块状纳米材料的设计理论研究

在二元共晶Spinodal系统中 ,Spinodal波长的大小随过冷度的增加而减少 ,并存在一个最小的波长 ,此时合金的生长速度最快 .提出当过冷度足够大时 ,液态Spinodal的波长进入到纳米尺度 ,形成块状纳米材料 .由于液态的扩散较易发生 ,当波长为纳米量级时 ,Spinodal的转变时间为微秒量级 .由于液体表面张力等的影响 ,液态Spinodal的组织由网状变成微粒形态 .     

Effect of deep cryogenic treatment on the properties of 80CrMo12 5 tool steel

The effect of deep cryogenic treatment on the mechanical properties of 80CrMo12 5 tool steel was investigated. Moreover, the effects of stabilization (holding at room temperature for some periods before deep cryogenic treatment) and tempering before deep cryogenic treatment were studied. The results show that deep cryogenic treatment can eliminate the retained austenite, making a better carbide distribution and a higher carbide amount. As a result, a remarkable improvement in wear resistance of cryogenically treated specimens is observed. Moreover, the ultimate tensile strength increases, and the toughness of the sample decreases. It is also found that both stabilization and tempering before deep cryogenic treatment decrease the wear resistance, hardness, and carbides homogeneity compared to the deep cryogenically treated samples. It is concluded that deep cryogenic treatment should be performed without any delay on samples after quenching to reach the highest wear resistance and hardness.     

Preparation of high-strength Al-Mg-Si-Cu-Fe alloy via heat treatment and rolling

An Al-Mg-Si-Cu-Fe alloy was solid-solution treated at 560°C for 3 h and then cooled by water quenching or furnace cooling. The alloy samples which underwent cooling by these two methods were rolled at different temperatures. The microstructure and mechanical properties of the rolled alloys were investigated by optical microscopy, scanning electron microscopy, transmission electron microscopy, X-ray diffraction analysis, and tensile testing. For the water-quenched alloys, the peak tensile strength and elongation occurred at a rolling temperature of 180°C. For the furnace-cooled alloys, the tensile strength decreased initially, until the rolling temperature of 420°C, and then increased; the elongation increased consistently with increasing rolling temperature. The effects of grain boundary hardening and dislocation hardening on the mechanical properties of these rolled alloys decreased with increases in rolling temperature. The mechanical properties of the 180°C rolling water-quenched alloy were also improved by the presence of β″ phase. Above 420°C, the effect of solid-solution hardening on the mechanical properties of the rolled alloys increased with increases in rolling temperature.     

基于XML Web服务监控系统的设计与实现

首先分析了一般监控系统的缺点 ,然后针对这些缺点提出了XMLWeb服务体系结构 ,并介绍了XMLWeb服务的基本原理和所用协议 .最后基于XMLWeb服务 ,在分布式环境中 ,设计和实现了机群监控系统 .在系统设计中采用了模块化设计 ,使系统可以按照不同的功能分成不同的模块 .该系统能够通过网络收集车辆状态信息和位置信息 ,并通过GIS组件显示车辆位置以达到监控目的 .该监控系统还利用分布式设计 ,实现了数据共享、功能分散 ,从而提高了系统的稳定性、安全性 ,并使系统易于扩充和维护 .     

莲房多酚的微波辅助提取技术

采用微波辅助提取莲房中多酚类化合物,并与体积分数60%丙酮回流提取法相比较.通过考察溶剂体积分数、微波输出功率、料液比、微波辅助萃取时间四因素,设计正交试验,优化莲房多酚提取工艺条件为:提取时间90 s,微波输出功率700 W,丙酮体积分数为60%,料液比1: 25(g·mL-1).在此条件下,莲房多酚和原花青素的提取得率分别为11.88%和5.58%,是体积分数60%丙酮回流提取法结果的2.1倍和2.6倍.经IR分析和HLPC检测,微波对莲房多酚类物质的结构和组成无影响,表明微波辅助法适合莲房多酚的提取.     

