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141.
铁锆混合交联蒙脱土的酸性和催化性能研究 总被引:3,自引:0,他引:3
制备了锆交联蒙脱土(Zr─PILC)和铁锆混合交联蒙脱土(Fe─Zr─PILC─1/4,Fe─Zr─PILC-1/5),并用吡啶吸附红外光谱和氨程序升温脱附等方法对其酸性进行了研究。结果表明:Fe-Zr-PILC-1/4,Fe-Zr─PILC-1/5与Na─原土相比,中强酸和强酸酸量均增加,而与Zr─PILC相比,中强酸和强酸酸量均减少,且中强酸强度减弱。以甲醇胺化反应为探针研究了样品酸催化活性。结果表明:Fe-Zr-PILC─1/4和Fe-Zr-PILC-1/5活性比Na─原土高,但低于Zr-PILC。起酸催化作用的主要是L酸中心。 相似文献
142.
Evaluation of flotation behavior, solution measurements, and surface analyses were performed to investigate the effects of chloride ion addition on the sulfidization of cerussite in this study. Micro-flotation tests indicate that the addition of chloride ions prior to sulfidization can significantly increase the flotation recovery of cerussite, which is attributed to the formation of more lead sulfide species on the mineral surface. Solution measurement results suggest that the addition of chloride ions prior to sulfidization induces the transformation of more sulfide ions from pulp solution onto the mineral surface by the formation of more lead sulfide species. X-ray diffraction and energy-dispersive spectroscopy indicate that more lead sulfide species form on the mineral surface when chloride ions are added prior to sulfidization. These results demonstrate that the addition of chloride ions prior to sulfidization can significantly improve the sulfidization of cerussite, thereby enhancing the flotation performance. 相似文献
143.
This paper is an extension of the application of neighborhood interference model--being modified--to the study of the interference between forest plants and herbaceous plants. The exploration of the neighborhood interference between triploid Populus tomentosa and Lolium multiflorum shows that the interference of Lolium multiflorum on triploid populus tomentosa is positive, with the primary interference factor living weight, and secondary factor cover degree; the growth of an individual tree is affected by the number, height, and coverage of the Lolium multiflorum; the more dense the coverage of the Lolium multiflorum in a certain area, the taller, faster and more trees will grow as a result of a greater positive neighborhood interference. The modified neighborhood interference model well serves as an effective approach to extend the application of neighborhood interference researches. 相似文献
144.
Synthesis of BiOCl photocatalyst by a low-cost,simple hydrolytic technique and its excellent photocatalytic activity 下载免费PDF全文
Yan Wang Zhu-qing Shi Cai-mei Fan Xiao-gang Hao Guang-yue Ding Yun-fang Wang 《矿物冶金与材料学报》2012,19(5):467-472
A novel photocatalyst, bismuth oxychloride (BiOCl) micro-nano particles with a fine ferrite plate structure, was prepared by a low-cost, simple hydrolytic method. The as-prepared BiOCl was characterized by scanning electron microscopy (SEM), thermogravimetric analysis-differential thermal analysis (TGA-DTA), X-ray diffraction (XRD), and UV-vis diffuse reflectance spectra (DRS). The effects of preparation conditions such as sodium dodecyl benzene sulfonate (SDBS) dispersant, HCl concentration, and heat treatment temperature on BiOCl performances were investigated. Moreover, its photocatalytic activity was evaluated on the degradation of methylene orange (MO) and was compared with that of TiO2 (P25). The experimental results confirmed that BiOCl micro-nano particles prepared with SDBS, the HCl concentration of 1.5 mol/L, and the heat treatment temperature of 80℃ exhibited the best performance for the photodegradation of MO solution, and they showed good stability and better photocatalytic activity than P25 photocatalyst. 相似文献
145.
Research on Computing Models of CBR Similarity 总被引:2,自引:0,他引:2
NIUXiao-tai MENGBo PENGDing-zhi 《武汉大学学报:自然科学英文版》2004,9(4):407-410
Several models of measuring case similarity in CBR systems are deeply explored. We also discuss the case matching process, and present three matching functions. Finally, we illustrate the significance of the models in CBR(Case Based Reasoning) systems implementation. 相似文献
146.
高温固相法合成Sr3 SiO5:Eu2+过程中,杂质相Sr2 SiO4:Eu2+的存在会不同程度影响Sr3 SiO5:Eu2+的光致发光性能及余辉性能。本文通过压片烧结和燃烧法两种方法制备Sr3 SiO5:Eu2+,结合热重-差热分析和X射线衍射分析,研究了Sr3 SiO5:Eu2+在合成过程中的相变化规律以及动力学过程。研究表明:原料与坩埚的接触处形成的界面以及原料在升温过程经过Sr2 SiO4:Eu2+的合成温度区间是导致杂质相产生的主要原因。在升温过程中,当温度经过1200℃左右的温度区间时,由于原料与坩埚接触处可以看作是两组不同物质的分界面,Sr2 SiO4:Eu2+的合成首先在该分界面处合成,而更多的原料需要扩散通过生成物层才能进一步反应;但随着温度的升高,原料随后进入Sr3 SiO5:Eu2+的合成过程,从而导致了Sr2 SiO4:Eu2+杂质相的生成。 相似文献
147.
提出了一种MOS器件失配时开关电流镜的简单模型,对开关电流(SI)非理想通用积分器进行了时域分析,以及积分器转移函数误差、Q值及灵敏度的计算,并与开关电容(SC)原型做比较,文中还以SI非理想通用积分器模型为基块,导出了器件失配时双二次滤波电路的直流失调电流和转移函数表达式,为研究器件失配对SI滤波器的影响提供了一条有效的途径。 相似文献
148.
邱伟德 《上海大学学报(自然科学版)》1998,4(2):126-132
设L是码,L=L1∪L2,L1∩L2=,L1≠,L2≠,我们定义码L的n次部分幂L(n)=Ln1∪Ln-11L2∪…L1L2∪L2并且与码的广义复合联系起来,得到了若干有趣性质.对于部分幂L(2)=L21∪L1L2∪L2,若|L1|=n,我们称L(2)是由Ln-部分生成.一个有限前缀码L(2)是n-素的,若L(2)不能由任一有限前缀码n-部分生成.若有限极大前缀码L(2)不是n-素的,则L(2)由唯一的一个n素极大前缀码以唯一的方式经有限次n-部分生成,因而我们能定义有限极大前缀码的n-秩,并由此对有限极大前缀作了分类.还证明L(n)在|L1|=1时是不可约的. 相似文献
149.
对粗糙脉孢霉双突变株arg-4,arg-13进行了紫外诱变,利用过滤富集法分离了不能利用乌氨酸,能利用瓜氨酸的3个突变株,利用互补针分离的约60个突变株分成了4个互补群,这可能代表4个独立的基因位点。 相似文献
150.
The effect of deep cryogenic treatment on the mechanical properties of 80CrMo12 5 tool steel was investigated. Moreover, the effects of stabilization (holding at room temperature for some periods before deep cryogenic treatment) and tempering before deep cryogenic treatment were studied. The results show that deep cryogenic treatment can eliminate the retained austenite, making a better carbide distribution and a higher carbide amount. As a result, a remarkable improvement in wear resistance of cryogenically treated specimens is observed. Moreover, the ultimate tensile strength increases, and the toughness of the sample decreases. It is also found that both stabilization and tempering before deep cryogenic treatment decrease the wear resistance, hardness, and carbides homogeneity compared to the deep cryogenically treated samples. It is concluded that deep cryogenic treatment should be performed without any delay on samples after quenching to reach the highest wear resistance and hardness. 相似文献