掺杂钕介孔分子筛MCM-41的合成及表征

以十六烷基三甲基溴化铵（CTAB）为表面活性剂,正硅酸乙酯（TEOS）为硅源,采用水热晶化法,合成了钕掺杂的MCM-41介孔分子筛.通过X射线衍射（XRD）、傅里叶变换红外（FT-IR）光谱、透射电镜（TEM）等测试手段对其孔结构和钕原子的存在状态进行了表征.XRD和TEM结果表明,合成样品具有典型的二维六方有序介孔结构,样品的傅里叶变换红外光谱表明钕被成功的引入到介孔骨架中.     

工程教育下的电工技术实验教学改革

在工程教育的背景下,针对传统高校实验教学中存在的问题,以电工技术实验教学方法的改革为切入点,从实验课堂讨论、工程实例讲解、实验仿真和演示实验室的建立四个方面,提出切实能够培养学生基本实验技能、掌握工程科学、提高工程实践能力的实验教学方法。     

Optical turbulence profiling with single star SCIDAR technique

In order to characterize optical turbulence, we have developed a single star SCIDAR （SSS） for measurement of the distribution of Cn^2 with height. The SSS consists of a 40 cm telescope and a CCD camera for fast sampling of stellar scintillation pattern. Spatio- temporal auto and cross-correlation functions of the single star images are computed, providing vertical profiles of optical turbulence intensity C2（h） and wind speed V（h）. Using this new SSS experiment, profiles of turbulence can be obtained from the ground to the top of atmosphere, allowing the determination of seeing, isoplanatic angle and coherence time. Detailed characteristics of atmospheric optical turbulence are important for active and passive imaging, astronomical site testing, adaptive optics, laser communications, target tracking and designation, and laser beam control. We plan to improve the robotization of the SSS to be able to use it routinely even under harsh weather and altitude conditions that we expect to encounter on the high Tibetan plateau or at Dome A in Antarctica. SSS will also be applied for the site testing campaign of the future Chinese extremely large telescope.     

High-pressure polymorph of TiO2-II from the Xiuyan crater of China

Abundant TiO2-II, a high-pressure polymorph of titanium dioxide, was found in the gneiss fragments of impact-produced breccias from the Xiuyan crater. Rutile in the gneiss was severely fragmented and fine-grained clasts less than 2 ~tm in size had been transformed to TiO2-II. Irregular thin layered TiO2-II is also observed in coarse-grained ruffle fragments, where the TiO2-II layers distributes along fractures and cracks in rutile, About 30 percent of rutile in the gneiss had been transformed to TiO2-II. Fine grains of TiO2-II display light bluish grey to light yellow brown in plane-polarized reflected light. Crystallographic investigation shows that TiO2-II has an orthorhombic structure with space group Pbcn. The cell parameters are a=4.543（1）/~, b=5.491（9）/~ and c=4.895（2） ,~. Its empirical formula calculated on the basis of two oxygen atoms can be written as （Tio.985Feo.oosNbo.oor- Si0.003Zr0.0Ol）l.0O302, or simply formula TiO2. According to the shock effects of quartz and feldspars, the peak shock pressure and post-shock temperature in the TiO2-II-bearing gneiss are estimated to be between 35 and 43 GPa and 300-900~C, respectively. The finding of TiO2-II in the shock-metamorphosed gneiss provides another mineral physics evidence for shock origin of the Xiuyan crater.     

脱硫石膏在水泥生产中的应用

主要阐述了脱硫石膏的概念、主要成分及其应用分类,及其在我国水泥工业中作为缓凝剂的性能和再处理方法,分析了脱硫石膏全部替代天然石膏生产水泥的优点及其注意事项,实现脱硫石膏的资源化利用。     

校园外环境景观与园林专业课程实践教学相关状况分析

高校校园外环境景观对师生学习和生活起着举足轻重的作用,而对于开设园林专业的高校来说,则可以将其与园林专业课程实践教学紧密联系,形成相互促进的关系。以阜阳师范学院西湖校区为例,通过对西湖校区可作为和已作为课程实践教学的外环境景观进行统计分析,总结出园林专业利用校园外环境景观进行课程实践教学存在的不足之处,最后提出要善于总结校园外环境景观可利用的实践教学资源、避免在校园外环境景观中重复性实践教学、培养学生学会利用校园外环境景观进行专业实践的方法、适当增加可供园林专业实践教学的优质园林要素的几点建议。     

三种市售大蒜中生物大分子含量比较研究

通过植物生理生化的方法,测定3种市售品种大蒜(四川免根、猴场红皮、化处白皮)蛋白质、脂肪和多糖含量,结果表明四川免根、猴场红皮、化处白皮蛋白质含量分别为2.52、2.92、2.28mg/g,脂肪含量分别0.05、0.09、0.07mg/g,多糖含量分别为84.4、69.7、88.3mg/g。3种大蒜中,猴场红皮大蒜是日常食用的品种之一。     

“病态科学”及其讨论

"病态科学"是很有争议的问题.本文介绍了朗缪尔所界定的病态科学的六大特征,以读者来信、见刊文章为基础,全面阐述各方专家、学者之见解.最后警示科学界注意"病态科学"的袭扰.     

皂化P507体系有机相负载硅对稀土La萃取的影响

在皂化P507萃取稀土过程中,乳化是溶剂萃取中常见的现象,会导致稀土萃取率低和成本升高等.因此,研究了皂化P507体系对Si的萃取,并用负载Si的有机相萃取La,分析Si在两相中的乳化和负载Si的有机相对萃取稀土的影响.结果表明:仅有少量的Si可以进入有机相,Si在两相中的乳化直接影响稀土的萃取效果,当有机相连续与含Si溶液混合四次后,La的萃取量减少了7g/L.负载有机相红外光谱研究表明:Si没有参与皂化P507的萃合反应;水峰和羟基变化说明乳化与萃取过程密切相关.     

工作不安全感、创造性自我效能感对员工创造力的影响研究

对目前关于工作不安全感、创造性自我效能感及创造力的相关研究成果进行系统性的总结,旨在探讨工作不安全感、创造性自我效能感对创造力的影响,并从概念定义、测量工具、研究内容及形式等方面为当前的相关研究指明方向。