关于工程造价中审核方法的思考

工程造价的预结算审核是合理确定工程造价的必要程序及重要手段.通过时预、结算进行全面、系统的检查和复核,能达到有效地控制工程造价的目的.本文简要分析了工程造价审核的意义及方法,并针对目前存在的问题,提出具体的对策.     

Diastereoselective addition of lithium enolate of γ-substituted α-diazoacetoacetate to <Emphasis Type="Italic">N</Emphasis>-sulfinyl imines

Highly diastereoselective addition of lithium enolate of γ-substituted α-diazoacetoacetate to chiral N-sulfinyl imines has been developed. The addition products were further subjected to photo-induced Wolff rearrangement or Rh(II)-catalyzed intramolecular N–H insertion to afford chiral 4,5-disubstituted 2-oxo and 3-oxo pyrrolidines, respectively.     

基于Tamura纹理和广义判别分析的岩屑图像识别算法

自动、快速、客观地对岩屑进行分类是录井过程中一个非常重要的问题.以往在现场主要是靠人工经验的方式对各类岩屑的百分含量进行估测.但该方法受人为因素的影响较大.本文针对这个问题,提出基于Tamura纹理和广义判别分析的岩屑图像识别算法.算法采用Tamura纹理特征对不同岩性的岩屑图像进行纹理提取,然后将提取的Tamura纹理特征带入GDA(Generalized Discriminant Aanalysis)分类器进行岩屑的识别.通过对四川某地气田4口井的现场随钻的实验结果表明本文算法识别算法具有较高的识别率,为快速自动岩屑分类提供了一个有效的方法.     

具有二维层状结构的铜配位聚合物的合成与晶体结构表征

以二齿配体对氨基苯磺酸为配体,合成了一个具有二维层状结构的铜配位聚合物,并用元素分析、红外光谱、X-射线单晶衍射方法对其进行了表征和晶体结构解析.结果表明该配合物属于单斜晶系,晶胞为P2(1)/c,晶胞参数:a=7.437(3)A°,b=17.408(6)°A,c=7.644(3)°A,β=116.638(5)°,V=884.6(5)A°3,Z=2,Mr=479.96,Dc=1.802 g/cm3,T=298(2)K,F(000)=494,μ(MoKa)=1.528mm-1,R=0.0278,wR=0.0713,S=1.113,(Δ/σ)max=0,层状配位聚合物通过分子间氢键形成三维网状结构.     

Warm/cold rolling processes for producing Fe-6.5wt% Si electrical steel with columnar grains

A new technical prototype for producing Fe-6.5wt% Si electrical steel sheets by directional solidification, heat treatment before rolling, warm rolling, and cold rolling was proposed in the present study. The formability of Fe-6.5wt% Si electrical steel before rolling and the reasonable process parameters of this technical prototype were obtained. Experimental results reveal that the formability of Fe-6.5wt% Si electrical steel is improved significantly under the combination of directional solidification and heat treatment before rolling. Fe-6.5wt% Si electrical steel sheets with the thickness of 0.15 mm, bright surface, few edge cracks, and high rolling yield can be successfully fabricated using this technology without any intermediate annealing during the whole rolling. The combination of directional solidification, heat treatment before rolling, warm rolling, and cold rolling can work as a new process for highly efficient and compact fabrication of Fe-6.5wt% Si electrical steel sheets.     

Discussion on the Construction Technology of Manual Hole Digging Pile Application

笔者根据自己多年的施工技术经验,结合工程实例,对人工挖孔灌注桩的施工工艺进行了详细的阐述与探讨.     

微生物学设计性拓展实验的教学探索

微生物学作为一门重要的专业基础课,知识涵盖面广、实践性和操作性强.在完成微生物学基本实验的基础上,开展设计性拓展实验,有利于进一步拓宽学生的视野,增强学生的动手能力,提高学生的探究能力.     

Comparative study on the passivation layers of copper sulphide minerals during bioleaching

The bioleaching of copper sulphide minerals was investigated by using A. ferrooxidans ATF6. The result shows the preferential order of the minerals bioleaching as djurleite>bornite>pyritic chalcopyrite>covellite>porphyry chalcopyrite. The residues were characterized by X-ray diffraction (XRD) and scanning electron microscopy (SEM). It is indicated that jarosite may not be responsible for hindered dissolution. The elemental sulfur layer on the surface of pyritic chalcopyrite residues is cracked. The compact surface layer of porphyry chalcopyrite may strongly hinder copper extraction. X-ray photoelectron spectroscopy (XPS) further confirms that the passivation layers of covellite, pyritic chalcopyrite, and porphyry chalcopyrite are copper-depleted sulphide Cu₄S₁₁, S8, and copper-rich iron-deficient polysulphide Cu₄Fe₂S₉, respectively. The ability of these passivation layers was found as Cu₄Fe₂S₉>Cu₄S₁₁>S₈>jarosite.     

丙烯酰胺降解菌的筛选及优势菌株降解条件优化

通过富集培养和选择培养分离, 从江西昌九农科化工有限公司厌氧池废水中筛选分离到能够降解丙烯酰胺单体的菌株, 对菌株的培养基配方及降解工艺条件进行优化. 测定菌株对丙烯酰胺的降解性能, 得到一株降解效果较好的菌株AM-4, 通过生理生化特性初步鉴定其属于葡萄球菌属.     

改进型序关系分析法及其应用

摒弃原序关系分析法中要求评价指标间满足强一致性的条件,提出了要求评价指标满足弱一致性的观点,并对序关系分析法进行了改进.基于评价指标贡献率的概念,在改进型序关系分析法的基础上,利用评价者的“宏观”判断信息,给出了一种确定评价指标权重的方法.最后,结合实例给出了应用.