Investigation on the synthesis mechanism of β-FeSi2 prepared by pulsed laser deposition

The FeSi2 target alloy was fabricated by conventional powder metallurgy technology, and then, β-FeSi2 thin films was successfully prepared by pulsed laser deposition (PLD). X-ray diffraction (XRD) and field emission scanning electron microscopy (FESEM) were used to characterize the structure, composition, and their changes in the process of β-FeSi2 preparation. In addition, a laser sintering process was also employed to prepare FeSi2 alloy. The analysis of radiation heat transfers in different-sized FeSi2 melt indicates that the cooling rate of the melt depends on the size, i.e., the cooling rate of the micron sized melt is 103 times greater than that of the millimeter-sized melt. The product α-FeSi2 by laser sintering and β-FeSi2 by PLD reveals the different phase transition process in crystallization of milli-meter-sized and micron-sized (or submicron-sized) FeSi2 melt. The results of PLD preparation process shows that β-FeSi2 could be pre-pared through a liquid-phase sintering, followed by a rapid cooling.     

压水堆核电站主管道窄间隙自动焊用焊丝研究

焊接填充材料不仅影响焊接过程的稳定性、焊接接头的性能和质量,同时也影响焊接效率。压水堆核电站建设中主管道传统手工焊接用的填充材料是ER316L,该材料焊接性能稳定,易于操作。主管道窄间隙自动焊采用窄间隙坡口和单层单道焊接技术,该工艺需要焊丝具有更好的熔池流动性和更高的纯净度以保证焊缝成形质量,该文就上述要求对自动焊专用焊丝进行研究。     

Genomic and genic sequence variation in synthetic hexaploid wheat （AABBDD） as compared to their parental species

In order to understand the genomic changes during the evolution of hexaploid wheat, two sets of synthetic hexaploid wheat from hybridization between maternal tetraploid wheat （AABB） and paternal diploid goat grass （DD） were used for DNA-AFLP and single strand conformation polymorphism （SSCP） analysis to determine the genomic and genic variation in the synthetic hexaploid wheat. Results indicated that more DNA sequences from paternal diploid species were eliminated in the synthetic hexaploid wheat than from maternal tetraploid wheat, suggesting that genome from parental species of lower ploidity tends to be eliminated preferentially. However, sequence variation detected by SSCP procedure was much lower than those detected by DNA-AFLP, which indicated that much less variation in the genic regions occurred in the synthetic hexaploid wheat, and sequence variations detected by DNA-AFLP could be derived mostly from non-coding regions and repetitive sequences. Our results also indicated that sequence variation in 4 genes can be detected in hybrid F1, which suggested that this type of sequence variation could be resulted from distant hybridization. It was interesting to note that 3 out of the 4 genes were mapped and clustered on the long arm of chromosome 2D, which indicated that variation in genic sequences in synthetic hexaploid wheat might not be a randomized process.     

粒度组成对KR搅拌头用浇注料性能的影响

以Andreassen颗粒紧密堆积理论为基础,研究KR搅拌头外衬莫来石浇注料临界粒度和粒度组成对其密度、强度和热震稳定性的影响.结果表明,随着临界粒度的增大,浇注料干燥和烧结后冷态密度与强度均明显提高;临界粒度一定时,粒度组成对浇注料冷态密度、强度以及热震稳定性的影响基本一致,但临界粒度不同的浇注料试样达到最佳性能所对应的粒度组成并不完全相同;与冷态性能相比,浇注料热震稳定性受临界粒度的影响较小.     

