三维超分子化合物[CuⅠ(en)2][PW2Ⅴ W10ⅥO39](Hen)2·2H2O的合成与表征

采用水热合成法制备了三维超分子化合物[CuⅠ(en)2][PW2Ⅴ W10ⅥO39](Hen)2·2H2O(en为乙二胺).通过元素分析、红外光谱和X射线单晶衍射确定了化合物的组成和晶体结构.结果表明:晶体属于三斜晶系,P-1空间群;晶胞参数a=1.090 91(9)nm,b=1.162 57(10)nm,c=1.943 43(15)nm,α=81.38°,β=84.47°,γ=65.29°,V=2.212 2(3)m3,Z=2,R1=0.080 4,ωR2=0.200 3.标题化合物由1个α-Keggin型杂多阴离子单元、1个[Cu(en)2] 配阳离子、2个质子化的en分子和2个结晶水构成.多阴离子单元通过共用端氧的方式形成无限延展的一维链,一维链通过复杂的氢键网络堆积成具有哑铃型孔道的三维有机-无机超分子化合物.     

No-Wait流水车间调度问题的MDIS算法研究

No-Wait流水车间调度问题的特性是工件加工一旦开始,必须连续进行,不允许工件完成某一加工工序后在机器上滞留等待.本文针对目标函数为Makespan的No-Wait流水车间调度问题,从对目标函数结构的分析入手,提出了一种基于最小化工件间距离的初始排序策略和插入方法的启发式算法.通过对大量典型算例的实验后验证了提出的算法的有效性.     

基于信息扩散和BP网络的黄土边坡稳定性分析

目的探讨基于信息扩散原理的BP神经网络的黄土边坡稳定性评价模型。方法收集黄土地区24组黄土边坡实例,采用模糊信息优化处理中的信息扩散原理,建立各评价因子与安全系数之间的模糊关系,并在此基础上建立与BP神经网络相结合的评价模型。结果建立的评价模型对4组预测样本的预测结果,效果良好,较好地解决了样本过少或含有矛盾样本的问题。结论该模型在黄土边坡稳定性评价中比普通神经网络具有更高的实用性和有效性。     

Efficient transformation and expression of gfp gene in the edible mushroom Pleurotus nebrodensis

An efficient transformation method mediated by PEG-protoplasts was developed for the newly commercial edible mushroom Pleurotus nebrodensis. Two plasmids were used to co-transform protoplasts of P. nebrodensis. One plasmid is pAN7-1 containing a positive selectable marker gene hph conferring hygromycin B resistance. Another plasmid is pBlue-GFP containing a reporter gene gfp conferring green fluorescent protein. PCR and Southern blot analysis showed that hph gene or/and gfp gene were integrated into the genome of P. nebrodensis transformants. The transformation efficiency of the positive selectable marker gene hph was 3 transformants per microgram of plasmid pAN7-1 DNA, which was about 30 times higher than that previously reported in thoroughly studied Pleurotus species such as Pleurotus ostreatus. The transformation efficiency of the reporter gene gfp was 9 transformants per microgram of plasmid pBlu-GFP DNA. The co-transformation efficiency was 23.68%. This is the first report that a ＂reporter＂ gene, green fluorescent protein gene can be successfully stably exoressed in this Pleurotus species.     

“依然”与“仍然”的比较分析

本文在大规模语料的基础上,比较分析现代汉语副词"依然"与"仍然"在句法特征、句式语义和固定格式上的差异。通过分析认为:在句法上,两者都能做状语,而"依然"还可以做谓语;做状语时在大多数情况下两者可以替换。在语义和格式上,"依然"侧重于对静态持续态的修饰,有成词的固定格式;"仍然"可以表动作的间隔重复,并具有更重的转折意味。     

Recent progress in studies on the nano-sized particle layer in rock shear planes

Since the 1990s, an ultramicro-particle texture in nano- or micron-sized scale has been continually found in shear planes of various rocks, and recently further progress was obtained by studying the generic mechanisms on both physics and mechanics. In this article, the characteristics of the nano-sized particle layer in rock shear planes (including the widespread distribution, layering texture, non-linear genetic mechanism, and multiple functions) on an ultra micro-scale were briefly introduced and more information was proposed by analyzing examples from home and broad.We found that there is a paragenetic relationship between the development of shear frictional-viscous and the formation of nano-sized particles and that in the shear movement, partitioning, segregating, and layering in rocks are initiated by the sliding motion of the nano-sized particle layer. Moreover, the plastic rheology of rocks is essentially the movement of ultra micro-sized particle (nano-size and micro-size), and the nano-sized particle layer in rock shear planes are characterized by some particular physical and chemical effects.     

增光子相干态光场与二能级原子相互作用中的含时维格纳函数

利用相互作用表象中增光子相干态光场与二能级原子作用的系统动力学波函数,通过约化密度算符和维格纳函数福克基矢展开技术得到描述光场随时间演化的含时维格纳函数,并用数值模拟分析该维格纳函数随时间演化及随光场振幅变化的特点.模拟结果显示,在随时间演化时,维格纳函数的负值性在单光子过程中不具周期性,在双光子过程中具有周期性;在随光场振幅变化时,维格纳函数的负值性随光场振幅的增强而逐渐减弱,光场的非经典特性逐渐趋近于经典特性.     

基于向量空间模型的Web服务描述相似度计算的研究与实现

服务描述是服务发现的基础．现有的服务发现多从关键词入手进行匹配,本文给出了一种通过服务描述进行相似度计算的方法,采用了The Porter Stemming Algorithm对服务描述进行预处理,引进向量空间模型的方法对描述进行度量,对比实验证明,该方法能充分利用服务描述的特点来计算服务之间的匹配度,是有效的和可行的．     

腺病毒载体介导GFP基因在鸭胚和雏鸭体内的表达

本试验旨在探讨腺病毒在鸭胚和雏鸭体内的感染情况,为腺病毒作为外源基因载体在活体上进行RNA干涉奠定基础．将GFP基因重组腺病毒（Adv-GFP）静脉注射15日龄鸭胚和10日龄雏鸭,在感染后不N时间采集组织器官,制作冰冻切片,荧光显微镜观察GFP基因在鸭胚和雏鸭组织器官中的表达,结果发现,GFP基因在Adv-GFP感染后24-72h能在鸭胚肝脏及心肌细胞中表达,在感染后1-5d,GFP基因可在雏鸭肝脏、脾脏、腔上囊中稳定表达,本试验首次证明腺病毒作为安全的外源载体,可介导外源基因在鸭胚和雏鸭体内的靶器官中持续稳定表达,为在鸭上进行病毒病的基因治疗提供了基础数据．     

微型旋风器分离超细粉尘的性能

针对分级领域中存在的问题,研究微型旋风分级器的分级性能,目的是利用微型旋风分级器将1μm左右的超细粉体从细粉中分离出来.首先建立旋风分级器的分离二维数学模型,模型方程解析证实粉尘分级效率只与Stk数有关,对3种微型旋风器在不同进口风速下进行实验研究.实验结果表明:分级效率与Stk数之间的关系在Rosin-Rammler坐标上为一条直线,用新理论计算的分级效率值较其他理论能更好地接近实验值,是一个相对比较准确的分离效率计算方法.对3组微型旋风器在入口风速为15~25 m/s范围内分级时,分级粒径可以达到0.6μm.