阔草清除草剂在玉米及土壤中残留动态研究

采用zorbaxSIL色谱柱、以二氯甲烷-甲醇为流动相的高效液相色谱法测定了阔草清除草剂在玉米田土壤、玉米籽粒和植株上的残留动态，建立了样品前处理方法和分析方法。阔草清在土壤、玉米籽粒、植株的添加回收率分别为88.00%～96.80%,90.30%～93.50%和84.20%～94.20%,阔草清在土壤中的半衰期（t1/2)吉林为12.1d。山东为20d，山东为20d，降解速度较慢；在植株中半衰期（t1/2)吉林为4.3h,山东为5.5h，降解较快。但在收获的土壤、玉米和植株中均未检出。说明其残留污染性很小，可以在玉米田安全使用。     

电话会议系统中电话事件状态及状态转移设计

以一个电话会议汇接系统的设计开发为例，针对电话会议汇接系统的实时性、多任务的特点，运用有限状态机模型，从状态和状态转移的设计入手，结合面向对象程序语言编程，探讨此类系统的软件设计的思路和方法。     

基于TDI的网络安全存储系统研究与实现

提出了传输层网络安全存储系统的体系结构和实现方法 ,将用户管理、访问控制、数据加密和审计日志等安全措施集中到普通网络存储系统中 ,并重点对系统中基于TDI的过滤驱动程序原理和实现进行了分析 .该系统为提高目前网络存储系统的安全性提供了一种方便安全、管理集中、高效可靠的解决方案     

Cryptomelane（KxMn8-xO16）： Natural active octahedral molecular sieve（OMS-2）

The Xiangtan manganese deposit (XTM) used to be considered a supergene oxide manganese ore in South China. We reported a new identification of the naturally outcropping cryptomelane by examining the physical, chemical and structural features of the XTM supergene oxide manganese ore. The MnO2 content was over 90%, K2O more than 3%, and water from 2.2%-3.1% which is similar to one in zeolite. The cell parameters of the cryptomelane were given as a0 = 0.9974 nm, b0 = 0.2863 nm, c0 = 0.9693 nm and β= 91.47°. There was a larger pseduotetragonal tunnel in the natural cryptomelane that was formed by [MnO6] octahedral double chains with aperture of 0.462×0.466 nm2, filled with K cations resulting in some Mn3+ substituting for Mn4+ to balance the negative charges of structure. The finding is important not only for prospecting manganese resources in South China, but also in application of octahedral molecular sieve of natural cryptomelane as that developed in the tetragonal molecular sieve of natural zeolite o     

Synthesis and Characterization of Porphyrin-Trisbenzimidazole Dinucleating Ligand and Its Heterodinuclear Complex as CcO Active Site Model

A new dinucleating ligand having two metal-binding sites has been designed and synthesized as model ligand for Cytochrome c Oxidase. The corresponding heterodi-nuclear complex, as an active site model of Cytochrome c Oxidase, consisting of a porphyrinatocobalt compound covalently linked with a copper derivative of tris(2-benzimidazylmethyl) amine bearing three benzimidazole ligands for copper was synthesized and spectroscopically characterized. The spectra data suggest that there are interactions between the cobalt and copper coordination units. The cobalt is coordinated to four central nitrogens of the porphyrin and the copper has pentaco-ordinate geometry with the four tertiary amine nitrogens and a chloride.     

Shift visual cryptography scheme of two secret images

A new visual cryptography scheme of two secret images, which is named the shift visual cryptography of two secret images, is given. The compound function family of a general construction model is also introduced. The uniqueness and validity of this model are proved, and the minimum rows and columns for realizing the scheme are obtained. Compared with visual cryptography of one secret image, the shift visual cryptography scheme can share two secret images with the same size of pixels expansion without losing the contrast. It has randomness and various forms, and furthermore, we can also visually recover two secret images even if the two shares are different in form and color.     

电视胸腔镜下微创脊柱侧弯前路松解术的初期临床结果

探讨电视胸腔镜在严重脊柱侧弯前路松解中的应用价值,并对其初期临床结果进行分析.2001年11月-2002年8月,共11例严重脊柱侧弯患者接受电视胸腔镜下前路松解,均为女性,特发性胸椎脊柱侧弯,年龄14～17岁.冠状面Cobb角90°～100°,Risser征+++～++++,松解范围T5～T12,松解节段5～7.术后行牵引二周再行后路TSRH矫形内固定术.术中出血量为100～150mL,手术时间180～220min,术后引流量520～650mL,引流时间48～96h,二期后路手术矫正率平均为58%.电视胸腔镜下脊柱侧弯的前路松解在不影响矫形手术效果的同时,能减少组织损伤,降低感染可能,减轻术后疼痛,缩短病人的康复时间.     

高科技企业竞争的网络特征及其对策

本文从提高我国高科技企业持续创新能力的现实需要出发 ,在对高科技产业核心资源和市场特性分析的基础上 ,从网络效应角度具体分析了其竞争的网络特征 ,最后从培育核心能力 ,实施网络作战等方面提出了在网络竞争环境下 ,提升高科技企业竞争优势的具体对策。     

Triassic U-Pb age for zircon from granites in the Tonghua area and its response to the Dabie-Sulu ultrahigh-pressure collisional orogenesis

Single-grain zircon U-Pb dating was carried out to constrain the emplacement timing of granitic plutons at Chaxinzi, Xiaoweishahe and Longtou in the Tonghua area, south of Jilin Province. The results show that these plutons formed in the Triassic with ages of 203—217 Ma. Geological and geochemical characteristics indicate that the plutons are composed of quartz diorite and granite. The former was derived from partial melting of mafic lower crust, whereas the latter originated from thickened crust with garnet as the residue in the source. It appears that protoliths of these two types of granitits are different although they have the same emplacement age. Considering that these plutons are petrologically different from the coeval granites in the Xingmeng (Xing‘an-Mongolian) to Jihei (Jilin-Heilongjiang) orogenic belt in the north, it is suggested that their formation was related to the Dabie-Sulu ultrahigh-pressure collisional orogenesis since their ages are only 10—20 Ma younger than timing of the ultrahigh-pressure metamorphism, but comparable to that of the first rapid exhumation of the ultra-high-pressure metamorphic rocks and the emplacement of the post-collisional granites.     

无关供者骨髓移植治疗多次复发性急性白血病

文章探讨无关供者骨髓移植治疗多次复发急性白血病的疗效 .经改良 Bucy方案预处理后对一例第三次复发的急粒患者行无关供者骨髓移植 ,同时给防治 GVHD、抗感染治疗 .结果 + 2 1天骨髓在患者体内植活 ,+ 35天细胞染色体分析呈供者型 ( 4 6,XX.正常核型 ) ,+ 84天血型转换成供者型 ,至今已无病生存超过 6个月 .结果表明 ,无关供者骨髓移植对多次复发的急性白血病患者具有治疗价值