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701.
SiO2/EPDM复合材料微观形态与动态力学性能的关系 总被引:2,自引:0,他引:2
利用DMTA方法研究了分散剂、硅烷偶联剂以及二者并用对二氧化硅增强乙丙橡胶复合材料动态力学性能的影响,采用扫描电镜和橡胶加工分析仪测试了填料在橡胶基体中的分散和填料在基体中形成的填料网络结构,利用结合胶测试研究了复合材料中填料橡胶之间的相互作用程度。实验结果表明:按照空白样和采用分散剂、硅烷偶联剂、分散剂+硅烷偶联剂对SiO2进行表面处理,填料在橡胶基体中的分散程度提高,填料填料的相互作用逐渐弱化,填料网络结构逐渐减弱,橡胶复合材料在低应变下的储能模量逐渐降低,抗滚动阻力性能逐渐提高。同时,结合胶含量逐渐提高,玻璃化转变峰逐渐变宽,复合材料的抗湿滑性能逐步提高分散剂与硅烷偶联剂并用改性二氧化硅对橡胶复合材料性能提高有协同作用。 相似文献
702.
Sol-Gel水热偶合法制备纳米AlOOH的晶相转变 总被引:4,自引:0,他引:4
以日本理学3015 X射线衍射仪研究了Sol-Gel 水热偶合法制备纳米AlOOH的晶相转变.(1) 在pH3.5、时间5 h、温度低于130 ℃时,主要生成三水铝;当温度高于130 ℃且升高至150 ℃时,三水铝完全转化为AlOOH;(2) 在pH3.5、温度150 ℃、时间小于3 h时,物相以三水铝和AlOOH共存,随时间延长至5 h,三水铝完全转化为AlOOH;(3) 在反应温度150 ℃、时间5 h、pH>8.0时,三水铝的含量随pH的增大而增加,pH<6.0才能转化为AlOOH . 相似文献
703.
基于FPGA的数字陷波器的设计与实现 总被引:4,自引:0,他引:4
以FPGA芯片为平台构建了数字信号滤波实时处理模块,给出了50Hz陷波器的切比雪夫Ⅱ型IIR数字滤波器4阶级联的结构,提出了对滤波器系数量化的逼近方法,完成了基于FPGA的陷波器实现,并成功地实现了对含有工频50Hz噪声干扰的心电信号的滤波处理,通过与Matlab计算所得到的滤波处理效果进行比较分析,结果表明:基于FPGA采用切比雪夫Ⅱ型4级级联结构的IIR数字滤波器的误差满足设计要求. 相似文献
704.
盗窃罪的既遂与未遂,关系到盗窃行为社会危害性大小的认定,关系到追诉时效的认定,关系到共同犯罪是否成立等等,因此有必要对之进行探讨.对于盗窃罪的既遂未遂,不能一概以控制说作为认定标准,应当根据我国刑法规定盗窃罪的犯罪构成,区分不同情况,依据不同标准来确定. 相似文献
705.
The density curve of F distribution 总被引:7,自引:0,他引:7
Employing the properties of special function,we discuss the positional relation between two density curves with different parameters for F distribution in this paper.Some varying regularities about the position of density curve of F distribution have been obtained. 相似文献
706.
LIUWei SHUWensheng LANChongyu 《科学通报(英文版)》2004,49(1):29-32
This paper reports upon the finding of Viola baoshanensis, a cadmium (Cd) hyperaccumulator through field survey and greenhouse experiments. Average Cd concentration in the shoots and roots of V. baoshanensis growing on Baoshan lead/zinc mine in Hunan Province, China, was 1168 and 981 mg/kg, respectively, varying from 456 to 2310mg/kg in the shoots, and from 233 to 1846 mg/kg in the roots.The ratio of Cd concentration in shoot to root (DW) and that in plant shoots to total concentration in surface soil was 1.32 and 2.38, respectively. Under nutrient solution culture, biomass (DW) of V. baoshanensis exposed to 0-30 mg/L Cd insolution increased with Cd supply increasing and reached a maximum at 30 mg/L Cd. Further increase of Cd concentration (40, 50 mg/L) in solution significantly reduced biomass.Cd concentration in the shoots was positively correlated with Cd concentration in the culture medium. Cd concentration in the shoots reached 4825 mg/kg at 50 mg/L Cd solution. Theratio of Cd concentration of shoots to roots in V. baoshanensis was greater than 1 at all Cd treatments, with an average of 1.67 (1.14-2.22). The results indicate that V. baoshanensis is a Cd hyperaccumulator plant. 相似文献
707.
