基于粒子追踪的风场可视化方法

为了更直观地表示三维风场的变化特点，针对气象风场数据集的特点采用粒子系统的方法可视化表示风场属性，提出了通过粒子的位置变化动态反映风场速度方向以及大小，同时将风场涡旋度的强弱映射成粒子本身的旋转状态，最后选取CDC数据中心的风场数据验证了实验结果。     

利用体系结构的建模方法支持测试设计的重用

将体系结构的建模方法应用于测试设计,测试设计和软件设计自上至下同步进行.利用基于体系结构的建模方法将软件设计规范和测试设计规范紧密结合,形成统一的模型描述框架,从而构建层次化的测试设计模型,同时给出了测试用例之间关系的精确定义.结论是:基于体系结构的建模方法能够大大提高软件开发过程中各工作产品的可测试性和测试用例的可维护性,能够有效地支持测试设计的重用.     

新的f(R)黑洞

f（R）引力是一个直接拓展广义相对论的修正引力理论,它的拉格朗日量是一个仅含曲率标量R的任意函数f（R）.在F（r）=1+αr的条件下（F（r）≡（df（R（r）））/（dr）和αr是一个对广义相对论小的修正量）,导出了度规f（R）引力理论中场方程的精确球对称真空解.此外,考虑了这个黑洞背景时空中的标量场扰动.用六阶WKB （Wentzel-Kramers-Brillouin）方法,讨论了拟正则模和这个黑洞的参数之间的关系,得出这个黑洞是稳定的结论.     

基于梯度的帧内自适应深度决策算法

提出了一种基于梯度的帧内候选模式裁剪算法,通过自适应深度划分并利用空间信息来简化帧内预测过程,大大减少了计算复杂度.实验结果显示,所提出的算法对比HM16.7,可以减少35.25%的计算复杂度,且只有极小的编码效率损失.     

叶酸修饰聚酰胺-胺负载5-氟尿嘧啶纳米给药体系的制备及其体外性能研究

使用化学键键合的方式分别将叶酸(FA)和5-氟尿嘧啶-1-基乙酸(FUA)偶联于树状大分子聚酰胺-胺(PAMAM)制备纳米载药体系FA-PAMAM-FUA,并结合单因素分析法筛选出最佳制备条件为FA∶PAMAM∶FUA的物质的量的比为10∶1∶450,p H值为6.用紫外可见光谱、红外光谱和纳米粒度仪对FA-PAMAM-FUA的光学特性、粒径大小和体外释药性能进行了表征.结果表明:优化条件下制备的FAPAMAM-FUA粒径呈正态分布,平均粒径为90.28±20.00 nm,分散度为0.258±0.002(n=3),体系载药量达28.45%,FA-PAMAM-FUA给药体系对药物具有一定的p H敏感特性以及缓释功能.采用MTT法考察了5-Fu、FA-PAMAM-FUA对乳腺癌细胞MCF-7的增殖抑制作用,结果表明两者对MCF-7细胞的增殖具有明显地抑制作用,剂量依赖性强,随浓度的增高,FA-PAMAM-FUA对癌细胞增殖抑制作用较5-Fu明显增强.     

潮汕牛肉丸煮制前后关键性香气成分对比分析

采用固相微萃取(solid-phase microextraction, SPME)结合气相色谱-嗅闻-质谱联用技术(gas chromatography-olfactometry-mass spectrometry, GC-O-MS)分析潮汕牛肉丸煮制前后挥发性香气活性物质,同时结合香气活性值(odor activity value, OAV)确定关键性香气活性成分。结果表明,在煮制前后牛肉丸中共鉴定出42种挥发性成分,包括含硫化合物11种,醛类7种,杂环化类4种,醇类4种,烃类10种,酯类2种,酮类1种,酚类2种,酸类1种;嗅闻鉴定出12种香气活性物质,经OAV分析确认生牛肉丸中的关键性香气成分是二烯丙基硫醚、二烯丙基二硫醚、甲基烯丙基硫醚、反式-2-辛烯醛、己醛、壬醛;熟牛肉丸的关键性香气成分是二烯丙基硫醚、己醛、壬醛、二烯丙基二硫醚。比较关键性香气物质OAV的前后变化,发现二烯丙基硫醚、甲基烯丙基硫醚、二烯丙基二硫醚、甲基烯丙基二硫醚、反式-2-辛烯醛、己醛是导致潮汕牛肉丸煮制风味变化的关键性香气成分。     