Cupric ion release and cytotoxicity for Yuangong Cu-IUDs and the release behavior of indomethacin for medicated 220 Cu-IUD

These years Yuangong copper-bearing intrauterine devices （Cu-IUDs） have been used because of less side effects in use. The corrosion of copper is essential to the success of contraception, and the release behavior of indomethacin from medicated Cu-IUD is related to its therapeutic effect. In this study, analytical methods were established to investigate the release behavior of cupric ion of three kinds of Yuangong Cu-IUDs and indomethacin of medicated Yuangong 220 Cu-IUD. Cu-IUDs were incubated in simulated uterine solution （SUS）. The concentrations of cupric ion and indomethacin were analyzed by flame atomic absorption spectrometer （FAAS） for 60 days and UV/vis -3310 spectrophotometer for 60 days, respectively. The morphology of copper after corrosion was characterized by SEM. In addition, we detected cytotoxicity by MTT of L929 mouse fibroblasts cells caused by extracts of the three Yuangong Cu-IUDs. The release behavior of cupric ion for three kinds of Yuangong Cu-IUDs was biphasic, which consisted of the initial burst release and then slow and constant release. In vitro release experiment confirmed a biphasic release of indomethacin from Yuangong 220. The copper wire of Yuangong Cu-IUDs showed uneven corrosion. The RGR value of Yuangong 365 Cu-IUD was smaller than that of medicated Yuangong 220 Cu-IUD and RGR value of medicated Yuangong 220 Cu-IUD was smaller than that of Yuangong 300 Cu-IUD. The cupric ion release and indomethacin release showed biphasic. Indomethacin increased the cupric ion release rate and might diminish the adverse effects caused by burst release of cupric ion. The toxicity grade of these three Yuangong Cu-IUDs was 4. We should canvass the adverse events of Cu-lUDs based on practical experiments, and try our best to reduce the toxicity of Cu-lUDs.     

高强混凝土扁柱拟静力试验

为研究高强混凝土扁柱的抗震性能,以6根缩尺模型为1∶3的不同轴压比、混凝土强度、剪跨比扁柱试件为研究对象,采用拟静力试验方法,通过对试验现象的观察以及试验数据的处理,定量地从刚度、骨架曲线、滞回曲线、延性、耗能能力等几个方面详细分析了试验试件的抗震性能.研究结果表明,此类构件延性较差,耗能能力差,但在合理构造措施下,破坏形式仍为压弯型,破坏截面符合平截面假定.     

A forensic method for efficient file extraction in HDFS based on three-level mapping

The large scale and distribution of cloud computing storage have become the major challenges in cloud forensics for file extraction. Current disk forensic methods do not adapt to cloud computing well and the forensic research on distributed file system is inadequate. To address the forensic problems, this paper uses the Hadoop distributed file system (HDFS) as a case study and proposes a forensic method for efficient file extraction based on three-level (3L) mapping. First, HDFS is analyzed from overall architecture to local file system. Second, the 3L mapping of an HDFS file from HDFS namespace to data blocks on local file system is established and a recovery method for deleted files based on 3L mapping is presented. Third, a multi-node Hadoop framework via Xen virtualization platform is set up to test the performance of the method. The results indicate that the proposed method could succeed in efficient location of large files stored across data nodes, make selective image of disk data and get high recovery rate of deleted files.     

基于E-H和VAR模型的国内外原油市场融合性研究

与国际原油市场的融合程度决定了国内原油市场对国际原油市场的影响程度,更意味着中国开放本国原油市场的程度,这与我国能源安全息息相关.分别运用E-H检验从市场边界层面和建立向量自回归模型从价格影响层面对国际国内原油市场的融合进行测度.可以发现,我国正加速与国际原油市场的融合,但这种一体化程度仍然较弱,反映在我国原油价格受世界原油价格的影响较大,但对世界原油价格的影响较小.因此,为保障国家能源安全,必须建立本国原油期货市场,加速争夺国际原油定价权,维持国内原油价格相对稳定.     

上海快速城市化不同阶段城市热场景观格局演变研究

本文以上海市为例对城市热环境的空间分布特点及不同城市化阶段的演变特征进行分析.研究表明:随着上海城市化的深入,热环境空间结构趋于复杂,不同的城市化发展阶段热环境格局呈现出截然不同的演变特征.结合景观格局指数与转移矩阵对热环境的演变规律进行分析得出:城市化高速发展阶段,主城区及近郊区内的低温斑块等级上升明显,热环境格局的聚合度显著下降,景观多样性指数明显上升.优化发展阶段,主城区内强热场面积下降,近郊或远郊地区强热场明显增加,总体热环境格局的聚合度及多样性指数变化趋势减弱.本次研究结果展现了城市化不同阶段中城市热环境格局的分布与演变特征,为科学制定应对城市热岛问题的措施提供科学的参考.