一种硫代酰胺基螯合功能纤维的研制

以腈纶纤维为起始原料,经乙二胺预交联后,以DMF作溶剂与硫化钠反应,合成了一种硫代酰胺功能基可达5.6mmol/g千纤维的含硫螯合功能纤维,利用红外光谱、硫含量测定等手段对这种功能纤维的结构进行了初步确定并探讨了溶剂、摩尔比以及时间、pH等对反应产物的影响.     

IMI及其微生物转化产物5-hydroxy IMI的HPLC分析

研究了烟碱类杀虫剂IMI及其微生物转化产物5-hydroxy IMI的反相高效液相色谱分析方法．采用Zorbox OSD反相柱，水和乙腈（75：25）（v／v）为流动相，流速为1mL／min，检测波长为269nm，IMI和5-hydroxy IMI得到较优分离．在0．5～50mg／L的浓度范围内，两种物质的色谱峰面积和浓度之间呈线性关系，IMI和5-hydroxy IMI的标准工作曲线分别为y=112．23x-1．7775和y=98．039x-17．508；相关系数为0．9999和0．9997．转化产物的样品中IMI和5-hydroxy IMI添加的回收率分别为99．3％和97．4％．     

药用植物紫草的研究进展

文章主要对近几年来药用紫草化学研究、药理、药剂、临床应用及研究进展进行了概述。     

用MMC扩展技术实现活动目录扩展属性的管理

首先简要介绍了微软的活动目录及如何实现活动目录的访问。然后介绍了微软的控制台技术和控制台的开发，尤其是对已有控制台的扩展。最后介绍了如何开发一个扩展的snap-in来实现控制台的扩展。     

基于USB接口的变电站自动化系统中通信控制器的设计

变电站自动化系统中采用通信控制器负责与上位机及调度中心的通信。传统的设计抗干扰能力差,且安装不便。本设计则利用USB总线的优点,采取多种抗干扰措施保障数据通信的安全高效,并对USB传输机制作了简要的介绍。     

氢对Ti—Al—Zr钛合金管材的组织和性能的影响

分析和试验了Ti -Al -Zr单相α -钛合金管材的化学成分、金相组织和室温机械性能后 ,采用人工吸氢法使该种钛合金材料获得了不同的氢含量。进而 ,测出了其延伸率随氢含量变化的关系曲线 ,从而认识到氢对该材料的塑性指标会造成显著的影响。随后 ,用氢含量为 132× 10 -6、342× 10 -6和 80 8× 10 -6的 3种试样和它们的拉伸断口分别进行了金相和SEM分析。观察到了不同氢含量的样品中氢化物的金相形态及其分布特征 ;由对拉伸断口的分析工作 ,得出氢化物呈薄片状析出的特点 ,而惯析面为α相 (hcp结构 )的基面、近基面和其它易滑移面。最后 ,讨论了氢化物的种类、析出特征 ,并对氢化物在无织构的钛合金管材内的分布特点对其氢损伤的影响程度作了说明     

重庆火锅文化旅游开发的思考

饮食文化资源是中国旅游资源的重要组成部分。火锅是重庆最具代表性的饮食文化和最有特色的优势资源之一。将火锅这一饮食文化资源与旅游结合起来，开发重庆火锅文化旅游，对促进重庆旅游发展既是必要的，也是可行的。打造重庆火锅文化旅游需要全方位的深层次挖掘，最终实现社会效益和经济效益的双赢局面。     

Lightning activity on the central Tibetan Plateau and its response to convective available potential energy

Lightning flash activities on the central Tibetan Plateau have been studied by using the satellite-based Lightning Imaging Sensor(LIS)database from January 1998 to July 2002.The lightning activity shows a clear diurnal variation on the central Plateau.The peak lightning activity appears at about 17:00 which is 3 h earlier than that in Jingxhou,Hubei in the same latitude belt nearby,indicating that the lightning activity is a sensitive indicator of solar heating on the Plateau.The lightning discharge is weaker on the Plateau than Jingzhou.Hubei and other low-altitude continental regions because of the lower convective available potential energy(CAPE)on the Plateau.The CAPE on the Plateau is 12 times lower than that in Jingzhou,Hubei,and 20 times lower than that in the sea-level region,such as Guangzhou and Florida.However,the sensitivity of lightning activity to CAPE changes on the Plateau is up to 30 times more sensitive than other prominent low-altitude regions.     

Inorganic chemical composition and source signature of PM2.5 in Beijing during ACE-Asia period

Aerosol samples for PM2.5 were collected in Beijing for 38 consecutive days from March to April 2001 using an IMPROVE Sampler. Concentrations of 20 elements in PM2.5 were determined using a PIXE method. Results show that the average mineral dust concentration of PM2.5 was 14.6 Ilg/m3 during the observation period. On the sand-dust event days of March 21 and April 10, dust PM2.5 mass concentrations were 62.4 and 54.1 μg/m^3, respectively.These demonstrate that fine particle pollution by dust event in Beijing was very severe. The enrichment factors of S and Cu reached minimums on the dusty days and were high on the non-dusty days. It is considered that enrichment factors of elements in PM2.5, which are associated with human activities, can probably provide an effective method to distinguish local sources from external sources of dust. Factor analysis on the chemical composition in PM2.5 shows that sources of crustal matters, anthropogenic emission, and oil combustion contributed to PM2.5 levels in air in the springtime of 2001 in Beijing.     

Progress in the study of tectophysicochemistry

Tectophysicochemistry is a research area that deals with the interrelations between physical and chemical changes of crustal materials caused by tectonism. A given tectonic force may be resolved into two parts: homogeneous stress and differential stress. Homogeneous stress refers to isotopic pressure, which is superimposed on the original pressure and affects the equilibrium of various chemical reactions. It is also a factor that influences petrogenesis,metallogenesis and metamorphism. Differential stress is commonly produced when external forces act on a given solid body. It may cause deformation of crustal materials and generate various kinds of structural features. Tectophysicochemistry pays special attention to pressure, temperature and other physicochemical conditions produced or induced by tectonism and studies the influences of additional tectonic parameters on various chemical equilibria, so it gradually develops into an independent area of science.