胸腺嘧啶分子振动光谱及其量子化学计算

分别检测了胸腺嘧啶粉末的拉曼光谱和红外光谱,并用量子化学B3LYP/6-311**G(含电子相关效应的杂化密度泛函理论DFT)方法,对胸腺嘧啶分子进行了几何结构优化,理论计算了胸腺嘧啶分子的拉曼散射光谱和红外光谱,并将计算结果与实验值进行比较.结果表明:采用DFT方法的计算结果能够和实验值很好的吻合.通过Gauss View可视化软件,对胸腺嘧啶分子的振动频率进行了全面的归属.     

Combinational electroporation and transplantation approach to studying gene functions in avian embryos

Gene transfection is an indispensable approach for studying gene function since it provides important information on gain- and/or loss-of-function. Chick embryos are also extensively employed for studying bio- logical function since they are easily accessible and can be maintained alive after manipulation. The combination of both techniques presents a powerful approach to under- standing how genes regulate embryo development. Fur- thermore, combining these approaches with tissue transplant techniques make even more attractive for elu- cidate gene function. Electroporation, employing parallelly fashioned electrodes, has been widely used in chick embryos. However, experimenters have been frustrated by unsuccessfully transfection in some embryonic tissue of interest because the electrodes were improperly positioned.We presently demonstrated the different patterns of orga- nizing and positioning the electrodes, in combination with tissue transplantation, to efficiently and specifically trans- fect the chick embryonic head, trunk neural tube, heart tube, somites and neural crest cells with the GFP reporter gene.     

双氧水氧化废轮胎胶粉在改性沥青中的应用

采用双氧水对废轮胎胶粉进行表面氧化改性,将氧化改性胶粉用于制备胶粉改性沥青.通过XPS表征证明氧化改性胶粉表面的C—O和C=O的含量显著增加.通过多因素正交试验方法研究氧化剂用量、氧化温度及氧化时间对胶粉改性沥青的25,℃针入度、软化点和5,℃延度等主要性能指标的影响.运用极差分析法和方差分析法探讨了各影响因素对改性沥青性能的敏感性,发现氧化温度对改性沥青性能指标的影响最大,并提出了胶粉氧化改性的最佳反应条件为:氧化剂用量10,m L,氧化温度80,℃,氧化时间3,h.氧化胶粉改性沥青在不使用界面改性剂的条件下,能够使5,℃延度提高到11.6,cm,主要性能指标达到美国废轮胎胶粉改性沥青标准,说明废轮胎胶粉的表面氧化能够显著提高胶粉与沥青的界面结合强度.     

高校图书馆基于微信的留学生信息服务模式探索——以中国石油大学为例

以中国石油大学为例,调查分析了高校图书馆在留学生信息服务方面存在的不足,提出了通过微信改善留学生信息服务的可行途径。     

增压汽油机早燃在线检测与诊断

基于缸内离子电流检测技术,在一台增压进气道多点喷射汽油机上研究了进气温度、负荷、点火提前角、空燃比对于早燃发生频率的影响.试验结果表明,在一定范围内提升进气温度并不会增加早燃发生频率,增大负荷及增大点火提前角将会增加早燃发生频率,缸内混合气加浓将有效抑制早燃发生频率但是会增加油耗.采用的离子电流检测技术,可以实时快速检测早燃循环.并与缸压阈值法相比,离子电流信号判断早燃更准确,能够识别全部早燃循环,包括燃烧压力较小的早燃循环,同时离子电流检测法能够在上止点前25°CA检测到早燃发生的特征信号,这为发动机采取早燃消除方法提供了技术可能.     

关于fnf'-c的值分布

设ｆ为超越亚纯函数,ｃ为不恒等于零的ｆ的小函数,本证得：当ｎ≥３时,ｆ＾ｎｆ‘－ｃ有无穷多个零点,若附加条件ｆ只有有限多个级≤２的零点,则对一切正整数ｎ,ｆ＾ｎｆ’－ｃ都有无穷多个零点,因而对Ｃｈｉａｎｇ Ｙ．Ｍ．的问题作出了部分回答。     

Peritectic solidification under high undercooling conditions

The solidification characteristics of highly undercooled Cu-7.77%Co peritectic alloy has been examined by glass fluxing technique. The obtained undercoolings vary from 93 to 203 K(0.14 TL). It is found that the α(Co) phase always nucleates and grows preferentially, which is followed by peritectic transformation. This means that the peritectic phase cannot form directly, even though the alloy melt is undercooled to a temperature far below its peritectic point. The maximum recalescence temperature measured experimentally decreases as undercooling increases , which is lower than the thermodynamic calculation result owing to the actual non-adia-batic nature of recalescence process. The dendritic fragmentation of primary α(Co) phase induced by high undercooling is found to enhance the completion of peritectic transformation. In addition, the LKT/BCT dendrite growth model is modified in order to make it applicable to those binary alloy systems with seriously curved liquidus and solidus lines. The dendrite growth velocities of primary α(Co) phase are subsequently calculated as a function of undercooling on the basis of this model.     

鼻粉剂四种常用辅料的物理性质考察

作为可以经鼻黏膜给药进脑发挥药效的新剂型———鼻粉剂近来日益受到关注。通过对四种常用辅料的物理性质,包括吸湿性、流动性和喷流性进行考察,可初步为鼻粉剂进一步的处方筛选提供参考。     

GL2(C)的一些不可约表示

设G=GL₂(C), 并且B是G的标准Borel子群, 并且CG, CB分别是群G和群B的在复数域C上的群代数.对于任意B的特征标θ, 定义G的离散诱导模M(θ) = CG×_CBθ. 证明了当θ是反支配权时,M(θ)是个不可约表示.由此给出了一类GL₂(C)全新的、无限维的不可约表示.     

玻璃纤维增强聚合物腰梁受力性能试验与有限元模拟

为探究基坑支护工程中玻璃纤维增强聚合物(glass fiber reinforced polymer, GFRP)腰梁的应力分布规律和变形特性,结合GFRP腰梁力学性能试验及数值模拟,依托于青岛某深基坑工程,利用ABAQUS有限元软件对不同工况下双腹板GFRP腰梁进行了有限元模拟。研究结果表明,与钢材相比,GFRP材料具备较高的抗弯强度,但弹性模量较低;最大加载至700 kN时,双腹板GFRP腰梁变形的室内试验结果和数值模拟结果的变化规律相似,随着荷载水平的增加,呈线性变化,说明GFRP腰梁始终处于弹性工作状态,整体稳定性强。明确了预应力锚杆轴力为300 kN时GFRP腰梁在两端自由、两端约束以及一端约束一端自由3种情况下的应力分布规律和变形特征;对于两端自由的GFRP腰梁,预应力锚杆轴力为150 kN时的应力、位移约为预应力锚杆轴力为300 kN时的50%。研究结果可为类似工程提供借鉴与参考。