分光光度法测定脯氨酸的含量

文章用分光光度法研究了脯氨酸与四氯对苯醌的荷移反应 .实验指出 ,在硼砂缓冲溶液中 ,脯氨酸与四氯对苯醌于 30℃的水浴中恒温 1 2 0 min,可形成 1∶ 1的稳定络合物 ,其λmax=35 8nm,表观摩尔吸光系数 ε=1 .5 0× 1 0 5L·mol- 1 ·cm- 1 ,在 60 ng·m L- 1 ～ 40 0 ng·m L- 1 的范围内符合比耳定律 ,用本方法测定药物制剂的含量与文献方法一致 ,回收率在 99.65 %～ 1 0 0 .7%范围内 ,相对标准偏差在 1 .4%以内 .     

APPLICATION OF BORON MODIFIED SILICA SOL ON RETENTION AND DRAINAGE

INTRODUCTIONRecently with the high speed, large-scale develop-ment of papermaking, in the manufacture of paper and paperboard conventional single and dual reten-tion and drainage systems cannot obtain satisfying re-tention and drainage. So in 1980 microparticulate systems appeared. Because of its superiority such as good retention effectiveness on fine and chemicals, improving drainage and paper formation, reducing waste water and enhancing the concentration of white water for good recover…     

广义不确定原理对一般静态黑洞熵的影响

把广义不确定原理引入黑洞熵的计算,采用薄膜brick-wall模型,对一般静态黑洞外部标量场的熵进行了计算,得到了熵计算公式.应用该公式结果表明,可以得到已知所有静态黑洞的Bekenstein-Hawking熵.作为比较和进一步研究,对视界面上的二维膜的熵进行计算,可以更方便和一般性地得到熵与视界面积成正比的结论,该讨论可直接表明黑洞熵就是其视界面上的量子态的熵.与原始brick-wall模型不同的是,这一结论是有限的,计算中无需引入截断,且小质量近似也可以避免.     

公文标题常见病例举隅

针对公文拟制过程中出现的不规范或错误的标题 ,从滥行省略、文种错用、语法不规范、表述不清、表达不简洁、适用不当、标点符号乱用、体号混乱八个方面 ,按《国家行政机关公处理办法》《国家行政机关公文格式》的规定加以分析 ,从多个角度提出了公文标题拟制的基本要素和规范要求     

Which survey indicators are useful for monitoring consumption? Evidence from European countries

This paper assesses the information content of two survey indicators for consumption developments in the near future for eight European countries in the period 1985–1998. Empirical work on this topic typically focuses on consumer confidence, the perceptions of buyers of consumption goods. This paper examines whether perceptions of sellers of consumption goods, measured by retail trade surveys, may also improve short‐term monitoring of consumption. We find that both consumer confidence and retailer confidence embody valuable information, when analysed in isolation. For France, Italy and Spain we conclude that adding retail confidence does not improve the indicator model once consumer confidence has been included. For the UK the reverse case is obtained. For the remaining four countries we show that combining consumer sentiment and retail trade confidence into a composite indicator leads to optimal results. Our results suggest that incorporating information from retail trade surveys may offer significant benefits for the analysis of short‐term prospects of consumption. Copyright © 2004 John Wiley & Sons, Ltd.     

小模数齿轮基节偏差影响下的降噪研究

深入分析了齿轮基节偏差影响下噪声的产生机理，在研究现有降噪措施的基础上，提出了一种新的降噪方案。该方案结构简单，安装调试方便，对轴承的影响小，尤其对小模数齿轮传动，效果更佳。     

关于"当事人承认"的基本问题

在民事诉讼中，当事人承认作为当事人陈述的一种，有其独特的作用，它既可免除对方当事人的举证责任，也对法院的判决起着约束作用。     

Electrocatalytic Oxidation of H_2 O_ 2 at a Carbon Paste Electrode Modified with a Nickel (Ⅱ)-5,11,17,23-Tetra-Tert-Butyl-25,27-Bis(Diethylcarbamoylmethoxy)Calix[4] Arene Complex and Its Application

0　IntroductionThegreatimportanceofnickelelectrochemistryinalkalinemedium ,especiallyforpotentialapplication ,hasattractedmuchattetionofresearcherseithertostudythebehaviorofnickel basedelectrodeitselforitsactivitytowardsothermolecules.Manyreportsshowedthatthenickelbasedelectrodeshaveelectro catalyticactivityforreactionsofappliedinterest,suchaselectro chemicaldeterminationofantioxidantsinfood[1 ] ,detectionofni tricoxide (NO )insolution[2 ] ,electrocatalyticoxidationofmethanol[1 ] ,alcohol[3] ,…     

几种照度计算方法的比较及研究

针对一个典型建筑模型，本文通过对目前几种常用照度计算方法所得结果的分析与比较，指出了造成这种差异的原因及各种计算方法的使用范围及其局限性，并结合照片计算及建筑光环理论基础，提出了较为精确的照明计算方法。