化学计量学在食品分析中的应用

简述了化学计量学、分析化学和食品分析三者之间的关系和各自的任务。评述了化学计量学中的多元校正、化学模式识别和人工神经网络等方法在食品营养成分分析、无机元素分析、维生素分析、有毒有害物质分析、分类和质量鉴别及某些过程分析领域中的应用。重点介绍了最小二乘法和偏最小二乘法在食品分析中的应用。同时,对该领域的研究方向和前景进行了展望。     

明代八股文对文人创作的背离

确立于明代的八股文,对明清文人和文学创作影响极大,它既带给文人荣华富贵的梦想,也给他们带来强烈的精神苦闷和焦虑。其程式化、格式化在某种程度上影响了文人独创性和个性的发挥,影响了他们文学创作的思维方式。后世才子背离八股文写作从而获得较大成就。     

差分方程xn+1=(α+βxn+γxn-1)/(A+Bxn+Cxn-1)两个猜想的证明

证明差分方程xn 1=α βxn γxn-1A B xn Cxn-1,n=0,1,…当C∈(0, ∞)时每个非负解是有界的.     

新型钴基耐热合金高温流变变形行为

在Gleeble-1500热模拟机上,采用等温压缩试验,研究了一种含Ti和Al的新型钴基耐热合金在850~1150℃温度范围的压缩变形行为.实验结果表明:该合金具有良好的抗高温流变性能,在850℃及应变速率0·0021~2·1s-1范围时其峰值流变应力可以达到360~475MPa.合金的流变行为可用Zener-Hollomon参数来描述.     

Approach to Weighted Geometric Evaluation Based on Projection Pursuit

Weighted geometric evaluation approach based on Projection pursuit （PP） model is presented in this paper to optimize the choice of schemes. By using PP model, the multi-dimension evaluation index values of schemes can be synthesized into projection value with one dimension. The scheme with a bigger projection value is much better, so the schemes sample can be an optimized choice according to the projection value of each scheme. The modeling of PP based on accelerating genetic algorithm can predigest the realized process of projection pursuit technique, can overcome the shortcomings of large computation amount and the difficulty of computer programming in traditional projection pursuit methods, and can give a new method for application of projection pursuit technique to optimize choice of schemes by using weighted geometric evaluation. The analysis of an applied sample shows that applying PP model driven directly by samples data to optimize choice of schemes is both simple and feasible, that its projection values are relatively decentralized and profit decision-making, that its applicability and maneuverability are high. It can avoid the shortcoming of subjective weighing method, and its results are scientific and objective.     

A Project Risk Ranking Approach Based on Set Pair Analysis

Set Pair Analysis （SPA） is a new methodology to describe and process system uncertainty. It is different from stochastic or fuzzy methods in reasoning and operation, and it has been applied in many areas recently. In this paper, the application of SPA in risk ranking is presented, which includes review of risk ranking, introduction of Connecting Degree （CD） that is a key role in SPA., Arithmetic and Tendency Grade （TG） of CDs, and a risk ranking approach proposed. Finally a case analysis is presented to illustrate the reasonability of this approach. It is found that this approach is very convenient to operate, while the ranking result is more comprehensible.     

朊圆酵母尿酸酶的基本特性研究

研究了尿酸酶分离纯化条件和pH、温度、底物浓度、一些有机和无机试剂对尿酸酶酶促反应速度的影响.研究结果表明,用Triton X-100及巯基乙醇处理细胞悬液(pH 8.5),再用超声波处理破碎细胞效果最佳.硫酸铵沉淀尿酸酶的最佳浓度为75%.用Phenyl-Sepharose CL-4B疏水层析和Xanthine-agarose亲和层析两步纯化步骤可获得理想纯度的酶制剂.在一定的条件下,尿酸酶的最适pH和酸碱稳定pH范围分别为8.5和5.0~12.最适温度为37℃;热稳定性较好,在50℃处理30 min时     

Shape controllable preparations of PbS nanocrystals using cysteine as the precursor of S^2- ions

Flowerlike, spherical and cubic PbS nanoparticles have been successfully synthesized by refluxing cysteine and lead nitrate in an alkaline solu- tion. The influences of the cysteine to Pb2 molar ratio, the pH value of the reaction mixture as well as the refluxing time on the shape of PbS nanoparticles were investigated. Detailed experimental results demonstrated that a higher molar ratio of cysteine to Pb2 (5.2:1) and shorter refluxing time favor the for- mation of flowerlike PbS nanoparticles at pH 9.0. While lower pH value (8.0) favors the formation of spherical PbS nanoparticles, and higher pH value (10.0), however, favors the formation of cubic PbS nanoparticles. The mechanism for the shape control of PbS nanoparticles is discussed.     

正则牛顿过程设计n分之一阶分抗电路(英文)

讨论基于一阶正则牛顿迭代求根过程进行任意阶分抗的近似求解方法.通过迭代求解n阶方程的正实根,作为分抗的模拟.给出迭代的精确公式,并分析其收敛必须满足的条件,最后给出相应的模拟无源电路实现方案.     

交换C~*-代数张量积的纯态和谱

讨论了非交换C*-代数的谱与纯态值域,得到了C*-代数张量积中两个元的本质纯态值域的表示.