影响新疆阜康荒漠地区红砂光合日变化因素的分析

目的 研究新疆阜康荒漠区域优势植物红砂（Reaumuria soongorica）光合及其影响因子的日变化，分析蒸腾速率、光合有效辐射、空气温度、气孔导度、相对湿度、叶面温度、胞间CO2浓度和空气CO：浓度对光合速率的影响。方法利用CI-301 CO2气体分析仪，测定光合及其影响因子的日变化，并进行相关性和多重线性回归分析。结果光合速率日变化形成典型的双峰型；蒸腾速率的日变化曲线呈双峰型；光合有效辐射、空气温度日变化和叶面温度的日变化曲线相近，在午后均呈逐步降低趋势；气孔导度与生境相对湿度的日变化为先下降，然后保持在一定的水平上；水分利用率全天递减。空气CO2浓度、空气温度、相对湿度及叶面温度和气孔导度对红砂光合速率具有显著的影响。结论红砂光合速率日变化曲线形成典型的双峰型，温度是影响红砂光合特性的重要因子之一，气孔因素则是导致其光合速率下降的决定因素。     

对空警戒网有效探测范围的计算方法

给出了空警戒网对不同高度、不同反射面目标有效探测范围的计算方法,可应用于对空警戒网有效探测范围的评估.     

Initiating, growing and cracking of hydrogen blisters

The growing process of a hydrogen blister in a wheel steel was observed in situ with an optical microscope, and the fracture surfaces formed from broken blisters on a wheel steel and bulk metallic glass were investigated. The initiating, growing, cracking and breaking of hydrogen blisters are as follows. Supersaturated vacancies can increase greatly during charging and gather together into a vacancy cluster （small cavity）. Hydrogen atoms become hydrogen molecules in the vacancy cluster and hydrogen molecules can stabilize the vacancy cluster. The small cavity becomes the nucleus of hydrogen blister. The blister will grow with entering of vacancies and hydrogen atoms. With increasing hydrogen pressure, plastic deformation occurs first, the hydrogen blister near the surface extrudes, and then cracks initiate along the wall of the blister with further increasing hydrogen pressure. A cracked blister can grow further through propagating of cracks until it breaks.     

Synthesis of a new meso／microporous composite molecular sieve of MCM-41／mordenite

An MCM-41/mordenite composite with twofold porous structure and stepwise-distributed acidity was prepared for the first time by using zeolite mordenite as the silica-alumina source. The composite molecular sieve has been investigated and compared with a mechanical mixture of mordenite and MCM-41 for their structure, acidity and catalytic activity by means of XRD, N2 adsorption and desorption, HRTEM, DTG, NH3-TPD and catalytic reaction. The characterization results show that the structure and property of the composite molecular sieve are quite different from those of the mechanical mixture, which might be ascribed to the incorporation of secondary building units characteristic of zeolite mordenite into the mesoporous walls of the composite which gives rise to the thicker mesoporous walls, the higher hydrothermal stability and more strong acid sites. Furthermore, the new strategy could be used as a new general method for the preparation of catalysts for the reaction system with multifold large molecules, and the results were well confirmed by the dealkylation of C10^ aromatic hydrocarbon.     

三种芳烃化合物荧光光谱的量子化学研究

芳烃化合物一般具有较大的共轭体系,是一类良好的电致发光材料.本文对三种芳烃化合物的荧光光谱进行了理论研究.在B3LYP/6-31G水平下优化了3种芳烃化合物的几何构型.在振动分析中,均未出现虚频率.基于此,在B3LYP/6-31G的水平下计算了该类化合物的荧光光谱,所有计算结果与实验值基本吻合.     

气相色谱法检测醒脑净冻干粉中龙脑和麝香酮的含量

建立气相色谱外标法分析醒脑净冻干粉中龙脑、麝香酮的含量。用INNOWAX(30 m×0.53 mm,1μm)色谱柱,火焰离子化检测器(FID)进行分析检测。在INNOWAX色谱柱上,龙脑与麝香酮能与其它组分很好的分离,分离度>2.0;龙脑浓度在2.03~0.000 230 mg/mL范围内,r=0.999 9;麝香酮浓度在1.09~0.000 109 mg/mL范围内,r=0.999 9;均呈现良好的线性关系。该方法对龙脑、麝香酮的加标回收率分别为94.1%~99.6%和93.3%~98.4%。该法操作简便、快速、准确性高、重复性好,对同一样品的5次平行测定的相对标准偏差(RSD)<3.0%,可作为本品的质量控制方法。     

SiO2纳米颗粒对电化学沉积半金属Bi膜的影响

研究了SiO2纳米颗粒对电化学沉积半金属Bi膜沉积过程和膜形貌、结构的影响。利用I-V循环扫描曲线分析了未掺与掺入SiO2纳米颗粒后薄膜沉积过程的电化学特性，应用扫描电子显微镜（SEM）和X射线衍射（XRD）对膜的微观表面形貌及相结构进行了表征。实验结果表明。加入SiO2纳米颗粒引起电沉积过程中还原电势向正电位方向移动，使Bi^3＋离子的还原沉积更容易，但不对Bi膜的溶解电位产生明显影响。加入SiO2纳米颗粒后能显著影响沉积膜的形貌，其有明显细化晶粒的效果。总之，SiO2纳米颗粒的加入及加入量显著影响Bi膜的电化学沉积过程和形貌、结构。     

半导体热电材料Bi1-xSbx薄膜的电化学制备

B I1-XSBX半导体合金是性能优异的热电和磁电功能材料,为制备固态电制冷器件、温差发电器件和磁电器件的重要材料。电化学沉积薄膜技术工艺设备简单成本低,在半导体薄膜制备方面有很好的应用前景。系统研究了高浓度盐酸(2.4 MOL/L)的B I和SB盐酸溶液,成份从纯铋逐步变化到纯锑的B I1-XSBX合金半导体薄膜电化学沉积特性。测试了沉积过程I-V循环曲线和和沉积电荷效率等电化学参数。结果表明在所有成份范围内都可以得到典型的B I1-XSBX固溶体结构的高质量薄膜。薄膜生长为典型的溶液扩散控制过程,具有高的沉积电荷效率。薄膜沉积和溶解之间的电位差随溶液中SB(Ⅲ)离子浓度增加而增大,生长的薄膜越来越稳定。在30%SB浓度附近,电化学过程、薄膜结构和性能发生明显的突变。应用X射线衍射和电子显微镜研究薄膜结构,发现薄膜具有明显的(012)择优取向,薄膜晶粒尺寸也随SB浓度的增加而变化。     

上海证券交易所Ａ股市场的波动性分析

运用主要的三种条件异方差模型：ARCH、GARCH、EGARCH模型，对上海证券交易所A股指数的波动性进行拟合，分析模型对上证A股指数收益的波动性、杠杆效应的拟合情况，比较不 同模型对未来波动性的预测情况。实证分析结果表明：EGARCH模型比较适合对我国股票市场 波动性作长期预测，若假设收益序列服从t分布，由此改进的EGARCH-T模型会得到比正态分 布下更好的拟合与预测效果。     

数学实验课的研究与认识

对数学实验这门课程的起源、目的、意义和作用做了明确的阐述。并对课程的内容和教法做了深入的讨论研究,建议数学实验课应该建设成为一门大学数学的技术基础课。