重庆地区4种不同蜜源原蜜的品质分析

【目的】了解重庆地区未加工原蜜的品质情况。【方法】对来自重庆地区的油菜(Brassica rapa var.oleifera)、五倍子(Rhus chinensis)、洋槐(Robinia pseudoacacia)、荆条(Vitex negundo var.heterophylla)等4种蜜源植物的9个原蜜样品进行了感官、理化、淀粉酶值、羟甲基糠醛(HMF)、微生物、农药残留等项目的检测。【结果】所有原蜜样品中:还原糖质量分数、酸度、淀粉酶值、HMF质量分数、细菌总数和农药残留均符合相关要求;水分质量分数均小于24%,属二级品;蔗糖质量分数均超过5%;霉菌和酵母计数均严重超标,其中酵母计数最高超标20倍。此外在南川油菜蜜的一个样品中检出微量甲萘威和涕灭威的残留。【结论】重庆地区的多种蜜源原蜜都存在水分、灰分及蔗糖质量分数较高,嗜渗酵母和霉菌超标,成熟度偏低等问题。
     

中文网络评论中的产品特征情感倾向提取算法研究

Web中的客户评论信息挖掘是大数据分析中的一项重要内容.分析客户评论中所包含的产品特征情感倾向,不仅可为消费者购买产品提供更具体的决策支持,还能有效帮助企业改进产品质量.针对商业应用的实际需要,提出了一种自动从中文客户评论中抽取产品特征并判断其情感倾向的方案.基于frequent pattern-tree (FP-tree)方法提取产品特征,结合基于语料库的方法和依存句法分析方法识别关于产品特征的主观评论语句、情感词及其情感词的依存关系,综合考虑情感词、否定词、程度词计算产品特征的情感倾向值.采用公开数据中的600篇手机评论作为实验数据,检验了算法的准确性.对比分析的结果说明,算法有很好的应用潜力,能够有效地从网络评论中获取有价值的商业信息.     

Al-Mg/Ti-Mg脱氧钢中夹杂物诱发点蚀行为研究

以不同脱氧方式熔炼的海洋工程用钢为研究对象,利用SEM、EDS及Image-Pro Plus 6.0软件对钢中夹杂物形貌、组成及尺寸分布等进行表征,通过3.5%NaCl溶液中阳极极化及腐蚀实验对钢中夹杂物诱发点蚀的行为进行探究。结果表明,与Al-Mg脱氧钢相比,Ti-Mg脱氧钢中形成了含有TiO_x的复合氧化物,夹杂数量更多且平均尺寸更小(小于1μm),有利于MnS的异质形核析出及弥散分布;低腐蚀活性的含TiOx复合氧化物及高度分散、异质局部析出MnS夹杂具有较低的点蚀敏感性及自腐蚀催化作用,降低了点蚀的诱发及扩展,有效提高了钢的抗点蚀性能。     

Reaction mechanism for in-situ β-SiAlON formation in Fe3Si-Si3N4-Al2O3 composites

In this work, Fe₃Si-Si₃N₄-Al₂O₃ composites were prepared at 1300℃ in an N₂ atmosphere using fused corundum and tabular alumina particles, Al₂O₃ fine powder, and ferrosilicon nitride (Fe₃Si-Si₃N₄) as raw materials and thermosetting phenolic resin as a binder. The effect of ferrosilicon nitride with different concentrations (0wt%, 5wt%, 10wt%, 15wt%, 20wt%, and 25wt%) on the properties of Fe₃Si-Si₃N₄-Al₂O₃ composites was investigated. The results show that the apparent porosity varies between 10.3% and 17.3%, the bulk density varies from 2.94 g/cm3 and 3.30 g/cm3, and the cold crushing strength ranges from 67 MPa to 93 MPa. Under the experimental conditions, ferrosilicon nitride, whose content decreases substantially, is unstable; part of the ferrosilicon nitride is converted into Fe₂C, whereas the remainder is retained, eventually forming the ferrosilicon alloy. Thermodynamic assessment of the Si₅AlON₇ indicated that the ferrosilicon alloy accelerated the reactions between Si₃N₄ and α-Al₂O₃ fine powder and that Si in the ferrosilicon alloy was nitrided directly, forming β-SiAlON simultaneously. In addition, fused corundum did not react directly with Si₃N₄ because of its low reactivity.     

《化工基础》课教学改革探讨

本文从高等师范院校化学专业的教学特点出发,通过理论分析并结合实际经验,对《化工基础》课的教学内容和教学方法、化工现场教学、考试形式三方面的改革进行了探讨,同时提出一些新的观点将之用于教学中并获得较大的成功。     

一种新的手写体汉字笔划提取方法

提出一种新的汉字结构特征提取方法．利用二维小波变换对汉字图像进行分析和处理,分别在其高频子图像中提取汉字的横、竖、撇和捺信息,使结构特征的提取比用其它方法更简单、明晰．     

Bi_2Sr_2CaCu_2O_x晶格振动模式的群论分析

利用群论分析方法对Bi_2Sr_2CaCu_2O_(?)正交晶系简正模进行了详细分析,预测了该超导体系的红外吸收峰和拉曼吸收峰的数目,为在实验上晶格振动光谱分析提供了理论依据.     

熏烤肉制品卫生安全性及其绿色产品开发的技术关键

熏烤肉制品是深受消费者喜爱的风味地方特产,但苯并芘等的污染残留是影响产品达到绿色标准的主要制约因素.研究表明,以严格控制原辅料质量及加工卫生管理为前提,通过对传统工艺的优化和改进,完全可能有效控制这一有害成分的残留.本文对熏烤肉制品卫生安全性及其绿色产品开发的技术关键进行了探讨.     

一类不确定性Lurie控制系统的鲁棒绝对稳定的新判据

针对一类具有范数有界不确定性系统,利用Lyapunov函数方法,结合矩阵不等式技巧,给出了系统基于线性矩阵不等式（LMI）的鲁棒绝对稳定性判别条件,并通过算例给予了验证．     

One-step and high-density protein immobilization on epoxysilane-modified silica nanoparticles

Silica nanoparticles are most commonly modified with amino-silanes, followed by post-modification activation for protein immobilization. In this work, epoxy-functionalized silica nanoparticles were prepared by modification with glycidyloxypropyl trimethoxysilane （GPTMS） for direct protein immobilization. Silica nanoparticles possessed an average size of 46 nm, but increased to 63 nm after GPTMS modification. Reaction time, reaction temperature and GPTMS content had no significant effect on par- ticle size. Zeta potential of SiO2 changed from -26mV to ＋38mV after modification. Fourier-transformed infrared spectroscopy revealed alkyl C--H bending and stretching bands at 2944 cm-1, 1343 cm-1 and 1465 cm-1, respectively, for the modified nanoparticles. Fluorescein cadaverine was found to bind to GPTMS-modified SiO2, but not to bare SiO2, indicating the chemical reactivity of epoxy groups on the modified nanoparticle with amines. Finally, fluorescenUy labeled bovine serum albumin （BSA） was used as a model protein to investigate the capacity of epoxy-SiO2 nanoparticles for protein immobilization. The results showed that more proteins were immobilized on the particle with longer reaction time, higher NaCI concentration, lower pH, and less GPTMS content. More importantly, proteins bound to epoxy-SiO2 nanoparticle were highly stable. Under optimized reaction conditions, as much as 25 mg BSA/g nanoparticle was covalentiy attached to the nanoparticle. The epoxy silane modification of silica nanoparticles offers a reactive surface for one-step and high-density protein immobilization.