啤酒酵母原生质体融合株HN31-6的啤酒酿造中试研究

为了考察啤酒酵母融合株HN31-6的啤酒酿造生产性能,以12.5°Bx麦芽汁为培养基,用500 L发酵罐在12℃下发酵,发酵期间每天取样测定发酵液的发酵度和酒精度以及发酵液的双乙酰、乙醛、高级醇和酯类等挥发性物质的含量.结果表明:在上述条件下,发酵14 d,发酵液的发酵度和酒精度分别为69.9%和4.46%;双乙酰和乙醛的含量分别为0.036 4 mg/L和4.53 mg/L;异戊醇、异丁醇和正丙醇的含量分别为46.47、8.34和9.82 mg/L,总高级醇的含量为64.6mg/L;甲酸乙酯、乙酸乙酯、乙酸异丁酯、乙酸异戊酯和己酸乙酯的含量分别为0.132、21.92、0.037、2.22和0.293 mg/L,总酯为24.6 mg/L;该菌株的发酵度以及发酵液的酒精、双乙酰、乙醛、总高级醇和一些酯类等的含量均达到国家优质啤酒的标准,啤酒口感良好.该融合株在啤酒酿造生产中具有很好的应用前景.     

基于ECA规则的计算机联锁故障诊断系统研究设计

分析计算机联锁故障诊断系统的主动性需求,结合数据库在计算机联锁故障诊断系统中的作用,提出基于主动数据库的系统设计.对主动规则的原理和执行进行分析,给出基于主动规则-ECA的故障诊断系统的设计和运行机制.并运用ECA规则,以定时服务与数据更新和系统故障告警两事件动作为例进行设计.     

Synthesis and anticonvulsant activity of 1-substituted benzyl-N-substituted-1,2,3-triazole-4-formamides

Substituted benzyl azids were synthesized through the reaction of substituted benzyl chloride and sodium azid，which subsequently underwent cyclization with ethyl propiolate and amidation to give thirteen 1-substituted benzyl-N-substituted-1,2,3-triazole-4-formamide derivatives (3a-3m). The structure of the synthesized compounds was confirmed by IR, H-NMR, MS and elemental analysis. Their anticonvulsant activity against maximal electrolshock (MES) induced seizure was tested and the result showed that all these compounds possess anticonvulsant activity in different degrees. Among those, the compounds containing chloro atoms on the phenyl ring were less potent in anticonvulsant activity, while introducing one or two fluorin atoms on benzyl system increased its activity. Furthermore, their activity decreased when there was substituent on the nitrogen atom of carboxamide, and the larger the substituent, the lower the activity.     

Geochemical characteristics of Jurassic coal and significance for the evolution of the environment, Yanqi Basin, China

The Mesozoic strata of the Yanqi Basin consists of coarse debris with coal beds, characterized by the developments of coal seams of the Jurassic sediments whose main petrologic contents are glutenite, fine sandstone, mudstone, carbonaceous shale and coal. Based on the analyses of the minerals, trace elements and REEs, we try to find geochemical characteristics of the coal seam formation process. The analysis results indicate that the contents of ash and sulfur are low while the content of phosphor is comparatively high, and that the specific value of Al2O3/SiO2 is relatively high and that of （Al2O3+SiO2）／（Fe2O3+CaO+MgO） is near 1. All these results indicate that the coal seams are formed in the relatively deep marsh, which is favorable for the evolvement of hydrocarbon at the diagenesis stage.     

