高压天然气管道喷射火热辐射计算

天然气燃爆喷射火事故可能造成人员建筑严重损害,为研究大型天然气喷射火燃爆特性,使用CFD计算软件,对质量流量在5 kg/s以上,压力分别为12 MPa与6 MPa,泄漏孔径在25 mm、50 mm与100 mm时的高压天然气喷射火进行仿真,得到这六种工况下喷射火火焰尺寸、温度分布和近地热辐射强度分布曲线,并得到喷射火长度与宽度和泄漏孔直径的线性变化关系.与喷射火常用的Thornton模型对比,仿真结果计算的火焰长度基本符合,热辐射结果在泄漏中心30 m以外基本相近,两种方法都可用于估算远距离喷射火热辐射强度,为天然气设施安全设计提供参考.     

天线时域平面近场测试的信号源误差修正

提出了天线时域平面近场测试中信号源稳定度误差的修正方法.建立了误差修正所需的参考信道,分析了信号源误差所包含的误差项,根据时域近场测试对采样信号进行近场重建和近远场变换的两种方式,分别给出时域-频域结合修正和纯时域修正的两种修正方法,针对信号源误差包含的误差项对采样信号进行修正.实测结果证明修正后得到的频域方向图和时远场波形与参考结果都比较吻合,证明了两种修正方法的正确性.      

Coupling effects of tungsten and molybdenum on microstructure and stressrupture properties of a nickel-base cast superalloy

In order to comprehensively understand the forming mechanism of abnormal phases solidified in a nickel-base cast superalloy with additives of tungsten and molybdenum, the coupling effects of W and Mo on the microstructure and stress-rupture properties were investigated in this paper. The results indicated that the precipitation of primary α-(W, Mo) phase depended tremendously on the amount of W and Mo addition. When the total amount of W and Mo was greater than 5.79 at%, α-(W, Mo) phase became easily precipitated in the alloy.With increasing of Mo/W ratio, the dendrite-like α-(W, Mo) phases were apt to convert into small bars or blockylike phases at the vicinities of γ′/γ eutectic. The morphological changes of α-(W, Mo) phase can be interpreted as the non-equilibrium solidification of W and Mo in the alloy. Since the large sized α-(W, Mo) phase has detrimental effects on stress-rupture properties in as-cast conditions, secondary cracks may mainly initiate at and then propagate along the interfaces of brittle phases and soft matrix. During exposing at 1100 ℃ for 1000 h, the α-(W, Mo) phases transformed gradually into bigger and harder M_6C carbide, which results in decreasing of stress-rupture properties of the alloy. Finally, the alloy with an addition of 14W-1Mo(wt%) maintained the longest stress lives at high temperatures and therefore it revealed the best microstructure stability after 1100 ℃/1000 h thermal exposure.     

UHPLC-MS/MS法同时测定大鼠血浆中汉黄芩素、隐绿原酸和白杨素-7-O-葡萄糖醛酸苷含量

建立了UHPLC-MS/MS同时测定大鼠血浆中的汉黄芩素、隐绿原酸和白杨素-7-O-葡萄糖醛酸苷含量的方法。以芹菜苷为内标,采用ACQUITY UPLC HSS T3色谱柱(2.1 mm×100 mm, 1.8 μm),乙腈和0.1％甲酸溶液为流动相,流速为0.2 mL·min^-1。结果表明,汉黄芩素、隐绿原酸和白杨素-7-O-葡萄糖醛酸苷线性范围为1～1 000 ng·mL^-1(R2>0.99),最低定量浓度为1 ng·mL^-1,提取回收率、基质效应均符合生物样品分析要求。建立的方法灵敏、准确,可用于大鼠血浆中汉黄芩素、隐绿原酸和白杨素-7-O-葡萄糖醛酸苷的测定及其药代动力学研究。     

Effect of cold rolling process on microstructure and mechanical properties of high strength β titanium alloy thin sheets

