Progress in magnetic couple system of nitroxidemetal complexes

Metal_radical method is an effective approach to synthesizing magnetic molecular materials. With the development in decades, the study of nitroxide_metal complexes has made great progress in model, theoretical treatment and design of molecules. Several mechanisms of the metal_radical magnetic coupling are discussed. Molecular magnetic project of nitroxide_metal complexes has made fruitful achievements, but crystal magnetic project is difficult to be controlled, and it is a challenge to chemists. The studies on nitronyl nitroxide_metal complexes are summarized. At present, there are three major approaches to increasing the T c of the metal_radical compounds: (ⅰ) Searching for nitronyl nitroxide ligands that can yield 3_D ferro_ or ferrimagnetic structures; (ⅱ) decorating the structure of radicals with the aim to enhance the coordinate capability of radicals; (ⅲ) grafting polynitroxide radicals as a versatile bridge. The third approach, namely searching for polynitroxide ligand, will serve as a hopeful strategy for exploring higher T c radical molecule_based magnets.     

Microstructure and optical properties of Ag5In5Te47Sb33 phase change thin films with high reflection in thermal annealing process

The microstructure and optical properties of Ag-5In-5Te 47Sb 33 phase change films with high reflection in the thermal annealing process were systematically reported. The as_deposited film is amorphous and its crystalline temperature is 160℃. The annealed films are crystalline. The crystalline phases are AgInTe-2, AgSbTe-2 and Sb when annealed at low temperature. When annealed at 220℃, the AgInTe-2 phase disappears and the amount of AgSbTe-2 is the largest. The research of electronic transmission microscopy shows that the morphology of AgSbTe 2 is sphere and that of Sb is bludgeon. The reflection of the annealed films is higher and reaches its peak value at 220℃.     

广西大瑶山蝶类调查

报道采自广西大瑶山蝶类１２４种（含亚种）,分属于１１科８１属。     

油库发油控制及管理系统的研究

阐述了油库发油体积及重量的测量过程,讨论了控制及管理的功能要求,提出了设定关阀提前量ΔＸ,并控制调整其大小以提高发油精度的思想。系统采用主从式上下两级微机网络。文中给出了该系统的实现方法,同时论述了保证系统安全运行的措施。     

贵阳地区蝗虫的危害与防治

论述了贵阳地区（5区1镇）7科17属23种蝗虫的生活习性,危害情况,并提出了防治措施。     

三乙基苄基氯化铵合成反应动力学研究

用电导法分别测定了三乙基苄基氯化铵合成反应在乙醇、正戊醇、１,２－二氯乙烷三种溶剂中的反应进程,此反应在三种介质均为二级反应;求出了不同温度下的反应速度常数、反应活化能、指前因子以及活化熵变;１,２－二氯乙烷是非质子性溶剂,对三乙基苄基氯化铵合成这类双分子亲核反应有利。乙醇溶剂的反应速度随温度升高而明显加快。     

甘蔗联合固氮菌对甘蔗叶片养分含量的影响

分析从广西不同地方、不同品种的甘蔗分离到的甘蔗联合固氮菌若干株的固氮酶活性,并将这些菌株接种甘蔗,分析接种了甘蔗联合固氮菌的甘蔗根组织的固氮酶活性,研究它们对甘蔗叶中氮、磷、钾及微量元素含量的影响。     

广西铺道蚁属昆虫研究(膜翅目:蚁科)

报道采自广西的铺道蚁属Ｔｅｔｒａｍｏｒｉｕｍ昆虫１０种,其中５种为广西区新记录种,即：茸毛铺道蚁Ｔ．ｌａｎｕｇｉｎｏｓｕｍＭａｙｒ、陕西铺道蚁Ｔ．ｓｈｅｎｓｉｅｎｓｅＢｏｌｔｏｎ、史氏铺道蚁Ｔ．ｓｍｉｔｈｉＭａｙｒ、相似铺道蚁Ｔ．ｓｉｍｉｌｉｍｕｍ（Ｓｍｉｔｈ）和克氏铺道蚁Ｔ．ｋｒａｅｐｅｌｉｎｉＦｏｒｅｌ。标本保存于广西师范大学生物系标本室。提供广西该属已知１０种的工蚁分种检索表。     

人非小细胞肺癌rasP^21和CD44的表达及意义

用免疫组化ＬＳＡＢ法检测４６例非小细胞肺癌ｒａｓＰ２１和ＣＤ４４的表达。结果：ｒａｓＰ２１的阳性率鳞癌为５９％,腺癌６３％;ＣＤ４４的阳性率鳞癌为４１％,腺癌６３％。统计学分析证明：不同临床分期的ｒａｓＰ２１表达强度有显著性差异（Ｐ＜００１）;有淋巴结转移与无淋巴结转移的ＣＤ４４表达程度有显著性差异（鳞癌Ｐ＜００１,腺癌Ｐ＜００２５）;ｒａｓＰ２１与ＣＤ４４表达强度两者无相关性（Ｐ＜００５）。结论：ｒａｓＰ２１的表达与预后不良有关,ＣＤ４４的表达与淋巴结转移有关。