Influence of minor boron on the microstructures of a second generation Nibased single crystal superalloy

Boron is added into single crystal superalloys as a micro-alloying element to strengthen low angle grain boundaries.However,systematic investigations on the effect of boron on microstructures of single crystal superalloys are limitedly reported.The effect of boron on as-cast and heat-treated microstructures was investigated in two experimental Ni-based single crystal superalloys containing 3 wt% Re.The current results indicated that the volume fraction of(γ+γ′)eutectic and M_3B_2 borides was evidently increased,while the number of micropores was evidently decreased with the addition of 0.02 wt% boron.The(γ+γ′)eutectic could not be dissolved completely due to the lower incipient melting temperature caused by the formation of M_3B_2 borides.Meanwhile,the M_3B_2 borides were found to be enriched with indispensable strengthening elements Cr,Mo,W and Re,and this may lower the strengthening effect and cause stress concentration during high temperature creep.     

Mechanical characterization and strain-rate sensitivity measurement of Ti- 7333 alloy based on nanoindentation and crystal plasticity modeling

The relationship between crystal orientations and meso-mechanical properties of β phase Ti-7333 titanium was investigated through the combination of nanoindentation experiments and simulation. The crystal plasticity finite element(CPFE) model for nanoindentation of single body-centered cubic crystal was established based on the experimental data. And the crystal plasticity constitutive law was implemented to simulate the nanoindentation process, obtaining satisfied results with an acceptable error. From the simulated pileup morphology patterns with different crystal orientations, it was found that the β phase experienced a symmetrical and orientation-related deformation process. Meanwhile, the strain-rate sensitivity(SRS) of β phase was investigated through nanoindentation tests based on continuous stiffness measurement(CSM) under different strain rates,varying between 0.2, 0.05 and 0.01 s~(-1). Two grains with different orientations exhibited similar SRS exponents,m, calculated from the experimental results.     

WO3 nanoflakes decorated with CuO clusters for enhanced photoelectrochemical water splitting

The low quantum efficiency arising from poor charges transfer and insufficient light absorption is one of the critical challenges toward achieving highly efficient water splitting in photoelectrochemical cells. Three dimensions(3D) structures and heterojunctions have received intensive research interests recent years due to their excellent ability to separate photo-generated charges as well as the enhanced light harvesting property. Herein,3 D Cu O/WO_3 structure was fabricated through a facile solvothermal method followed by chemical bath deposition. The loading of Cu O clusters on WO_3 nanoflake arrays results in a much improved photocurrent density compared with that of pristine WO_3 nanoflake arrays, which reaches 1.8 m A/cm2 at 1.23 V vs. the reversible hydrogen electrode. The electrochemical impedance spectroscopy measurement demonstrates that the improved performance of Cu O/WO_3 electrode is attributed to the accelerated charge transfer kinetics as a result of the desirable band alignment in Cu O/WO_3 heterojunction. This work demonstrates a facile strategy to construct superior WO_3 electrode, which will ultimately allow for efficient storage of solar energy into hydrogen.     

新的非线性常微分方程的可积类型

本文给出了文[1]、[2]研究的非线性常微分方程可积类型以统一的形式,提供了可积的充分条件及其通积分,并且推广了文[1]、[2]的有关结论,因而得到了新的非线性常微分方程的可积类型。     

一类数字图像篡改的被动认证

在没有被嵌入水印也没有辅助信息可利用的前提下，针对一类特殊的图像篡改——复制遮盖篡改即遮盖的内容复制自同一幅图像中，提出一种基于小波分解的自相关检测方法，将图像划分为相互重叠的小块，提取每一个小块的小波分解低频子带作为特征向量，采用Pearson相关系数进行块相似性匹配检测，实验结果表明该方法能够抵抗图像复制部位的无缝处理，对一般的高斯噪声、低通滤波、JPEG压缩等噪声攻击具有较好的鲁棒性。     

茁霉多糖发酵工艺条件研究

以出芽短梗霉为生产菌株，蔗糖为碳源进行发酵生产茁霉多糖．通过摇瓶实验，确定了该菌株的发酵条件，并对发酵条件进行了优化，在此条件下，获得了较高的多糖产量．实验表明，摇瓶转速和发酵初始pH值是多糖发酵的重要影响因素，它们与多糖的合成密切相关．     

高层短肢剪力墙结构变形能力分析优化

短肢剪力墙结构以剪力墙为基础,并吸取框架的优点,已广泛应用于工程实践中.应用ANSYS软件对高层T形短肢剪力墙结构的变形能力进行了仿真试验,分析了楼层层数、连梁跨高比、墙肢截面高厚比和轴压比等因素对变形能力的影响,并对结果进行了分析优化,为工程中的T形短肢剪力墙结构设计提供理论和试验依据.     

基于散射电场的飞机旋翼多普勒回波模拟

旋翼飞机飞行过程中会产生具有独特多普勒特征的雷达回波,通过对旋翼回波的准确模拟,可为不同类型飞机的精确识别提供重要依据.针对现有散射点叠加算法的假设缺陷,从目标高频电磁散射理论出发,提出了基于散射电场的飞机旋翼回波模拟方法.依据电磁散射场与雷达回波方程间的数学关系,发现目标回波的基带信号与目标后向散射电场的复振幅矢量具...     

有毒生物难降解有机污染物的研究进展

对有毒生物难降解有机污染物（Persistent Toxic Substances,简称PTS）的特性、分布、迁移及来源进行了介绍,综述了目前对PTS的分析和控制处理方法,对光催化高级氧化技术处理PTS进行了阐述.     

关于大型科研仪器共享问题的一个产权理论解释

大型科研仪器的共享问题是我国科技资源配置和管理工作中面临的重要问题,现有研究和对策主要集中于促进共享理念的传播、加强共享效率的考核以及仪器中心等共享机制的建设方面,但对于为什么存在共享障碍等基本问题缺少关注。本文以经济学中的产权理论为基础,从大型科研仪器所有权与控制权分离的现实出发,探讨了当前我国仪器共享中存在的利益冲突和机制障碍。在此基础上,借鉴发达国家的一些做法,提出从仪器资助体制出发解决仪器共享问题的新思路。