红豆蔻挥发油化学成分的GC/MS法分析

用水蒸气蒸馏法从红豆蔻中提取挥发油．采用不同类型的毛细管柱进行分析，找出最佳分析条件，用归一化法测定其百分含量，并用气相色谱-质谱法对化学成分进行鉴定．鉴定得到48个成分，占挥发油总成分的84％以上．     

基于内容的Web集群系统负载均衡策略

Web集群技术解决了Web服务器系统容量问题，其核心思想是负载均衡策略和算法。传统的策略对某些站点类型有效，而不能满足各种类型站点的要求。笔者分析了各种类型站点的负载特点，讨论了负载均衡需要解决的主要问题，提出了一种基于内容的Web集群负载均衡策略和相应的负载均衡算法，并通过仿真实验验证了该策略和算法的有效性。     

Cryptomelane（KxMn8-xO16）： Natural active octahedral molecular sieve（OMS-2）

The Xiangtan manganese deposit (XTM) used to be considered a supergene oxide manganese ore in South China. We reported a new identification of the naturally outcropping cryptomelane by examining the physical, chemical and structural features of the XTM supergene oxide manganese ore. The MnO2 content was over 90%, K2O more than 3%, and water from 2.2%-3.1% which is similar to one in zeolite. The cell parameters of the cryptomelane were given as a0 = 0.9974 nm, b0 = 0.2863 nm, c0 = 0.9693 nm and β= 91.47°. There was a larger pseduotetragonal tunnel in the natural cryptomelane that was formed by [MnO6] octahedral double chains with aperture of 0.462×0.466 nm2, filled with K cations resulting in some Mn3+ substituting for Mn4+ to balance the negative charges of structure. The finding is important not only for prospecting manganese resources in South China, but also in application of octahedral molecular sieve of natural cryptomelane as that developed in the tetragonal molecular sieve of natural zeolite o     

Preparation of (R)-and (S)-2-Allyl-1,3,2-Dinaphtho(α,β)[d.f]dioxaborepin and Their Reactions with Aldehydes

0　IntroductionEnantiopure 1,1′ bi 2 naphtholspossessingC2 chiralityhaveprovedtobeversatilechiralauxiliariesinanumberofasym metricreactions[1 \|6] .Althoughsomeboroncompoundsofthemhavebeenprepared[7 1 6] ,chemistryoftheirallylboranederivativeshasneverbeenreported .Toexplorepossibilityofapplyingseven memberedcyclicchrialallylboronateesterstoasymmetricsynthesisofchiralβ alkenylalcohols,whichareimportantintermediateinthepreparationofopticallyactivenaturalproducts,werecentlyat temptedtosynthesi…     

Climatic significance of stable carbon isotope in tree rings of Abies spectabibis in southeastern Tibet

The annually cross-dated stable carbon isotope of tree-ring a-cellulose of Abies spectabibis collected from the southeastern Tibetan Plateau is used to examine its rela-tionship with climatic parameters. The residual D13C series in treerings is constructed after removing the effects of age trend and rising CO2. We found a close relationship between D13C in tree rings and the relative humidity of September—November of the previous year measured at the nearby Ny-ingchi Meteorological Station, albeit a strong 搇agged effect? Thus we developed a transfer function to reconstruct the autumn relative humidity for the Nyingchi region, which explained 37.9% of the total variance (p < 0.001). Our results suggest a high frequency and moderate amplitude variance of the relative humidity before 1800, and the variance re-versed afterwards.     

土工格栅加筋路堤的三维有限元分析

运用通用有限元程序ANSYS ,对软弱地基上路堤加筋的作用和效果进行了三维有限元分析 .计算中采用DP模型模拟土体的材料非线性 ,采用面—面接触单元考虑筋土界面的状态非线性 ,并采用薄膜单元来模拟土工格栅 .通过对相关参数的敏感性分析 ,证明了土工格栅模量对加筋效果有显著影响 ,并且加筋位置靠近路堤底部时更能发挥加筋性能 ;证明了在土体发生显著侧向变形时土工格栅能够发挥抗拉效果 ,从而限制土体侧向变形和路堤外侧土体的隆起 ,达到减小沉降和不均匀沉降的效果 .研究成果对软弱地基路堤加筋处理和新老路基结合部处理均有借鉴意义     

分层海洋中大直径桩柱的波浪力

研究了在两层流体中大直径桩柱的水动力特性。基于分离变量方法，建立了绕射势的级数解，导出了作用于大直径桩柱上的绕射力的计算公式。与单层流体不同的是，对两层流体，由于内波的存在，作用在大直径桩柱上的绕射力，除了自由表面波绕射力外，还存在内波绕射力的作用。对所建立的绕射力的求解模型进行了数值模拟，并与单层流体的情况进行了比较，得到了一些有意义的结果。     

小菜蛾捕食性天敌主要类群——蜘蛛的初步研究

捕食小菜蛾的蜘蛛有12种,主要有食虫沟瘤蛛Oedothorax insecticeps Boes.et Str.、草间小黑蛛Erigonidium graminicolam(Sundevall)、八斑球腹蛛Theridion octomaculatum Boes.et Str.、拟环纹狼蛛Lycosa pseudoannulata Boes.et Str.、三突花蛛Misumenops tricuspidatus(Fabricius)等.粽管巢蛛Clubiona japonicola Boes.et Str.对小菜蛾2-3龄幼虫的日平均捕食量最大为17.6头,其次是拟环纹狼蛛,八斑球腹蛛攻击力最低,日平均捕食量仅为2.4头.农药对蜘蛛的毒性测定结果表明,敌敌畏对三突花蛛杀伤力最大,生物农药8010毒性最低.     

基于树形模型的血管三维拓扑结构描述

针对磁共振血管成像的特点，提出了一个系统框架，将其中的血管表示为具有一定逻辑结构且保持原血管拓扑结构的特征树，先通过预处理提取出血管并进行三维细化，再递归跟踪血管骨架生成特征树并进行遍历提取出血管的分支点和端点．考虑到实际图像的复杂性，进一步引入森林来完全描述血管树．利用该系统可以进一步实现数字减影血管造影和磁共振血管成像的融合，并在此基础上实现脑血管的三维重建，对于临床血管图像的实验证明了该系统的可行性与有效性。     

基于CTI技术呼叫中心的实现

研究了如何应用CTI(Computer Telephony Integration)技术设计呼叫中心，概述了设计基于CTI技术的呼叫中心的基本问题，从系统的体系结构、硬件实现和软件实现3个方面详细描述了如何建立基于CTI技术的呼叫中心系统，这种技术方案的优点是投资较小、软件的开发和扩展比较容易，特别适合于业务量不大的小型呼叫中心。