苯甲醛缩氨基硫脲Cu(I)、Zn(Ⅱ)配合物的直接电化学合成

用电化学金属阳极氧化法在非水溶剂中合成了苯甲醛缩氨基硫脲（ＨＬ）与Ｃｕ（Ｉ）、Ｚｎ（Ⅱ）配合物,通过元素分析、红外光谱、紫外光谱、磁矩、摩尔电导等对配合物进行了表征。     

SAG法合成钛酸铅纳米晶粒的工艺和结构研究

ＳＡＧ法合成钛酸铅纳米晶粒的工艺和结构研究李永祥刘泽吴冲若（东南大学电子工程系,南京２１００９６）ＰｂＴｉＯ３是应用广泛的铁电和光电材料之－,研究ＰｂＴｉＯ３纳米晶粒的合成技术和电学性能对基础研究和新型复合功能材料研究都有重要意义．作者曾采用Ｓｏｌ...     

土法造纸木素降解之探索Ⅲ.嫩毛竹自然发酵过程中的细菌分离鉴定与嫩竹软化菌的筛选

试验证实,嫩毛竹自然发酵过程中的微生物主要是细菌。分离出并纯化了１００株细菌,其中６０株是芽胞杆菌。将分离出的１００株细菌分别接入石灰预处理过的嫩竹,从中筛选出能使嫩竹进一步软化的菌株３株,也均为芽胞杆菌。对这６０株芽胞杆菌进行了形态学及其生理生化特征的鉴定,按Ｐｒｉｅｓｔ氏等（１９８８年）的数值分类系统分类到组,将３株（３０８,３０９,３１０）对嫩竹软化有明显作用的芽胞杆菌的１株（３０８）鉴定到种,认为是短小芽胞杆菌（Ｂ．ｐｕｍｉｌｕｓ）。另外４０株非芽胞杆菌参阅《伯杰氏系统细菌学手册》第１卷和第２卷,鉴定到科或属,有微球菌、葡萄球菌、李氏杆菌、不动杆菌、肠杆菌科等。     

五种药剂对美洲斑潜蝇Liriomyza sativae的毒力测定

美洲斑潜蝇是近年来传入我国的一种检疫性害虫,给疏菜、花卉生产造成了很大损失。本文采用液浸法对豇豆上的美洲斑潜蝇室内子一代幼虫进行了毒力测定.结果表明,毒死蜱、杀虫双、氯氰菊酯、毒杀土、制潜灵对美洲斑潜蝇的LC_(50)分别为:272.02、254.46、109.16、85.76、32.42ppm。制潜灵的毒性最强、毒杀土、氯氰菊酯次之,毒死蜱、杀虫双较差。     

甲氰菊酯与单甲脒复配对桔全爪螨Pnonychus citri的增效作用研究

将甲氰菊酯和单甲脒通过复配对桔全爪螨进行室内毒力测定,表明两种药剂的各种配比均对桔全爪螨存在着不同程度的增效作用,其中以甲氰菊酯与单甲脒按1:4的比例复配增效作用最为明显,共毒系数达到373。田间药效试验也表明,20％的混剂乳油(4％甲氰菊酯 16％单甲脒)的药效明显高于20％的甲氰菊酯乳油和25％的单甲脒乳油。     

Leakage of mantle helium from the Liaodong Peninsula, China

The isotopic cumpositions of helium have been investigated in hot spring gases sampled from the Liaodong Peninsula. China. The³He/⁴He ratios range from 0.14 Ra (0.14 times the atmospheric³He/⁴He ratio of 1.40 × 10^-6 to 0.72 Ra.³He/⁴He versus⁴He/²⁰Ne ratios and He contents suggest that a small amount of mantle-derived helium reaches the earth’s surface. Helium iwtope ratios of the hot spring gases show a distribution pattern similar to the regional heat flow values, indicating that the positive thermal anomaly occurring in the rtrea is closely associated with the presence of mantle-derived helium. The observations described above provide some significant evidence that the molten magma originating from partial melting of the upper mantle may have intruded into the continental crust along the activity fault. The coupling of the presence of mantle He and heat flow anomalies to seismic activity in studied region seem to imply that there is an internal relationship between mantle degassing and seismic activity.     

Properties of a supercritical superdiffusion and solutions of its corresponding differential equation

The range and the nonextinction property of a supercritical superdiffusion and solutions of its corresponding differential equation are studied. It is pruved that under a suitable condition, the conditioned superprocess of the supercritical superdiffusion is a subcritical superdiffusion.     

Cloning, construction of prokaryotic expression vector and expression ofEscherichia coli cytosine deaminase gene

Cytosine deaminase gene ofEscherichia coli strain H-30 was cloned, and its initiation codon of ‘GTG’ was mutated to ‘ATG’ by PCR. Prokaryotic recombinant expression vector pBV220-CD was constructed. Clone with high enzyme activity were selected by detecting their specific activity of cytosine deaminase. 5-FC(5-FC, 5-fluorocytosine) could induce the lethal toxicity to cells containing active CD gene. DNA sequence analysis indicated that there were 16 altered bases and 5 of them resulted in the alteration of amino acids in predicted peptide by comparing DNA sequence of the clone H-30-CD-11 with high enzyme activity with CD gene reported in Gene Bank.     

用^1H—NMR测定纤维素的摩尔取代度

用＾１Ｈ－ＮＭＲ测定羟丙基纤维素的摩尔取代度,根据纤维素在ＤＣｌ中水解后的＾１Ｈ－ＮＭＲ谱峰面积来计算ＭＳ值。同时还应用铬酸氧化蒸馏法测定了羟丙基纤维素的ＭＳ值,以及利用ＭＳ与羟丙基含量的关系得到ＭＳ值,可以发现ＮＭＲ的方法是可行的。     

射流携带床气化炉内混合过程的数值模拟

采用ｋ－εＥ模型对射流携带床气化炉内α－萘酚与对氨基苯磺酸重氮盐的偶合竞争串联反应的分隔指数进行了数值模拟,研究了气化炉出口面积,长径比,两股射流动量比对分隔指数的影响。模拟结果表明,ｋ－ε－Ｅ模型由于同时考虑了宏观混合和微观混合的作用,其观测值和实验测试值吻合较好。