pH、温度和浓度对苯酚在V掺杂MoOx-C/Ti电极上的电催化氧化的影响

采用溶胶-凝胶法合成MoOx、MoOx-V5 (x%)胶体,通过Vulcan XC-72炭黑负载制备炭载钼系氧化物电催化剂.利用循环伏安法(CV)测试手段研究苯酚在电极上的氧化降解,考察了掺杂元素、溶液pH值、苯酚浓度、扫描速率、温度对苯酚氧化性能的影响.测试结果表明:苯酚在电极上的氧化是受扩散和电子转移联合控制的复杂过程;掺杂过渡金属元素V可以降低苯酚氧化的表观活化能,提高电化学性能;溶液的pH值越低,MoOx-C/Ti电极对苯酚的催化氧化活性越高;pH在0～6,苯酚的氧化经历了相似的历程,包含了相同的电子数和质子数;苯酚氧化峰电流随着浓度、温度的增加而增加,到一定程度后趋于稳定.     

早产合并胎膜早破96例分析

目的 :探讨早产合并胎膜早破的处理方法 ,减少围生儿死亡。方法 :对96例确诊为早产合并胎膜早破的产妇进行回顾性分析。结果 :未保胎51例 ,保胎45例 ,21例保胎成功 ,占46 7%。围生儿情况 :孕周≤34w 6 者 ,围生儿死亡率高于孕周>35周者 ,围生儿窒息率孕周≤34w 6者高于孕周>35w者。结论 :恰当处理早产合并胎膜早破是减少围生儿窒息和死亡的关键     

师范院校体育教育专业篮球普修课教学改革的思考

通过对师范院校体育教育专业篮球教学目标、教学内容、教学模式、课的结构及对学生的学业成绩评价进行分析和思考 ,提出了当今篮球教学中存在的问题及其解决方法。     

用钼蓝反应动力学方法作微量磷的分光光度测定

提出用ｄ－葡萄糖试剂做钼蓝反应的还原剂测定磷的动力学方法。用吸光度监测反应速度，用假一级反应的关系式测定了反应速度与磷浓度的线性范围为０．６～２．５μｇ／ｍＬ。用内标法计算五种土壤样品中的含磷量，分析结果与常规方法比较，符合程度令人满意。     

三峡二期围堰工程几个问题的研究及实践

三峡工程二期围堰是三峡工程最重要的临时建筑物之一，大江截流水深大，流量大；防渗墙深度大，工程量大，工期紧，且还要穿过各种复杂地层，通过试验，研究，采取有效地对策确保大江安全，顺利截流，基坑按三峡总工期目标要求抽干，检查渗漏量仅为设计估计量的1／10。     

网络教学中的预测分析

阐述了开发网络教学系统的系统构成及开发工具,在此基础上提出了基于Web技术的辅助教学系统及预测分析模块,介绍了预测分析模块的工作原理及其构成预测分析模块的量化数据的来源,包括课程资源、讨论答疑、作业提交、测验考试资源等.另外,综述了预测分析的功能特色,应用效果,以及网络教学评价前景和发展.     

Analysis of Pyrolysates for Phenol Formaldehyde Resin by Py-GC/MS

Pyrolysis of phenol formaldehyde resin has been investigated by Pyrolysis Gas Chromatography-Mass Spectroscopy at the different temperatures from 500℃ to 750℃. Its composition of pyrclysates has been analyzed. Several compounds, especially benzene, toluene, p-xylene could only be formed above 500-550℃. Howerver, peak intensities for some pbend derivatives were decreased at the higher temperature. During pyrolysis, for thermo-setting phenol formaldehyde resins, polymeric chain scissions take place as a successive removal of the monomer units from the polymeric chain. The chain scissions are followed by secondary reactions, which leads to a variety of compounds. Addition reactions can also take place among the double-bond compounds during pyrolysis.     

Intramammary expression and therapeutic effect of a human lysozyme-expressing vector for treating bovine mastitis

To develop a gene therapy strategy for treating bovine mastitis, a new mammary-specific vector containing human lysozyme (hLYZ) cDNA and kanamycin resistance gene was constructed for intramammary expression and clinical studies. After one time acupuncture or intracisternal infusion of healthy cows with 400 μg of the p215C3LYZ vector, over 2.0 μg/ml of rhLYZ could be detected by enzymatic assay for about 3 weeks in the milk samples. Western blotting showed that rhLYZ secreted into milk samples from the vector-injected cows had molecular weight similar to that of the natural hLYZ in human colostrums. Twenty days after the primary injection, the quarters were re-injected with the same vector by quarter acupuncture and even higher concentrations of rhLYZ could be detected. Indirect competitive ELISA of milk samples showed that the vector injection did not induce detectable humoral immune response against hLYZ. Clinical studies showed that twice acupuncture of quarters with the p215C3LYZ vector had overt therapeutic effect on clinical and subclinical mastitis previously treated with antibiotics, including disappearance of clinical symptoms and relatively high microbiological cure rates. These data provide a solid rationale for using the vector to develop gene therapy for treating bovine mastitis.     

双馈电机运行速度对稳态性能的影响

研究双馈电机运行速度对双馈电机稳态性能的影响．首先对比了双馈电机运行于超同步转速及次同步转速时的稳态波形，然后对谐波及稳态参数的变化进行了分析．研究表明双馈电机稳态运行速度对其稳态运行性能有较大影响．     

Metamorphic Algorithm of Self-reconfigurable Modular Robotic System

Introduction Aself reconfigurableroboticsystemconsistsofman simpleidenticalmechatronicmodules.Thesemodulesca connectanddisconnectfromonetoanothertochangethe overalltopology.Thesystemcanautonomouslyandynamicallyadaptitsshapetosuittheneedsofthetask hand,e.g.manipulation,locomotion,andcreationo staticstructures.Thegeneralphilosophyofsel reconfigurableroboticsystemistosimplifythedesignanreducemanufacturingcostandenhancefunctionalityan versatilitythroughalargernumberofidenticalmodules.I addition…