Synthesis and properties of a Pr（Ⅲ） complex with 2-acetylbenzimidazoledehyde-glycine Schiff-base ligand

Abstract The 2-acetyl-benzimidazoledehyde-glycine Schiff-base ligand and the corresponding Pr（Ⅲ） complex Pr2L3（NO3）3· 2CH3OH （L=C11H10N3O2） were synthesized in methanol and characterized by a series of methods, including chemical analysis, elemental analysis, TOF-MS, ^1H NMR, UV-, IR-, Raman spectra, thermal analysis, and the three-dimension fluorescence excitation and emission spectra. The Pr（Ⅲ） complex exhibits extraordinary water-solubility and the Pr（Ⅲ） hydroxide appears at pH≥13. The complex also possesses specific fluorescent properties. Thus, at the excitation wavelengths 200.0-280.0 and 260-350 nm the fluorescence bands were observed at 290.0 and 400.0 nm, respectively.     

Sr-Nd isotope geochemistry of eolian dust of the arid-semiarid areas in China： Implications for loess provenance and monsoon evolution

Strontium (Sr) is a divalent alkaline earth element. Its ionic radius (0.113 nm) is slightly larger than that of calcium (0.099 nm), and Sr thus substitutes isomor- phously for Ca in many minerals. Neodymium (Nd) is a rare earth element. Its chemical prop…     

Seasonal variation of snow microbial community structure in the East Rongbuk glacier, Mt. Everest

Mt. Everest, the zenith of the world, plays an impor- tant role in the global climate change. During the lastdecade, some studies on glacier and snow have been undertaken in this region. The climate and environment changes in the past hundred years have b…     

Studying the stability of the middle atmosphere (30―60 km) over Wuhan by Rayleigh lidar

The stability of the middle atmosphere ranging from 30 km to 60 km over Wuhan is elementarily studied, according to the observational data obtained in about one year through the WlPM Rayleigh lidar. The stability parameter （buoyancy frequency squared）, which was obtained through the temperature field, shows that the middle atmosphere over Wuhan is stable all the year round, but the stability appears variable because the stability of summer and winter is lower, and that of spring and autumn is higher.     

Thermal conductivity measurement of InGaAs/InGaAsP superlattice thin films

The thermal conductivities of InGaAs/ InGaAsP superlattices with different period lengths were measured from 100 to 320 K using 3ω method. In this temperature range, the thermal conductivities were found to decrease with an increase in temperature. For the period length-dependant thermal conductivity, the minimum value does exist at a certain period length, which demonstrates that at a short period length, superlattice thermal conductivity increases with a decrease in the period length. When the period is longer than a certain period length, the interface thermal resistance dominates in phonon transport. The experimental and theoretical results confirmed the previous predictions from the lattice dynamics analysis, i.e. with the increase in period length, the dominant mechanisms of phonon transport in superlattices will shift from wave mode to particle mode. This is crucial for the cutoff of the phonons and lays a sound foundation for the design of superlattice structures.     

Growth ages of ferromanganese crusts from the western and central Pacific： Comparison between nannofossil analysis and ^10Be dating

Based on results of nannofossil analysis and 10Be dating in ferromanganese crusts M1-1 and A1-1 (no nannofossils were found in it),from the western and central Pacific respectively,it is found that the crust growth ages from nannofossil biostrati-graphy agree well with those based on 10Be isotope analysis. Both crusts have three growth layers,and the oldest layer was deposited in Miocene at about 12.80 Ma. The maximum,minimum,and average growth rates of crust A1-1 (from the central Pacific) are 8.11,1.92 and 3.47 mm/Ma,and those of crust M1-1 (from the western Pacific) are 2.93,0.47,and 0.94 mm/Ma.     

强磁性纳米材料CoFe2O4磁稀释体系磁化强度的表征

建立了一个表征强磁性纳米材料磁稀释体系磁化强度的新方法，该方法不同于传统的Gouy法．采用永久磁矩和未偶电子为零的无磁性物质为磁稀释体系，将纳米材料的强磁性稀释后，用Gouy磁天平表征了不同粒径系列的强磁性纳米材料CoFe2O4的磁化强度，探讨了纳米材料粒径与磁稀释体系磁化强度的关系．结果表明，谊方法具有样品用量少、数据准确、重现性好的优点．     

多双曲复数中广义正则函数的Riemann-Hilbert边值问题

研究一类双曲复变函数的超定双曲型方程组的解（即多双曲复数的广义双曲正则函数），讨论它在一类柱形域上的Riemann—Hilbert边值问题，得到了其解的存在性和解的积分表达式．     

英语专业精读教师话语分析

教师话语是大学英语课堂的重要交际媒介,它既是目的语的来源,也是管理课堂的手段。教师话语成功运用与否,直接关系到教学效果的好坏。本文通过对精读英语教师话语类型、特征和功能的描写,对英语精读教师话语和课堂互动活动进行分析和评价的基础上,得出结论:教师应转变传统角色,应更关注教师话语的质量而不是数量,课堂上应以提高学习者的语言水平和培养学习者意义协商的能力为主,以便学习者从外部环境获取更多的优化语言输入。     

"化"缀词的语法和语义研究

“化”缀词中“X”的语法单位是语素、语素组或准词组,其语法性质可以是名词性成分、动词性成分、形容词性成分、区别词性成分、数量词性成分甚至副词性成分等。通过实例考察,“化”缀词的基本语法功能是动词,但不排除为形容词甚至是区别词,而其整体意义与词根“X”的联系也有很强的规律性。