铜转炉烟灰酸浸净化液中锌的萃取分离

以p204为萃取剂,260号磺化煤油为稀释剂,从铜转炉烟灰酸浸净化液中萃取分离锌.考察萃取振荡时间、p204的体积分数、相比率(O/A)以及料液初始pH值对锌萃取率的影响.通过正交实验和单因素分析确定p204从铜转炉烟灰酸浸净化液中萃取分离锌的主要影响因素和最佳工艺条件.研究表明:室温条件下,当萃取平衡时间为6 min,p204的体积分数为30%,相比率(O/A)为2∶1,料液初始pH值为3.0时,锌的一级萃取率达到57.32%.经4级错流萃取可以将料液中锌的质量浓度降低到0.027 g/L,锌萃取率达到97.26%.负载有机相经2 mol/L的H2SO4反萃,锌可完全反萃.     

Particle simulation of the failure process of brittle rock under triaxial compression

In order to investigate the failure process of brittle rock under triaxial compression through both experimental and numerical approaches, the particle simulation method was used in numerical simulations and the simulated results were compared with those of the experiment. The numerical simulation results, such as fracture propagation, microcrack distribution, stress-strain response, and damage patterns, were discussed in detail. The simulated results under various confining pressures (0–60 MPa) are in good agreement with the experimental results. The simulated results reveal that rock failure is caused by axial splitting under uniaxial compression. As the confining pressure increases, rock failure occurs in a few localized shear planes and the rock mechanical behavior is changed from brittle to ductile. Consequently, the peak failure strength, microcrack numbers, and the shear plane angle increase, but the ratio of tensile to shear microcracks decreases. The damage formation during the compression simulations indicates that the particle simulation method can produce similar behaviors as those observed through laboratory compression tests.     

黄土高原坡沟系统径流泥沙过程

利用概化的坡沟系统模型,采用室内放水冲刷试验,对黄土高原坡沟系统径流侵蚀产沙过程进行模拟研究。结果表明:坡沟系统的产流产沙速率随流量的增大而增大;产流量随放水量的增大呈明显的指数函数变化趋势,且增长率有增大趋势;产沙量随冲刷流量的增大呈幂函数增大趋势,增长率却逐渐减小;冲刷流量相同时,产沙速率随冲刷历时呈现出波动式的双峰增长趋势;在实验流量和时间范围内,坡沟系统的累积产沙量随累积径流量呈现出非常显著的二次函数关系.     

A preliminary study of chronology for a newly-discovered ancient city and five archaeological sites in Lop Nor,China

In the past century, it has long been debated in the archeological, historical, geographical, and many other related communities where the capital of the Luolan and Shanshan states was in the Lop Nor region. This paper presents three AMS radiocarbon ages from a newly-discovered ancient city at about 6.3 km to the northwest of the Xiaohe Graveyard, and fifteen new radiocarbon ages from the Loulan (LA), LE, Qieerqiduke, Milan, and Tuyin sites in Lop Nor. The new investigation shows that the age of newly-disco...     

解析双证书制度的推行障碍——论深化“赋能于人”的教改

衡量使命,应大力推行双证书制度,开展"赋能于人"的教改与创新,使受训者赢得更好的就业机会和就业后的发展前景。有效推行双证书制度,必须解决系统功能不适、必须破解关键障碍。     

黄原胶质量分数对受压猪肉凝胶品质的影响

将黄原胶作为脂肪替代物,采用单因素试验方法,研究超高压作用下(压力400 MPa、保压时间30 min、加压介质温度40℃)黄原胶浓度对受压猪肉凝胶保水性、色泽与质构特性的影响.结果表明,黄原胶质量分数对受压与未受压猪肉凝胶的保水性、色泽和质构参数均有显著影响(P0.05);质量分数提高,受压与未受压凝胶的保水性显著提高、各TPA参数显著下降、黄度显著增强(P0.05);在质量分数0.4%~0.6%时,受压凝胶的各质构参数均显著高于未受压组(P0.01),而在质量分数为1%时,受压凝胶的各质构参数反而显著低于未受压组(P0.05).由此说明黄原胶添加水平不同,受压凝胶的质构参数变化也不同.     

论教师的法律地位及其权利义务

教师的法律地位是指通过教育法律法规确认的教师的职业地位、法律人格和教师的权利义务。文章通过对教师法律地位的理论分析把教师法律地位界定为＂准公务员＂。教师的权利义务是教师法律地位的具体体现。《中华人民共和国教师法》规定的教师权利义务已经存在缺陷,不适应现代教育理念和目标的需要,只有提高教师待遇,健全教师权益的保障机制,明确教师法律地位并完善教师的申诉制度才能保障教育的持续、可靠发展。     

基于自评估HMM的离心泵状态识别方法研究

由于HMM本身的特点,在实际应用中如何找到一个合适的HMM模型始终是一个难点.采用传统的Baum-W elch算法对HMM进行训练,并提出了一种对训练结果进行评估的方法,构建了可自动评估的HMM训练体系.     

TiO_2纳米管薄膜的制备及其光电性能研究

将水热法制备的TiO2纳米管在600℃下焙烧,用焙烧产物制备染料敏化太阳能电池中的薄膜电极,同时与未焙烧的TiO2纳米管制备的薄膜电极进行光电性能比较。结果表明,600℃焙烧纳米管产物制备的薄膜电极短路电流和开路电压分别达到17.45mA/cm2和0.60V,光电转化效率提高到5.65%,高于未焙烧的TiO2纳米管制备的薄膜电极相应值,且机械性能良好,不易剥落。     

Gen-2标签的RFID认证协议的研究

针对RFID系统的Gen-2类标签容量有限的特点,提出了一种基于Gen-2标签的RFID认证协议,将标签32位ID号分为低16位和高16位,利用标签的CRC-16位生成相应校验码作为密文传输.该协议避免了已有协议在安全性方面的5个缺陷,提高了数据库查询速度、降低了RFID标签的设计成本.并利用BAN逻辑对所提出协议的目标、假设和消息传递进行形式化分析,从理论上证明了该协议是安全可达的.