Synthesis and characterization of bifunctional terbium complex-based nanoparticles

Novel bifunctional terbium complex-based nanoparticles were developed using a modified Stber method and a layer-by-layer assembly process. A magnetic core of Fe3O4 nanoparticles was coated with a silica shell to form the first layer. Then a ternary Tb3+ complex (TESPPA-Tb), which acted as a luminescent marker, was covalently bound to the silica surface by stable Si-O-Si bonds. The TESPPA monomer was synthesized by binding pyridine 2,6-dicarboxylic acid to 3-aminopropyltriethoxysilane, which was used as a ligand for coordination with the Tb3+ ions. An outer shell of silica was applied to the nanoparticles to allow for versatility with surface functionalization. The nanoparticles were characterized by X-ray powder diffraction, transmission electron microscopy, Fourier transform infrared spectroscopy, ultravioletvisible spectroscopy, vibration sample magnetometer, and photoluminescence spectroscopy. The bifunctional nanoparticles exhibited favorable superparamagnetic behavior and photoluminescence properties of Tb3+. These nanoparticles have potential applications in biolabeling, bioseparation, immunoassays, and pathogenic diagnosis.     

扬弃·改造·复兴──兼评《出路在于向西方乞灵》

中国传统音乐文化与西方音乐文化存在着相对性差距与绝对性差距。清醒地认识到这个事实，在坚持发挥本民族音乐的内在神韵与气质的同时，认真学习西方音乐文化中更丰富地展示人类灵魂的表现体制，才能为中国音乐的发展确定正确的方向，实现民族音乐的全面复兴。     

电镀铬生产中三价铬行为分析及控制

本介绍了电镀铬生产中三价铬所起的作用，分析其在溶液中含量变化给生产带来的影响，提出了正确控制三价铬的方法，对解决由于三价铬变化赞成的电镀铬质量问题具有一定的参考价值。     

数学教学中培养学生思维能力的途径

思维能力是认识能力的核心,它受诸多因素的影响,而且因人而异,客观上存在着差异.优秀的思维品质不是与生俱来的,而是在解决问题的实践中逐步形成的.因此,在数学教学中应不失时机地培养学生的思维能力.     

催化剂电梯抱闸控制系统的改进

通过对实际现场中电梯抱闸控制系统的调查与研究,发现目前此控制系统存在较大的问题,经常引发控制系统故障的产生,导致电梯不能正常运行,维修成本居高不下、严重影响了装置的正常生产。因此对此控制系统做出改进。     

Synthesis of novel superhard materials under ultrahigh pressure

Superhard materials are solids whose Vickers hardness is beyond 40 GPa. They have wide applications in industry such as cutting and polishing tools, wear-resistant coatings. Most preparations of superhard materials are conducted under extreme pressure and temperature conditions, not only for scientific investigations, but also for the practical applications. In this paper, we would introduce the recent progress on the design and preparations of novel superhard materials, mainly on nanopolycrystalline diamond, B–C–N superhard solid solutions, and cubic-Si3N4/diamond nanocomposites prepared under ultrahigh pressure and high temperature（HPHT）, using multi-anvil apparatus based on the hinged-type cubic press. Bulk materials of all these superhard phases have been successfully synthesized and are systematically tested. We emphasize that ultra-HPHT method plays an important role in the scientific research and industrial production of superhard materials. It provides the driving forces for the light elements forming novel superhard phases as well as the way for sintering high-density nanosuperhard materials.     

从天时地利人和谈篮球比赛的主场优势

中国传统文化的成功论讲究天时、地利、人和,我国古代战争中常指占有这几种优势的一方,其胜算就大.现在在世界顶级篮球联赛的NBA、我国的CBA及欧洲的各种篮球联赛,组织者都是从这几方面着手,来激发主场运动员的潜能,发挥球队的主场优势,从而夺取比赛的胜利.本文运用文献资料法,通过分析天时、地利、人和在篮球主场比赛中的具体体现,旨在进一步提高我们对主场优势的认识.     

The Closest and Farthest Points to an Affine Ellipse or Ellipsoid

Affine ellipses/ellipsoids based bounding volumes are widely used in various graphics applications,such as ray tracing and collision detection.They provide a much tighter fit than the regular ellipses/ellipsoids.The most important operation involved is to compute the closest/farthest point,on a given ellipse/ellipsoid,with respect to a user specified point.In this paper,we first formulate such a problem for the ellipse case into solving a quartic equation and then for the ellipsoid case by solving a system of quartic equations.The method proposed in this paper is elegant and highly efficient.     

硬轴连接的多台直流电动机拖动系统

本文对多台直流电动机（他励）硬轴联接时的负荷平衡问题进行了研究，并给出了双电机拖动的负荷平衡调节的方案。     

基础防水混凝土冬期负温施工

以鞍钢三烧改造工程中的带冷机基础混凝土的施工为例，讨论要求达到Ｓ８抗渗标号的冬期负温施工问题。分析此种混凝土的防冻机理，采取综合技术措施可获得预期效果。