改进的溶胶-凝胶法制备超细铜粉

对溶胶－凝胶法进行了改进，由溶胶直接制备出超细铜粉，找到了制备超细铜的Ｇ分散剂及最佳制备条件，并获得了平均粒径为１０ｎｍ的铜粉。     

On convergence for trigonometric interpolation of analytic function

In this paper, we give a necessary and sufficient condition of sequence of nodes, such that, the error of trigonometric interpolation for analytic function converges to 0. Foundation item: Supported by the Science Foundation of SEC of China and Foundation of Wuhan University Biography: LIU Hua (1971-), male, PH. D candidate, Research interest is in complex analysis.     

The tectonic uplift of the Hua Shan in the Cenozoic

Six granite samples were collected from six difference elevation locations at the Hua Shan in a main ridge of the Qinling Mountain. Apatite and zircon separated from these six samples were dated by the fission track technique. An assessment of the Cenozoic uplift or exhumation rate was obtained from the altitude difference of sampling samples dated by fission track, and from the difference of fission track dates of both apatite and zircon for a sample. The preliminary results suggest that the beginning of uplift of the Hua Shan was as early as 68.2 MaBP and the uplift rates for different periods are 0.02–0.19 mm/a (from the elevation difference) or 0.12–0.16 mm/a (from two mineral fission track dates). The average uplift rate is 0.12 mm/a (from the elevation difference) or 0.14 mm/a (from two mineral fission track dates). The uplift of the Hua Shan might accelerate since (17.8±2.0) MaBP, and the average uplift rate is about 0.19 mm/a.     

荧光光谱法研究甲基蓝与羊毛角蛋白的相互作用

在0.1 mol/L Tris-HC1弱酸和中性缓冲液中,采用荧光光谱法研究了甲基蓝(MB)与羊毛a-角蛋白相互作用.结果表明:在25℃和37℃,pH分别为5.45、6.25和7.20,MB与a-角蛋白结合形成1:1配合物,猝灭蛋白质内源荧光,敏化MB峰位在460 nm处的荧光.它们之间的结合反应是吸热、熵增驱动的自发过程,即反应过程中△H＞0和△S＞0,则其主要作用力是疏水作用.中性pH时其结合常数增大,表明中性环境蛋白质的局部构象更有利于MB的疏水结合.同时,37℃与25℃结合常数相比,37℃环境的KA大于25℃,与反应过程是吸热过程即△H＞0的结果一致.     

植物细胞核不同制备方法的比较研究

以玉米为研究材料,分别采用悬浮液法、丙烯酰胺凝胶包埋法、涂片法及酶解火焰干燥法等4种不同的方法制备细胞核,对所得到的细胞核在形态及结构等方面进行了分析和比较,根据其优缺点归纳出适用范围,为细胞核的制备提供可借鉴的依据.     

Radial Yarn Movement in Yarn Duct of Interlacer

In order to find the relations between the production performonce of interlacer and its cross-sectional Shapcs of yarn duct,radial yarnsd movement in varions yarn ducts of interlacer and its effect on performance of interlaced yarn were studied in this paper. Seven interlacers,which were diffcrent in the cross- sectional shape of yarn duct,were made. Yarn motion in yarn duct of interlace was observed with optical fibers and photo- sensors. Performance of the interlaced yarn was evaluated by the number and the strength of tangles. Experfmental results disclose the relations between the yarn motions and the properties of the interlaced yarn. The interlacer with round yarn duct is capable of producing an interlaced yarn with bigger number of tangles,since It can make yarn transverse frequently the axis of air jet issuing from air jet nozzle. The interlacer with cornered shape of yarn duct makes yarn subjected to the action of compressed air for a longer time,which results in larger strength of tangles.     

多目标规划下伪不变凸函数的性质

从广义凸性的角度,首先引入了两种新的不变凸函数,考虑了向量关键点,并且在多目标规划下,证明了每个向量关键点均是有效解这一重要性质.     

信息化环境下高校《中国古代史》教学的思考

如何进行信息化环境下高校《中国古代史》教学,可以从两个方面进行思考：首先教师素质要提高,既要有传统功力,又必须与时俱进,兼备现代信息技术的熟练使用;其次,除了要提高自身素质外,教师在教学中亦须转变教学理念,要在教学中探索和实施研究性教学,这种研究性教学应从两方面变革和突破,即教师研究性教学和学生研究性学习。     

低温氧漂活化剂的制备与应用

为解决纯棉针织物练漂温度高、能耗大等问题,制备了能用于低温漂白的锰配合物MnⅡ(L) (ClO4)2(其中L为1,4,7,10-四氮杂环十二烷),并研究了双氧水用量、配合物浓度、NaOH用量、练漂温度和练漂时间共5个工艺因素对漂白效果的影响.通过单因素试验和正交试验,得到优化的工艺条件:DM-1361用量为0.5 g/L,DM-1408用量为1 g/L,H2O2(35％)用量为8g/L,NaOH用量为6 g/L,配合物浓度为20 μmol/L,练漂温度为70℃,练漂时间为50 min,浴比为1∶10.结果表明:低温优化工艺整理后织物的白度和毛效略差于传统工艺,但达到服用要求；顶破强力与织物失重率均优于传统工艺.     

Influence of Spinning Technology on Dye Uptake of Modified Polypropylene Fiber

By adding small amount of olefin polymer additive, the dyeability of polypropylene fiber can be improved. Research results show that the improvement of dyeing performance of modified PP fiber is mainly due to the formation of looser structure of PP matrix and the micro-channels among additive particles in blended fiber. The dye uptake of drawn fibers decreases with drawing ratios obviously and changes with temperature of heat plate and heat roller a little.