甲胺磷原油中硫酸二甲酯的正相高效液相色谱分析

采用 Ｃ１８ 柱，示差折光检测器，以７０３０（ 体积比） 正己烷 异丙醇为流动相的正相高效液相色谱对甲胺磷原油中的硫酸二甲酯进行了分析，方法准确，快速，其平均回收率为９８ ．４ ％ ，相对标准偏差小于０ ．５ ％ ．     

时间延缓的动力学计算

从动力学的观点计算相对论效应中的时间延缓，提出一种关于时间延缓的因果型说明     

The role of endosomal-recycling in long-term potentiation

Long-term potentiation (LTP) defines persistent increases in neurotransmission strength at synapses that are triggered by specific patterns of neuronal activity. LTP, the most widely accepted molecular model for learning, is best characterised at glutamatergic synapses on dendritic spines. In this context, LTP involves increases in dendritic spine size and the insertion of glutamate receptors into the post-synaptic spine membrane, which together boost post-synaptic responsiveness to neurotransmitters. In dendrites, the material required for LTP is sourced from an organelle termed the endosomal-recycling compartment (ERC), which is localised to the base of dendritic spines. When LTP is induced, material derived from the recycling compartment, which contains α-amino-3-hydroxy-5-methyl-4-isoxazole propionate-type glutamate receptors (AMPARs), is mobilised into dendritic spines feeding the increased need for receptors and membrane at the spine neck and head. In this review, we discuss the importance of endosomal-recycling and the role of key proteins which control these processes in the context of LTP.     

Co-substituted ATS-type molecular sieves and films for cyclohexane oxidation

Pure CoAPO-36 crystal grains were synthesized by hydrothermal reaction. Porous α-Al₂O₃, stainless steel and K₂Ti₆O₁₃ supported CoAPO-36 films were fabricated using in situ crystallization for the first time. SEM images and XRD measurements demonstrate that a continuous CoAPO-36 film was obtained on the K₂Ti₆O₁₃ substrate. Diffuse reflectance UV-Vis spectra indicate that Co²⁺ has been incorporated into the ATS framework. Both CoAPO-36 crystal grains and the K₂Ti₆O₁₃ supported CoAPO-36 film exhibit satisfactory catalytic activities for the oxidation of cyclohexane.     

BotGuard: Lightweight real-time botnet detection in software defined networks

The distributed detection of botnets may induce heavy computation and communication costs to network devices. Each device in related scheme only has a regional view of Internet, so it is hard to detect botnet comprehensively. In this paper, we propose a lightweight real-time botnet detection framework called Bot-Guard, which uses the global landscape and flexible configurability of software defined network (SDN) to identify botnets promptly. SDN, as a new network framework, can make centralized control in botnet detection, but there are still some challenges in such detections. We give a convex lens imaging graph (CLI-graph) to depict the topology characteristics of botnet, which allows SDN controller to locate attacks separately and mitigate the burden of network devices. The theoretical and experimental results prove that our scheme is capable of timely botnet detecting in SDNs with the accuracy higher than 90% and the delay less than 56 ms.     

Does an Old Art Suffice for New Problems?

In this review I argue that Puech draws on two important currents in modern thought: the criticism of the ontological and social priority of conflict, and the rehabilitation of praxis vis-à-vis theoria. Still, his plea for a non-confrontational art of living leaves important questions unanswered. What is the problem exactly? What does exactly count as (non)confrontational? What is non-confrontation exactly meant to solve? What is the antiposition here? And: how does this new (or rather: old) art of living relate to the political and ethical varieties of Technology Assessment?     

Superconvergence of mixed covolume method on quadrilateral grids for elliptic problems

This paper considers the mixed covolume method for the second-order elliptic equations over quadrilaterals.Superconvergence results are established in this paper on quadrilateral grids satisfying the h~2-parallelogram condition when the lowest-order Raviart-Thomas space is employed in the mixed covolume method.The authors prove O(h~2) accuracy between the approximate velocity or pressure and a suitable projection of the real velocity or pressure in the L~2 norm.Numerical experiments illustrating the theoretical results are provided.     

Maximum likelihood estimator of the parameter for a continuous one-parameter exponential family under the optimal ranked set sampling

This paper studies a maximum likelihood estimator (MLE) of the parameter for a continuous one-parameter exponential family under ranked set sampling (RSS). The authors first find the optimal RSS according to the character of the family, viz, arrange the RSS based on quasi complete and sufficient statistic of independent and identically distributed (iid) samples. Then under this RSS, some sufficient conditions for the existence and uniqueness of the MLE, which are easily used in practice, are obtained. Using these conditions, the existence and uniqueness of the MLEs of the parameters for some usual distributions in this family are proved. Numerical simulations for these distributions fully support the result from the above two step optimizations of the sampling and the estimation method.     

Selective susceptibility to nanosecond pulsed electric field (nsPEF) across different human cell types

Tumor ablation by nanosecond pulsed electric fields (nsPEF) is an emerging therapeutic modality. We compared nsPEF cytotoxicity for human cell lines of cancerous (IMR-32, Hep G2, HT-1080, and HPAF-II) and non-cancerous origin (BJ and MRC-5) under strictly controlled and identical conditions. Adherent cells were uniformly treated by 300-ns PEF (0–2000 pulses, 1.8 kV/cm, 50 Hz) on indium tin oxide-covered glass coverslips, using the same media and serum. Cell survival plotted against the number of pulses displayed three distinct regions (initial resistivity, logarithmic survival decline, and residual resistivity) for all tested cell types, but with differences in LD₅₀ spanning as much as nearly 80-fold. The non-cancerous cells were less sensitive than IMR-32 neuroblastoma cells but more vulnerable than the other cancers tested. The cytotoxic efficiency showed no apparent correlation with cell or nuclear size, cell morphology, metabolism level, or the extent of membrane disruption by nsPEF. Increasing pulse duration to 9 µs (0.75 kV/cm, 5 Hz) produced a different selectivity pattern, suggesting that manipulation of PEF parameters can, at least for certain cancers, overcome their resistance to nsPEF ablation. Identifying mechanisms and cell markers of differential nsPEF susceptibility will critically contribute to the proper choice and outcome of nsPEF ablation therapies.