Biomimetic fluorapatite films for conservation of historic calcareous stones

Fluorapatite protective films were prepared on marble substrates using a biomimetic method. By mimicking the mineralization mechanism of enamel, phosphorus and fluorine were introduced on the surface of the marble substrate. In the presence of a biological template, namely collagen, an integrated fluorapatite film was produced and the marble substrate was entirely covered. The prepared fluorapatite films were characterized by scanning electron microscopy (SEM), X-ray diffraction (XRD), and energy dispersive X-ray (EDX) spectroscopy. The performances of the fluorapatite films were evaluated by color changes, capillary water absorption, and acid resistance tests. The results revealed that the fluorapatite films had good compatibility with the marble substrate; the physical properties such as color and capillary water adsorption of the marble substrates were unchanged. The fluorapatite films also had good acid resistance and were stable even in heavy acid rain.     

海马MF-CA3突触习得性LTP诱导后PPF效应的变化

采用电生理学与行为学结合的方法，通过慢性微电极埋植技术及双脉冲检测技术，观察大鼠海马MF-CA3突触在明暗辨别学习过程中形成习得性长时程增强（Long-term potentiation, LTP）后双脉冲易化（Paired-pulse facilitation, PPF）效应的变化. 结果表明:Mossy fibers-CA3（MF-CA3）突触习得性LTP形成前的PPF易化率为138.36%9.25%，形成后则为114.75%8.42%，差异极显著（p 0.01），而基线对照组在长达7天的检测中，PPF易化率稳定在140%左右. 研究结果显示，MF-CA3突触的习得性LTP的表达可能与突触前递质释放的改变有关.     

超高效液相色谱—质谱法测定金属罐内壁涂层中三聚氰胺及其类似物迁移检测技术研究

本研究建立了金属罐体内层涂料中三聚氰胺、三聚氰酸、三聚氰酸一酰胺、三聚氰酸二酰胺的超高效液相色谱-电喷雾串联质谱法检测技术。通过对不同提取溶液模拟金属灌装饮料的生产流程,对其中模拟物进行测试,采用正离子扫描和负离子扫描的方式进行仪器条件研究,确定了三聚氰胺、三聚氰酸、三聚氰酸一酰胺、三聚氰酸二酰胺的监测模式和特征离子对,并进行了MRM模式定性定量分析。该方法的检出限为5.0~25μg/L;线性范围0.5~200μg/L内,相关系数均大于0.995。实验结果表明,灌装饮料使用的金属罐在特定条件下会发生三聚氰胺的迁移,存在食品安全风险,同时未检出其类似物的存在。     

Effect of KNbO3 content on the crystal structure and electrical properties of (1 − x)PbZr0.54Ti0.46O3-xKNbO3 piezoelectric ceramics

(1 ? x)PbZr_0.54Ti_0.46O₃-xKNbO₃ (0 ≤ x ≤ 25mol%) (abbreviated as PZT-xKN) piezoelectric ceramics were successfully fabricated by a traditional sintering technique at 1225°C for 30 min. The influence of KNbO₃ content on the crystal structure and electrical properties of the PZT-xKN piezoelectric ceramics was studied. Samples with 0 ≤ x ≤ 0.20 show a pure perovskite structure, indicating that all KNbO₃ diffused into the crystal lattice of PZT to form a single solid solution in this compositional range. A second Pb₃Nb₄O₁₃ phase is observed in the PZT-0.25KN sample, showing that the maximum solid solubility of KNbO₃ in PZT matrix ceramic is less than 25mol%. Compared with pure PZT piezoelectric ceramics, samples containing KNbO₃ have smaller crystal grains. PZT-0.15KN exhibits excellent piezoelectric properties with d ₃₃ = 209 pC/N.     

层面理论的核心技术概念——映射语句

映射语句将内容层面、被试层面以及反应范围层面链接起来,对研究中的观察内容进行分类,表达了研究中各种观察变量之间关系的基础假设。本文重点介绍层面理论的核心技术概念——映射语句,也对映射与分配、幂集、笛卡尔积、笛卡尔集等相关概念做了简要介绍。同时也介绍了一些优化映射语句、简化研究设计的方法与技巧。     

一致半Bp-（p，r）K不变凸多目标半无限规划的最优性条件

利用局部渐进锥K在半p-不变凸集的基础上定义了一致半Bp-（p，r）K不变凸函数，研究了涉及这些广义凸性的一类多目标半无限规划问题的最优性，并得到了若干最优性条件．     

An improved 3-D ray tracing method using linear traveltime interpolation

An approach of three-dimensional seismic ray tracing is presented, which is derived from adopting two-dimensional linear traveltime interpolation (LTI). By adjusting the forward process using the partition of grid interface, and backward step by considering more directions, the new approach is suitable for the application of three-dimensional models. The calculation results show that, with the same accuracy, the improved 3-D method is much faster than the method of traditional LTI directly applied in the three-dimensional case.     

小团体队形编排在高校健美操教学考核中的实验研究

运用实验法、文献资料法、问卷调查法等研究方法,对高校健美操"小团体队形编排"教学考核方法与传统的健美操教学考核方法进行分析比较。结果表明,"小团体队形编排"考核方法有效地活跃了课堂气氛,促进了技术动作的学习,增加了课堂练习的密度,加强了师生、生生相互间的交流,培养了学生的团队意识,有效地改变纯技术教学的现状,加强了学生创造性思维的锻炼。     

提高凝汽器胶球清洗工作可靠性浅析

文章以200 MW机组为例,介绍了近年来国内许多汽轮发电机组胶球自动清洗系统的应用情况,WF-1600循环水二次滤网和RZ16-Ⅱ胶球收球网的使用,可提高凝汽器运行的可靠性,经济效益显著,最后还指出了胶球自动清洗系统的使用注意事项及存在问题。     

新建本科院校《大学物理实验》教学实践与思考

新建本科院校物理实验条件不足和生源基础薄弱,为了提高新建本科院校《大学物理实验》教学质量,顺利实现教学培养目标,教学实践中自编讲义、重视教学过程和严格考核学生成绩是关键环节.