent, which shows a fluorescence maximum emission at 650 nm and 8.4 ns lifetime. The reason can be attributed to two points. Firstly, the increase of solvent polarity can enlarge outer reorganisational energy, which is favorable to reduce the activation free energy of charger-transfer transition based on Marcus theory of electron transfer. Moreover, the internal heavy-atom effect on Cu（TPPCIE） is encouraging to stabilize the 2T1 state also, which increases the possibility of population to CT band from 2T1 state. This result is in accord with an earlier estimate of a 10 ns lifetime and CT absorption at 640 nm bands for the CT state of Cu （11） octethylporphyrins. Other possible reasons arousing unusual fluorescence like H-bonding, axial ligands, molecular aggregation are excluded.     

替硝唑缓释微球的制备及高效液相法测定的含量及包封率

目的:建立替硝唑缓释微球的制备方法及微球的含量和包封率的测定方法.方法:采用乳化溶剂扩散法制备替硝唑缓释微球及高效液相色谱法测定替硝唑缓释微球的含量及包封率,色谱条件:色谱柱为迪马C18(250 mm ×4.6 mm,5μm),流动相为甲醇-乙腈-水(20∶10∶70),检测波长为317nm.结果:替硝唑浓度在99.19 μg/mL～148.78 μg/mL范围内线性关系良好,R值为0.999 8.精密度试验RSD为0.94％,回收率为100.3％.结论:该制备和测定方法可用于替硝唑缓释微球的制备及含量和包封率的测定,且方法简便、快捷,准确可靠.     

用亚硫酸氢钠提高不饱和有机烯酸的产率

对合成山梨酸,肉桂酸,2—呋喃丙烯酸的方法进行了改进:在卤仿反应发生后,酸化前用亚硫酸氢钠去除去过量的次氯酸钠,产物的产率比直接酸化分别提高了21.3%,19.74%,27%,重结晶后纯度达99.05%,99.3%,99.1%。经红外,质谱,碳氢数据分析均符合要求。     

云计算环境中基于属性的多权威访问控制方法

在云计算环境中,如何实现在不可信及动态变化的云计算环境中对加密数据的访问控制是云计算走向实际应用亟待解决的问题之一.文中提出了一种基于属性的访问控制方法,该方法将密文长度及加解密过程的计算量限制为固定值,提高了系统的计算效率,并且引入了层次化的授权结构,降低了单一权威授权的负担,提高了安全性.文中分析了方法的安全性、可扩展性和计算复杂性等性能,实验结果证明了该方法在域权威授权、用户授权及加解密等过程中的计算量上的优越性.     

Direct splitting of water under visible light irradiation with an oxide semiconductor photocatalyst.

The photocatalytic splitting of water into hydrogen and oxygen using solar energy is a potentially clean and renewable source for hydrogen fuel. The first photocatalysts suitable for water splitting, or for activating hydrogen production from carbohydrate compounds made by plants from water and carbon dioxide, were developed several decades ago. But these catalysts operate with ultraviolet light, which accounts for only 4% of the incoming solar energy and thus renders the overall process impractical. For this reason, considerable efforts have been invested in developing photocatalysts capable of using the less energetic but more abundant visible light, which accounts for about 43% of the incoming solar energy. However, systems that are sufficiently stable and efficient for practical use have not yet been realized. Here we show that doping of indium-tantalum-oxide with nickel yields a series of photocatalysts, In(1-x)Ni(x)TaO(4) (x = 0-0.2), which induces direct splitting of water into stoichiometric amounts of oxygen and hydrogen under visible light irradiation with a quantum yield of about 0.66%. Our findings suggest that the use of solar energy for photocatalytic water splitting might provide a viable source for 'clean' hydrogen fuel, once the catalytic efficiency of the semiconductor system has been improved by increasing its surface area and suitable modifications of the surface sites.     

多孔氧化铝膜的制备及其光学性质

提出了一种制备具有周期结构金属薄膜的新方法--阳极氧化法制备多孔氧化铝膜.以草酸为电解液,制备出了几种表面孔径不同的多孔氧化铝膜,并在其表面镀银制得样品.用场发射扫描电镜观察多孔氧化铝膜的表面形貌,并采用光谱仪测定了样品的透射光谱.研究发现,由于表面等离子激元波(surface plasmon polaritons, SPPs)的作用,在可见光波段观察到了透过率异常增强现象.     

基于模糊综合评价的矿井提升机系统安全性分析

针对矿井提升机的结构复杂性和地下运行环境的特殊性,采用安全系统工程理论中的人-机-环境三要素分析矿井提升机系统中存在的危险因素,建立了矿井提升机系统安全性三级评价指标体系.根据矿井提升机系统安全性模糊综合评价的基本程序,对某矿区主井提升机系统的安全性进行实例分析,评价结果表明该系统的安全程度在可接受范围内.     

一种基于粒子群算法和Hopfield网络求解TSP问题的方法

针对Hopfield网络求解TSP问题经常出现局部最优解,将粒子群算法(PSO)与Hopfield神经网络结合,提出一种基于粒子群的Hopfield神经网络方法. 实验证实这种方法能够以更大概率收敛到全局最优.     

基于Jaguar CTS的企业多层分布式应用架构

在综合分析了企业计算机应用系统的现状、多层分布式应用和Jaguar CTS技术的特点的基础上，提出了一个以Jagur CTS技术和多层分布式体系结构相结合的企业计算机应用解决方案．该方案以企业现有的网络系统为支撑，实现多层分布式计算机应用系统，给出了一个用Jaguar CTS技术构建企业多层分布式应用系统的架构．最后给出了一个多层分布式应用系统的实例．