The microstructure and mechanical properties of Ti-3.5Al-5Mo-6V-3Cr-2Sn-0.5Fe high strength titanium alloy sheets prepared by unidirectional cold rolling and two-step cross cold rolling were investigated. Results showed that the β phase grains were refined significantly by cold rolling followed by solution treatment for a short time.Compared to unidirectional cold rolling, the short time solution treatment after two-step cross rolling could significantly reduce the non-uniformity of the microstructure of the alloy sheets. After aging treatment at 550 ℃,the anisotropy of the mechanical properties still existed in the unidirectional rolled sheets, and the tensile strength was highest along the rolling direction. After solution and aging treatment, the anisotropy of the mechanical properties of the two-step cross rolling process sheet was not obvious than unidirectional cold rolling,and alloy had good strength and plasticity matching.     

The hidden disintegration of cluster heterogeneity in Fe-based glass-forming alloy melt

The evolution of liquid metal at high temperature is known much less than their solid states. This is partially due to that the message concerning clusters, metastable phase or heterogeneity in liquid is usually too slight to be traced. Here, we shed some light on the nature of structural evolution of Fe-based glass-forming alloy during overheating process by the investigation of high-temperature melt viscometry and first principles simulations. It was found that a structural transition around 1400 ℃ occurred in the melts of initial homogeneous ingot, heterogeneous ingot and amorphous ribbons jointly, and was confirmed by the results from differential scanning calorimeter(DSC), and ab initio molecular dynamics(AIMD). Combining these results with Fe-Si-B ternary phase diagram and the melting characteristics of Fe-B compounds, it is safe to conclude that the disintegration of Fe_2B type clusters to Fe_3B-type clusters leads to the observed transition. These results offer a significant reference for the preparation and property control of Fe-based amorphous alloys.     

全天候海冰气象监测系统可靠性研究

目的】为了减少海冰对平台生产所造成的影响,JZ9-3海域首次引用了全天候海冰气象监测系统。为了确保系统的正常运行,需要对系统进行可靠性评估。【方法】采用动态模糊故障树法,对全天候海冰气象监测系统的可靠性进行评估,同时提出初步的预防措施。【结果】通过应用动态模糊故障树对系统可靠性进行评估,获取了系统的薄弱环节,并提出了有效措施对薄弱环节加以控制。【结论】通过研究,有效地提高了系统的可靠性,这也是动态模糊故障树在国内的首次应用,为未来动态模糊故障树的广泛应用奠定基础。     

多发性硬化症患者DTI图像定量化分析

提出了一种联合体素和白质图谱的磁共振扩散张量成像(DTI)方法,明确了多发性硬化症(MS)患者脑白质中受损区域的位置和严重程度.通过计算受检者脑白质区域内各体素中水分子扩散的各向异性指数(FA)和平均扩散率(MD),找出MS患者组和健康对照组(HC)之间FA和MD存在显著性差异的体素及分布情况.结果表明,与HC组相比,MS组FA值在胼胝体体部、压部和双侧放射冠上部等11个脑区有显著性降低;MD值在胼胝体体部、压部和右侧内囊后肢等22个脑区有显著性升高,为临床MS诊断和治疗提供了更有效的参考价值.     

虚拟仿真实验平台的慕课设计

从课前准备、教学实施和评价总结等环节讨论了虚拟仿真实验慕课设计,结合数字电子技术给出了具体的虚拟仿真实验慕课设计结果,从而达到理论与实践相结合、推进基于慕课学习进程和提高学生学习效果的目的。     

我国高校图书馆创客服务存在的问题与对策

高校图书馆开辟创客空间,提供创客服务是在大众创业、万众创新时代浪潮的推动下必然需求。通过调研与比较国内外典型高校图书馆提供的创客服务,分析我国高校图书馆创客服务存在的问题,提出对策与建议,以期为国内高校图书馆提供借鉴与启示。