改性B72文物保护材料耐光老化性能研究

目的研究改性后的B72(Paraloid B72)文物保护材料的耐光老化性能。方法采用紫外线吸收剂UV326对目前广泛使用的文物保护材料B72进行改性。通过傅立叶变换红外光谱、反射光谱、光失重来表征改性材料的耐光老化性能。结果在光老化过程中,B72材料比UV326紫外线吸收剂改性B72材料的红外光谱曲线变化更快,特别是羰基和酯基谱带强度减小更明显。改性材料能够有效阻止B72变黄,并且实现对基质材料和壁画的保护作用。改性B72比纯B72有更好的耐光老化性能。结论光老化过程对材料表面的亮度改变不大,而B72材料泛黄程度远大于UV326改性B72。改性B72材料比原材料的耐光老化性能有了明显改善,是一种大有潜力的文物保护材料。     

Distributed Fault Detection for Consensus in Second-Order Discrete-Time Multi-agent Systems with Adversary

This paper is concerned with distributed fault detection of second-order discrete-time multi-agent systems with adversary,where the adversary is regarded as a slowly time-varying signal.Firstly,a novel intrusion detection scheme based on the theory of unknown input observability（ UIO） is proposed. By constructing a bank of UIO,the states of the malicious agents can be directly estimated. Secondly,the faulty-node-removal algorithm is provided.Simulations are also provided to demonstrate the effectiveness of the theoretical results.     

Molecularly Imprinted Polymer Based on GO-QDs as Enhanced Fluorescent Nanoscale Device for Specific Recognition of Target Protein

In this work the enhanced molecularly imprinted optosensing material based on graphene oxide-quantum dots （ GO- QDs） was synthesized for highly selective and sensitive specific recognition of the target protein, bovine serum albumin （BSA）. Here, GO was introduced to enhance the efficiency of mass-transfer in recognition of target protein. Molecularly imprinted polymer coated GO-QDs using BSA as template （BMIP-coated GO-QDs ） exhibited a fast mass-transfer speed, which could be ascribed to the high volume of efficient surface area and high target recognition efficiency of the synthesized nanoscale device. Under optimal conditions, it was found that the BSA as target protein could remarkably quench the relative fluorescence intensity of BMIP- coated GO-QDs linearly in a concentration-dependent manner that was best described by a Stern-Volmer equation. The Ksv （Stern- Volmer constant） for template BSA was much higher than bovine hemoglobin （BHb） and lysozyme （Lyz）, implying a highly selective recognition ability of the BMIP-coated GO-QDs to BSA. This enhanced fluorescent nanoscale device may provide opportunities to develop a system that is efficient and effective and has potential in the design of highly effective fluorescent receptor for recognition of target protein in Droteomics studies.     

基于PCA和PSO-SVM在葡萄酒分类中的应用研究

针对葡萄酒的物理化学成分冗余数据,提出了一种基于主成分分析(PCA)和粒子群优化—支持向量机(PSO-SVM)的模型用于葡萄酒的分类.首先,对葡萄酒的物理化学成分进行主成分分析,提取主要影响因素,减少输入维数,再利用粒子群优算法寻找支持向量机的最佳参数,并用支持向量机完成对训练集样本的学习和测试集样本的预测分类.结果表明,该模型与其他模型相比较,具有较高的准确性,有一定的适用价值.     

汽车尾气余热热电转换装置设计与初期试验

为有效利用汽车尾气中的废热以提高其燃油经济性,构建了汽车尾气余热热电转换台架试验装置,通过初期试验分析了在汽车发动机不同转速下分流器对出口尾气温度的影响因素,并测试了不同气体流场结构下的集热器表面温度分布情况和热电转换模块的输出性能.结果表明,分流器在尾气热传输方面构成了很大的热阻,延长尾气在集热器内部的流动时间和路径可以有效提高其表面温度和热电转换装置的输出能力,采用蛇形流道结构的集热器表面温度分布比空腔结构更加均匀.结合初期试验结果和实际经验提出了系统设计与集成的改进措施,对今后的进一步研究工作有一定指导意义.     

高压绝缘子串电压分布及其表面温升的理论研究

高压绝缘子电阻劣化发热和表面污秽发热均与绝缘子串的电压分布有关,研究绝缘子串的电压分布以及与表面温升的关系,无论是对工程设计还是对实际检测都非常重要.利用绝缘子等值电路模型,在理论上讨论了高压绝缘子串的电压分布及其影响因素,以及绝缘子串的电压分布与绝缘子表面温升之间的对应关系,所得的结论对绝缘子故障的红外热像检测诊断具有一定的指导意义.