粒状FeCu纳米颗粒体磁性和磁粘滞性的研究

溶胶法制备了不同粒度的ＦｅＣｕ纳米颗粒体,Ｘ射线衍射（ＸＲＤ）确定了样品的相组成和颗粒的平均粒度,振动样品磁强计（ＶＳＭ）测量了样品在不同温度下的磁化曲线,磁滞回线,涨落场和有效激活体积．“趋近饱和定律”方法求出了样品的有效磁各向异性常数．利用均匀反磁化模型计算了样品的矫顽力,计算值与测量值基本相符．结果表明,样品的激活体积随颗粒体积的增大而增大,激活体积与颗粒的平均体积的大小基本属于同一数量级,粒状ＦｅＣｕ纳米颗粒的反磁化基本符合均匀反磁化．     

瓦斯流动对电磁辐射频谱的影响

制造了大直径密封缸体，建立了瓦斯气体流动及电磁辐射测试的实验系统，用傅里叶变换对不同压力梯度和不同种类瓦斯气体在煤体中流动时电磁辐射的频谱进行了分析。结果表明，瓦斯气体流动产生的电磁辐射频带一般在较低频带，瓦斯流动时电磁辐射的主频带基本随压力梯度的升高而增大。压力梯度越大，瓦斯流动速度越高，对煤体的破坏作用越强，动电效应也越明显，裂隙振荡的频率也越高，从而产生的电磁辐射也越强，频率也越高。     

基于MSP430F5438A的工业排污督察管理终端设计

工业排污占环境污染高达70％,传统水质监测方法效率低且排污企业暗自偷排、突排污水问题严重,为此设计了一款基于MSP430F5438A和北斗的工业排污督察管理终端.工业排污督察管理终端以MSP430F5438A为核心控制器,利用北斗定位模块定位排污口位置并借助水质检测单元实时采集pH值、温度、浑浊度、溶解氧、氨氮浓度等信...     

电弧炼钢炉电极液压调节自适应系统的研究

针对电弧炉炼钢过程中因电弧压降梯度变化引起开环增益改变,从而导致电极调节液压伺服系统品质不稳定的现象,根据参考模型自适应原理,本文提出了两种在开环状态下进行增益补偿,然后形成闭环的方法。经仿真和实验,说明按此设计的电极调节自适应系统,不仅能克服由于电弧压降梯度变化对系统动态品质的影响,而且还能提高系统的响应能力。     

一种新型高效生物可降解ε-多聚赖氨酸修饰阳离子聚合物抗菌剂的合成与性能（英文）

目前临床上使用的大多数抗生素杀菌或抑菌的主要机制为:选择性的作用于细菌细胞核酸和蛋白合成系统的特定环节,妨碍细菌生命活动,导致细菌死亡.然而,细菌形态结构完整性仍然保持,导致细菌产生耐药性.最近研究发现大肠杆菌和金黄色葡萄球菌感染是一些慢性疾病发生的重要因素.纳米颗粒能够选择性的作用于微生物表面,破坏细菌结构完整性,抑制细菌耐药性的产生.本文设计并合成一种生物相容性好且生物可降解ε-多聚赖氨酸修饰阳离子聚合物(EPL-PCL).该多聚物能够自主装形成单分散的纳米颗粒,且对大肠杆菌、金黄色葡萄球菌和枯草芽孢杆菌具有广谱的抗菌活性.相比于ε-多聚赖氨酸,EPL-PCL纳米颗粒具有更强的抗菌活性.进一步研究发现,EPL-PCL纳米颗粒抗菌作用的主要机制为:(1)带正电的EPL-PCL纳米颗粒与带负电的细菌表面相互作用并穿透细胞壁和细胞膜,破坏细菌表面完整性,抑制细菌耐药性的生成;(2)EPL-PCL纳米颗粒暴露显著提高细菌内ROS水平;(3)ROS水平升高显著的破坏细菌细胞代谢,例如提高碱性磷酸酶活性破坏细菌磷的稳态平衡.因此,本文合成的可降解ε-多聚赖氨酸修饰阳离子纳米聚合物可以作为一种有效且广谱的抗菌剂,特别是用于病原菌感染的疾病.     

数字化创新:回顾与展望

结合数字化创新的特征与发展趋势,基于5W2H的分析思路,本文从数字化创新特征(WHAT)、数字化创新研究时间线(WHEN)、数字化创新场景(WHERE)、数字化创新动因(WHY)、数字化创新参与者(WHO)、数字化创新途径(HOW)以及数字化创新代价(HOW MUCH)七个方面对数字化创新相关文献进行了梳理.研究发现,...