Shear-thickening behavior of Fe-ZSM5 zeolite slurry and its removal with alumina/boehmites

A cryogenic scanning electron microscopy (cryo-SEM) technique was used to explore the shear-thickening behavior of Fe-ZSM5 zeolite pastes and to discover its underlying mechanism. Bare Fe-ZSM5 zeolite samples were found to contain agglomerations, which may break the flow of the pastes and cause shear-thickening behaviors. However, the shear-thickening behaviors can be eliminated by the addition of halloysite and various boehmites because of improved particle packing. Furthermore, compared with pure Fe-ZSM5 zeolite samples and its composite samples with halloysite, the samples with boehmite (Pural SB or Disperal) additions exhibited network structures in their cryo-SEM images; these structures could facilitate the storage and release of flow water, smooth paste flow, and avoid shear-thickening. By contrast, another boehmite (Versal 250) formed agglomerations rather than network structures after being added to the Fe-ZSM5 zeolite paste and resulted in shear-thickening behavior. Consequently, the results suggest that these network structures play key roles in eliminating the shear-thickening behavior.     

TTAC-HPMo/SiO_2催化剂的表征及其氧化脱硫性能分析

以十四烷基三甲基氯化铵(TTAC)为模板剂,正硅酸乙酯(TEOS)为硅源,采用溶胶-凝胶法制备TTAC-HPMo/SiO_2催化剂,利用FTIR、XRD、SEM和N_2吸附-脱附等技术对其进行表征,并分析催化剂制备条件和反应条件对模型油氧化脱硫性能的影响。结果表明,在m(HPMo)/m(SiO_2)=15%、焙烧温度为400℃条件下所制TTAC-HPMo/SiO_2催化剂,其孔隙结构发达、氧化脱硫性能最佳;对于10mL以二苯并噻吩(DBT)为目标含硫化合物的模型油(硫含量为400μg/g),当m(TTAC-HPMo/SiO_2)/m(模型油)=0.43%、V(H_2O_2)/V(模型油)=0.2%、反应温度为60℃、反应时间为14min时,所制TTAC-HPMo/SiO_2催化剂对模型油中DBT的脱除率达到100%。     

WO3 nanoflakes decorated with CuO clusters for enhanced photoelectrochemical water splitting

The low quantum efficiency arising from poor charges transfer and insufficient light absorption is one of the critical challenges toward achieving highly efficient water splitting in photoelectrochemical cells. Three dimensions(3D) structures and heterojunctions have received intensive research interests recent years due to their excellent ability to separate photo-generated charges as well as the enhanced light harvesting property. Herein,3 D Cu O/WO_3 structure was fabricated through a facile solvothermal method followed by chemical bath deposition. The loading of Cu O clusters on WO_3 nanoflake arrays results in a much improved photocurrent density compared with that of pristine WO_3 nanoflake arrays, which reaches 1.8 m A/cm2 at 1.23 V vs. the reversible hydrogen electrode. The electrochemical impedance spectroscopy measurement demonstrates that the improved performance of Cu O/WO_3 electrode is attributed to the accelerated charge transfer kinetics as a result of the desirable band alignment in Cu O/WO_3 heterojunction. This work demonstrates a facile strategy to construct superior WO_3 electrode, which will ultimately allow for efficient storage of solar energy into hydrogen.     

不同株系丹参有效成分比较研究

为比较不同株系之间丹参有效成分的差异,采用高效液相色谱法测定丹参中包括丹参酮ⅡA在内的4种脂溶性成分和包括丹酚酸B在内的3种水溶性成分的含量,并应用SPSS软件对所得数据进行分析。通过对两大类成分的比较,发现10种株系丹参中,3、7号株系的脂溶性成分含量较高,可考虑培育为脂溶性成分提取原料;而1、9、10号株系的水溶性成分较高,可考虑培育为水溶性成分提取原料。显著性分析结果表明,所测10种不同株系丹参在其主要水溶性和脂溶性成分上存在显著差异。该研究可以为丹参优良种质的筛选提供依据。