西洋参总皂苷碱降解产物的分离及结构鉴定

从西洋参总皂苷碱降解产物中分离得到了5种化合物，经理化方法鉴定为人参皂苷Rh1（1），人参皂苷Rh2（2），人参皂苷Rk2（3），达玛烷型-20（21），24-二烯-3β，12β-二醇（4），人参皂苷Rg3（5）；本研究同时还提供了化合物更多的理化数据．化合物3、4为首次从碱降解物中获得．     

大学生心理健康问题探讨

通过揭示近年来由大学生心理问题引发的令人触目惊心的事实，结合权威数据，分析了大学生心理健康问题，提出了大学生心理健康教育的几点建议，旨在找到大学生思想问题的根源，加强和改进大学生心理健康教育质量。     

分布式无线通信系统中STBC和V-BLAST的组合方案

在分布式天线分簇放置的单用户分布式无线通信系统中,为了有效地实现下行分集与复用的折中,提出了一种空时分组码(space-time block code,STBC)和垂直分层发送方案(vertical bell-labs layered space time,V-BLAST)的组合方案。在发送端根据反馈的发送相关矩阵的特征值,提出了天线选择和功率、速率分配的方案,使得系统误符号率(symbol error rate,SER)的上界最小。仿真结果表明:不同方案实际SER性能之间的关系和通过SER上界得到的关系完全一致。该方案简化了下行发送方案的设计,适合于实际应用。     

阴、阳离子聚合物交替注入用于注聚区封窜和调剖

胜利孤岛油田注聚区块过早见聚,为封堵聚合物从油井窜流产出和调整注聚剖面,研制出阳离子调剖剂NCP。室内试验结果表明,向用1000mg/L的HPAM驱油后的岩心中注入1.5×10~4～3.0×104mg/L的NCP1.0PV,在70℃恒温24h后的堵油率大于96％,突破压力梯度2.6～3.3MPa/m。注入2.0×10~4mg/L NCP溶液的岩心,连续注入50PV含800mg/LHPAM的地层水,水相渗透率持续下降;在岩心试验中,堵水率随NCP浓度的增大而增大。结果表明:NCP可用于注聚区块调整注聚剖面,在孤岛注聚区进行的5井次封窜试验中,3口井收到良好效果。     

Tracking data management using topology of moving object database system for moving object constrained trajectory in LBS application

Advances in wireless technologies and positioning technologies and spread of wireless devices, an interest in LBS (Location Based Service) is arising. To provide location based service, tracking data should have been stored in moving object database management system (called MODBMS) with proper policies and managed efficiently. So the methods which acquire the location information at regular time intervals then, store and manage have been studied. In this paper, we suggest tracking data management techniques using topology that is corresponding to the moving path of moving object. In our techniques, we update the MODBMS when moving object arrived at a street intersection or a curved road which is represented as the node in topology and predict the location at past and future with attribute of topology and linear function. In this technique, location data that are corresponding to the node in topology are stored, thus reduce the number of update and amount of data. Also in case predicting the location,because topology are used as well as existing location information, accuracy for prediction is increased than applying linear function or spline function.     

钨合金弹体超高速撞击混凝土靶成坑特性研究

为探究钨合金弹体超高速撞击混凝土靶的成坑直径和成坑体积随动能变化的规律,采用二级轻气炮开展了钨合金弹体以1。97～3。66km/s的速度撞击混凝土靶实验,利用CT图像诊断方法得到了实验后的成坑特性实验数据,并基于点源假设进行了超高速撞击条件下成坑特性的量纲归—化分析。结果表明:超高速撞击条件下靶板成坑为“弹坑+弹洞”型;成坑直径和成坑体积随动能增加而单调递增,通过量纲分析得到成坑直径3次方和成坑体积都与弹体动能近似成正比,拟合指数μ接近动能主导的指数2/3,说明成坑过程主要受动能影响。      

新型抗高温耐盐起泡剂AGS合成与性能研究

采用环氧氯丙烷在TTA路易斯酸催化作用下分别与正辛醇、正癸醇和正十二醇发生开环反应,然后在碱性条件下闭环,最后与亚硫酸氢钠在高温条件下发生磺化反应的三步法,合成出一系列烷基甘油基醚磺酸钠（AGS）表面活性剂AGS-12,AGS-10和AGS-8,并利用红外光谱对其结构进行分析,测定其Krafft点,评价AGS作为起泡剂的抗高温性能以及盐和油类物质对其泡沫性能的影响。结果表明,AGS表面活性剂可耐250℃高温,无论是在5％NaCl或5g／L Ca2＋的盐水溶液中,还是在15％柴油或原油的高含油溶液中都具有良好的泡沫性能。     

冷家稠油黏温特性及流变特性实验研究

应用回归分析理论,开展现场取样、室内测量实验,建立数学模型,对辽河油田冷家稠油黏温特性及流变特征进行分析,得到稠油黏度关于温度、剪切速率的二元函数,回归出剪切应力与剪切速率、屈服应力值与温度、表观黏度与剪切速率的关系曲线。研究认为,冷家稠油随着温度升高、剪切速率的增大,黏度降低;临界温度Tc=72.51℃是牛顿流与非牛顿流的转变点;温度从40℃上升到70℃时,屈服应力值随着温度的升高而呈线性递减,当温度达到Tc时,屈服应力值就变为零;在非常低的剪切速率范围内,黏度下降最快,在高剪切速率情况下,黏度近似于不变。     

Extraction and DNA Digestion of 5'-Phosphodiesterase from Malt Root

This study investigated the extraction of 5'-phosphodiesterase from malt root and the degradation of nucleic acids by this enzyme.The extraction used grade precipitation with ammonium sulfate and enzy-matic hydrolysis.Samples were assayed using the modified Bradford method and high performance liquid chromatography.The results show that 5'-phosphodiesterase is isolated by grade precipitation with 30% and 80% saturation of ammonium sulfate and can be utilized to degrade deoxydbonucleic acid.The hydrolysate has four kinds of deoxynucleotides: 5'-dCMP,5'-dTMP,5'-dAMP,and 5'-dGMP.The optimum reaction tem-perature is 70℃,and the optimum pH is 5.5-6.0 for the reaction.The percentage of deoxynucleotides indi-ceted by the China Pharmacopoeia (2000 edition) in the product is over 70%.The extraction of 5'-phosphodiesterase from malt root is shown to be possible and economical.Products from the enzymatic hydrolysate of DNA meet the pharmacopoeia.     

MgSO4对2-酮基-L-古龙酸发酵影响的实验研究

通过摇瓶实验和2 L搅拌釜式发酵罐实验,研究了发酵培养基中初始MgSO4浓度对维生素C前体2-酮基-L-古龙酸(2-KGA)发酵过程的影响.实验结果表明:2-KGA发酵的最佳MgSO4初始浓度w0≈0.084%,在这一浓度下,产物2-KGA的得率和容积生产率均达到峰值;MgSO4初始浓度过高将降低产物得率和容积生产率.