超稳Y-沸石催化合成乙酰乙酸乙酯缩酮

用脱铝超稳Ｙ－沸石作催化剂合成了乙酰乙酸乙酯与乙二醇缩酮和丙二醇缩酮,其产率可达到８０％和９６％,考察了催化剂组成和反应时间对反应的影响规律,发现产物比反应物更易在催化剂表面吸附,对反应机理作了讨论。     

一种新型电池的开发和研究

本文从燃料电池在国内发展的技术状况,各类型燃料电池特性对比,结合我国国情,提出了我国应研究开发熔融碳酸盐燃料电池的建议和设想。     

WINDOWS应用程序中实现二维动画的SDK编程方法

介绍如何利用ＳＤＫ开发具有二维动画效果的ＷＩＮＤＯＷＳ应用程序．程序运行时，动画不断地进行变化，用户可以在生动活泼的环境下进行各项程序功能的操作．     

取代苯基酰基吡唑啉酮Cu(Ⅱ)、Cr(Ⅲ)配合物的合成与表征

合成了新 β双酮试剂 ,1 -对硝基苯基 - 3-甲基 - 4- (α -呋喃甲酰基 )吡唑啉酮 - 5 (HL)及其铜和铬的配合物 .元素分析、摩尔电导数据表明配合物的组成为 :[CuL2 (C2 H5OH) 2 ]·C2 H5OH、[CrL2 (C2 H5OH) 2 ]OH·C2 H5OH .通过红外光谱、紫外光谱、差热 -热重分析对配合物进行表征     

阿斯匹林铜的高效液相色谱分析

建立了用于新药阿斯匹林铜的高效液相色谱分析方法 .采用YWG C1 8柱 ,在室温下 ,n(乙腈 )∶n(水 )(内含 0 .2 %三乙胺 ,用H3 PO4调pH值至 2 ) =32∶68为流动相 ,药用标准品阿斯匹林和水杨酸为对照品 ,在紫外 2 30nm处检测阿斯匹林和水杨酸的含量 ;阿斯匹林铜和水杨酸铜的最小检测限为 0 .0 52mg·L-1 ,0 .0 4mg·L-1 ;阿斯匹林铜和水杨酸铜的平均回收率为 99.7% ,99.9% .     

基于STL-Informer-BiLSTM-XGB模型的供热负荷预测

供热负荷预测是指导供热系统调控的重要手段。提高供热负荷预测精度十分重要,针对机器学习中输出目标的分解预测,提出了一种基于季节和趋势分解(Seasonal and Trend decomposition using Loess, STL)的供热负荷预测方法,构建了适用于供热负荷预测的输出目标。首先利用STL算法将供热负荷时间序列数据分解为趋势分量、周期分量和残差分量,分别训练Informer、BiLSTM和XGB三个模型,将构建好的三个分量预测模型的输出叠加作为初步预测结果,分析误差序列,以BiLSTM预测误差提高模型精度,构建出STL-Informer-BiLSTM-XGB预测模型。将上述模型与常用预测模型进行对比,结果表明所构建的STL-Informer-BiLSTM-XGB 模型的MAPE、MAE和MSE,分别为0.871%、96.18和13202.2,预测效果最优,验证了所提出的方法具有较高的供热负荷预测精度。     

An Efficient Constrained Model Predictive Control Algorithm Based on Approximate Computation

1 .ＩＮＴＲＯＤＵＣＴＩＯＮＭｏｓｔｓｙｓｔｅｍｓａｒｅｓｕｂｊｅｃｔｔｏｃｏｎｓｔｒａｉｎｔｓａｎｄｔｈｅｄｅｓｉｇｎｏｆｃｏｎｔｒｏｌｌｅｒｓｆｏｒｓｕｃｈｓｙｓｔｅｍｓｉｓａｖｅｒｙａｃｔｉｖｅａｒｅａｏｆｒｅ ｓｅａｒｃｈｎｏｗａｄａｙｓ.Ｉｔｉｓｗｅｌｌ ｋｎｏｗｎｔｈａｔｍｏｄｅｌｐｒｅｄｉｃｔｉｖｅｃｏｎｔｒｏｌ (ＭＰＣ) ,ａｌｓｏｃａｌｌｅｄｒｅｃｅｄｉｎｇｈｏｒｉｚｏｎｃｏｎｔｒｏｌ(ＲＨＣ) ,ｈａｓｂｅｅｎｗｉｄｅｌｙａｎｄｓｕｃｃｅｓｓｆｕｌｌｙａｐｐｌｉｅｄｉｎｐｒｏｃｅｓｓｉ…     

The numerical method of inversion for the interior Radon transform

The interior Radon transform arises from a limited data problem in computerized tomography. The corresponding operator R is investigated as a mapping between wightedL ₂-spaces. Our result is the explicit construction of a singular value decomposition for R. This immediately leads to an inversion formula by series expansion and range characterizations. Foundation item: Supported by the Foundation of the Ministry of Education of China and the Science Foundation of Wuhan University Biography: WANG Jin-ping (1963-), male, Ph.D candidate, Research interests are in numerical solution of singular integral equation and integral transformation.     

Two Sorts of Fiber Optic Sensor Monitoring the Cure Process of Composite Laminate

Two new sorts of fiber optic sensor are designed.Firstly, the variation of refractive index of resin surrounding the embedded fiber optic was mean to observed by measuring the speckle spatial spectrum at the end-face of the fiber optic.Secondly, it is proposed to measuring the change of thickness of the laminate by using fiber optic microbend attenuation.The experiment results measured by the fiber optic sensors are given.The first sort of sensor was found to be able to detect the viscosity process of the resin matrix during cure process includeing the minimum point of viscosity, the gelation point and the end point of cure process; the second sort of sensor could detect the course of change of the thickness of composite laminate pressed by operation pressure.It is benefit for us to optimize the operation technology and to establish the intelligent monitoring system about curing process of composites for the reason that the viscosity process and the change course of the thickness of laminate can be monitored.     

基于螺旋理论的机构弹性的几何分解

介绍一种对模拟机器人弹性的６×６刚度和柔顺矩阵进行对角化的几何分解方法．采用螺旋理论，从三个正交的外载螺旋柔顺轴和三个正交的变形螺旋柔顺轴推导得一个相似变换，对角元素是线性及旋转柔顺和刚度的静态值．这与应力、应变及转动惯量的主轴和主值类似，证明了对非奇异及奇异情况，分解总是存在的，并给出了分解表达式．