邻硝基氯苯催化加氢的选择性

研究了邻硝基氯苯催化加氢制备２，２＇－二氯氢化偶苯的反应，并从主催化剂、助催化剂和反应温度对选择性的影响进行了研究。在优化条件下，选择性可达９３％。     

N-氯乙酰基-5-芳氧甲基-2-噁唑烷酮类化合物的合成

目的研究N-氯乙酰基-5-芳氧甲基-2-噁唑烷酮类化合物的合成方法。方法以三乙胺为催化剂，甲苯为溶剂，在110℃反应3h制备目标产物，并对产物进行了薄层色谱、元素分析、红外、核磁的分析鉴定和表征。结果合成了7种化合物，产率大于80％。结论反应条件温和，方法简单，具有较好的应用价值。     

影响高校学生管理法制完善的若干因素分析

高校学生管理法制化是实施依法治国的重要环节。笔者认为,传统观念中的人治观念、义务本位观念、息诉观念、教育观念等影响着学生管理法制的完善;高校与学生的法律地位不明确,导致学生管理的规章制度中学生的权利、义务界定不清;高校自主权作为一种权力在行使的过程中,法律责任不明、缺乏必要的监督;高校在教育市场上的强势地位,使得学生管理的法律、法规没有得到很好的贯彻和执行。     

非线性系统参数的时域识别及优化方法

采用一种非线性迭代在时域中识别非线性系统参数,将计算方法归结为一个求最小值问题。     

溶剂萃取法提取衣康酸

研究了磷氧类萃取剂对稀水溶液中衣康酸的萃取行为,考察了溶剂配比、料酸浓度、操作温度等因素的影响。测定并关联了相平衡数据,证实萃合物为H_2Ita·(TBP)_2·H_2O。对于浓度约为40g/L的衣康酸发酵液,建议用50%TBP-ker为萃取剂,在室温(298 K)下萃取,反萃取用353 K热水。     

Structure of the dimerized hormone-binding domain of a guanylyl-cyclase-coupled receptor

The atrial natriuretic peptide (ANP) hormone is secreted by the heart in response to an increase in blood pressure. ANP exhibits several potent anti-hypertensive actions in the kidney, adrenal gland and vascular system. These actions are induced by hormone binding extracellularly to the ANP receptor, thereby activating its intracellular guanylyl cyclase domain for the production of cyclic GMP. Here we present the crystal structure of the glycosylated dimerized hormone-binding domain of the ANP receptor at 2.0-A resolution. The monomer comprises two interconnected subdomains, each encompassing a central beta-sheet flanked by alpha-helices, and exhibits the type I periplasmic binding protein fold. Dimerization is mediated by the juxtaposition of four parallel helices, arranged two by two, which brings the two protruding carboxy termini into close relative proximity. From affinity labelling and mutagenesis studies, the ANP-binding site maps to the side of the dimer crevice and extends to near the dimer interface. A conserved chloride-binding site is located in the membrane distal domain, and we found that hormone binding is chloride dependent. These studies suggest mechanisms for hormone activation and the allostery of the ANP receptor.     

浅谈高职院校思想政治教育的创新

高校思想政治教育要克服在落实教育目标过程中的不足,要拓宽教育途径,为了做好高校思想政治教育工作,作者提出了进行观念上的创新、内容上的创新、教育方法上的创新的方法.     

Determination of the optical thickness and effective particle radius of clouds from transmitted solar radiation measurements

A method is presented for determining the optical thickness (τc) and effective particle radius (re) of stratiform cloud layers from transmitted solar radiation measurements. A detailed study shows that the cloud optical thickness and effective particle radius of water clouds can be determined from transmission function measurements at 0.75 and 2.13 μm, provided that the scaled optical thickness τ′0.75>1 and re>5 μm. The wavelengths adopted by our study are similar to the channels of the moderate resolution imaging spectrometer (MODIS). The proposed method is invalid for optically thin clouds since transmission at 2.13 μm is less sensitive to re. The retrieval errors of τ′0.75 and re monotonically decrease with increasing τc. For clouds having τ′0.75≥2, the retrieval errors of τ′0.75 and re are below 10% and 20%, respectively. Transmissions at 0.75 and 1.65 μm can also be used to retrieve τc and re.     

复变函数在换元积分法中的应用

讨论了复变函数方法在换元积分法中的应用．     

复合工业助磨剂助磨性能研究

本文对复合工业助磨剂的助磨性能进行了研究 ,研究表明在粉磨过程中添加少量助磨剂到欲粉磨物料中 ,即能吸附在物料颗粒的表面上 ,通过物理化学或化学作用产生力学效能 ,从而加速粉磨过程的进行。本文还对应用工业废料开发助磨剂新品种的可行性进行了研究