WANGYihua WANGBaohan LIUYun CHENWeizu WANGCunxin 《科学通报(英文版)》2004,49(5):426-431
In the present study, we have developed the method brought forward recently for protein design based on the relative entropy. The new approach can be used in more common situation other than the special limits in the anterior method. The results indicate that our generalized method has increased the prediction precision for protein sequence and will be in favor of the study for protein design. 相似文献
708.
SEM analysis of the changes of carbon layer structure of mesocarbon microbeads heat-treated at different temperatures 总被引:4,自引:0,他引:4
LITongqi WANGChengyang LIUXiujun ZHENGJiaming WANGHui 《科学通报(英文版)》2004,49(11):1105-1110
Mesocarbon microbeads (MCMB) with narrow size distribution, excellent sphericity and no obvious conglutination have been prepared with a coal tar pitch containing quinoline insolubles (QI) as the raw material. Optical microscopy and scanning electron microscopy (SEM) are used to examine the structure of the MCMB. It has been found that SEM technique shows the structural information of MCMB clearly in the form of micrographs even when the structure of MCMB is complex, while the optical technique is useful for analysis of the regular structure of the mesophase spheres but cannot be effectively used to analyze either the complex structure of the green MCMB or the structures of the further heat-treated ones at different temperatures. According to the characteristics of the carbon layers, the structures of the as-prepared MCMB in the present experiment could be classified as (I) Parallel Layer type structure and (2) Bent Layer type structure with the carbon layers gathering at one or two points in the MCMB. In the experiments, SEM is also utilized to investigate the structures of MCMB that are heat-treated at different temperatures. It has been found that the MCMB without any further heat-treatment show no layered-carbons, while the ones heat-treated at temperaturehigher than 1000℃ exhibit obvious layered carbons across their sections. When increasing the heat-treatment temperature, the carbon layers become thinner and flatter. 相似文献
709.
Photocatalytic effect of nature and modified V-bearing rutile 总被引:2,自引:0,他引:2
LUAnhuai GUOYanjun LIUJuan LIUFei WANGChangqiu LINing LIQiaorong 《科学通报(英文版)》2004,49(21):2284-2287
A natural rutile TiO2, which displays photocatalysis on degrading halohydrocarbon pollutants, was reported. The rutile contains up to 1.22% V2O5 (weight percent). Substitutions of Ti by V, as well as Fe, Cu and Zn, result in lattice distortions and defects. Grinding, heating and quenching modify the surface characteristics of ruffle, and consequently increase its photoactivity. It is found that the heating and quenching treatments enhance visible-light absorption of ruffle, especially at 1000 and 1100℃. Ground rutile is effective to degrade tetrachloroethylene and trichloroethylene. While, heating at 1000℃, and quenching at 1000 and 1100℃ distinctly improve degradation rate of samples. The special properties of the natural rutile have particular capabilities in photocatalytic oxidation, especially in degradation of halohydrocarbons. 相似文献
710.
尿激酶原的N-末端135个氨基酸片段包含了表皮生长因子结构域和环柄结构域,参与了尿激酶原和其受体的结合以及尿激酶原诱导的化学趋化活性.利用RT-PCR,从人脐带静脉内皮细胞中克隆ATF基因.将ATF基因插入pET-29a( )中构建表达质粒pET-29a( )/ATF,并转化至大肠杆菌BL21(DE3)中,经IPTG诱导表达及纯化后,从每升培养液中获得15mg rhATF,其纯度超过95%.活性测定结果表明rhATF能够阻断尿激酶原与尿激酶受体的结合,并能抑制尿激酶对纤溶酶原以及纤溶酶对尿激酶原的激活. 相似文献