浅议构建西安非物质文化遗产保护体系

科学地实施西安非物质文化遗产保护,关系到国家的文化安全、社会的和谐发展和民族文化的血脉传承;构建西安非物质文化遗产保护体系是西安发展战略的重要组成部分,是西安持续、全面发展必然的文化诉求。     

正则半群上与格林关系有关的同余

讨论正则半群上与格林关系有关的同余生成的格,研究这个格的Hasse图的几种退化情形,然后确定逆半群和两类特殊的完全正则半群上与格林关系有关的同余所生成的同余格.     

溴酸钾存在下苯丙氨酸的极谱催化波研究

在0.10mol/L LiCl-0.02mol/L HCl-8.0×10-3mol/L KBrO3支持电解质中,苯丙氨酸产生一个极谱催化波,峰电位为-1.65V(vs.SCE).该极谱催化波二阶导数峰电流与苯丙氨酸的浓度在2.0×10-5～2.5×10-3mol/L范围呈线性关系,其检测下限为6.5×10-6mol/L.本文建立了苯丙氨酸的分析测定方法,讨论了该极谱催化波的产生机理.     

吉安市吉州工业园区规划设计与思考

工业园区是工业化的载体,是现代城镇总体布局中的一个重要功能区和发展主要因素。本文运用新城市主义、可持续发展等设计理念,通过对吉州工业园区规划的用地空间布局、空间景观、生态环境保护的分析和探讨,提出构建经济欠发达地区工业园区建设的城市新区发展模式。     

定态量子流体动力学模型解的一些估计

有关量子流体动力学模型的研究成为了一个热点问题。研究了当电子密度为正,引入新的变换ω=ρ后,得到稳定态半导体量子流体动力系统的解的L∞估计、H1估计和H2估计。     

Transports of K^＋, Ca^2＋ Ions in Liquid Membrane with Calixarene Derivatives as Carriers

A few derivatives of calixarenes have been synthesized and characterized by IR, ^1H NNtR, thermal and elemental analysis. The transport of potassium or calcium ion through the liquid membrane, in which the derivatives act as carriers, has been studied. The electron-effect of the substituent on the upper rim of calixarene possesses important effect on the net transport of metal ions. The p- tert-butylcalix[4]arene is the best carrier of calcium ion, compared with p-tert-calix[4]arene（n = 4, 6, 8）. The ptert-butylcalix[4]arene acid is better than p-tert-butylcalix [4]arene. The calixr43crown is the best carrier of calcium ions of all the carriers. The pH gradient between the source and receiving phase, and the concentration of K^＋ , Ca^2＋ ions in the source phase affect mainly transport. After the transport, the pH value of the source phase is found to be decreased, once the calix [n ] arene derivatives act as carrier. But it is not the case for the calix[n] crowns. It might be interpreted as the result of their different mechanisms.     

Synthesis and Characterization of Titania and Rare Earth Doped Titania Nanoparticles by Sol-gel Process

Titania sol has been prepared by the sol-gel process with Ti（OC4H9）4, as precursor. TiO2 gel was obtained through hydrolysis and condensation process. Rare earth such as La2O3, CeO2 and Gd2O3 were introduced into the nanostructure TiO2. After TiO2 and rare earth doped TiO2 powders were calcined at 400℃, 500℃, 600℃, 700℃ and 800℃ respectively, the characteristic analyses of the TiO2 samples were studied by UV-VIS, XRD and TEM etc. It was found that there are some stringer absorption peaks at 200 - 325 nm. The rare earth doping can increase the phase transition temperature convertin8 anatase phase into rutile phase, can decrease the grain size of TiO2particles and can improve the ann-UV capacity of the coating fabrics.     

基于四元数的导弹反步控制及全方位算法应用

针对传统四元数适应范围小,分析误差困难问题,基于误差四元数的概念深入研究了姿态误差形式和姿态角和四元数全方位转换问题,提出了姿态角和四元数的全方位转换算法。该算法实现了姿态角和四元数的-1800到1800全空间转换,并且具有抗扰动的能力,同时将四元数与非线性反步(backstepping)方法结合,进行了导弹姿态控制。仿真表明了全角度算法的正确性,以及基于文中的四元数姿态误差方程可有效进行导弹全方位姿态控制。     

极谱分析法测定生活固体废弃物中痕量铅

采用浓硫酸炭化、硝酸-高氯酸消解废弃报纸、导购彩报和废弃尼龙麻袋样品,在6%溴化钾、1%酒石酸钾钠、0.7%的盐酸、5%磷酸、2%盐酸羟胺、3%(体积)三乙醇胺混合底液中,以单扫描极谱法测定样品中痕量铅的含量.结果表明,铅在滴汞电极上于-0.47V(相对饱和甘汞电极)处产生一灵敏催化极谱波,极谱峰电流与铅浓度在0.2～300ng/mL范围内有良好的分段线性关系,检出限为0.16ng/ml.该方法的RSD为5.6%～7.1%,加标回收率为89%～105%.本法快速简便,准确度高,用于实际样品测定的结果满意.     

催化极谱法测定土壤中的痕量镉

采用单扫描极谱法测定土壤中镉含量,确立了1%碘化钾-1.5%酒石酸钾钠-2%三乙醇胺-0.6%盐酸-9%磷酸测定体系.在此测定体系中,镉在滴汞电极上于-0.71V(相对饱和甘汞电极)处产生一灵敏催化极谱波,镉浓度在0.2ng/ml～1μg/ml范围内与极谱峰电流有良好线性关系,检出限为0.1ng/ml.该方法用于土壤样品测定的RSD为0.6%～9.5%,加标回收率为90%～110%.该方法操作简便,用于土壤样品测定的结果满意.