一种组氨酸修饰的芘类Hg2+荧光探针

〖JP2〗以组氨酸和芘甲酸为原料，设计合成了一种荧光化合物芘甲酰组氨酸甲酯，通过核磁、质谱表征其结构. 荧光测试结果表明，在水溶液中该化合物能够对Hg2+表现出荧光猝灭响应，而相同条件下其他金属离子对该化合物几乎没有类似的荧光识别现象，因此该荧光化合物对Hg2+具有专一荧光识别作用，是一种有效的Hg2+荧光探针.〖JP〗     

The effect of corporate governance on debt financing cost of listed companies

In recent years,bank credit business is booming with the increasing borrowing intention of China’s listed companies,and debt financing has become the major approach among listed companies’financing strategies.As a series of institutional arrangements about rights,responsibilities and benefits between different shareholders,corporate governance mechanism has a significant influence on the cost of debt financing.This paper employs variable coefficient panel data model to investigate the relationship of the listed company’s debt financing costs and corporate governance mechanism in terms of structural characteristics and time series characteristics.The results show that optimizing the structure of both Board of Directors and Board of Supervisors,establishing a reasonable management incentive system and reducing the concentration of ownership properly can directly contribute to a lower company’s debt financing costs.Meanwhile,property rights have an interactive influence on corporate governance from four aspects,which indirectly effect in company’s debt financing costs.     

蒽与马来酸酐的微波辐射干反应

以微波辐射方法进行了蒽与马来酸酐的干反应。同时考察了微波辐射时间，辐射能量对反应收率的影响，并与常规反应进行比较。结果表明：微波辐射3min反应收率可达80％，比常规干反应速率提高近120倍，比常规溶液法反应速率提高近30倍。     

浅谈建筑外墙涂料的质量控制

任何不符合质量要求的产品，都势必影响整个建筑物的质量。为此，从最基础的原材料把关入手，注重操作工序质量的改进和提高，是文章阐述的特征。对施工过程中容易出现的质量问题和一些不正确的做法及表现做简要分析，并按照现行标准及规范，结合本地区的特点，提出预防及改进措施。     

电火花线切割加工中放电间隙状态的实时检测

通过对电火花放电状态的分析,提出了基于数字电路的电火花线切割(WEDM)放电间隙的实时检测方法。采用对单位时间内放电状态的统计,得到电火花线切割过程中各种状态的概率,为电火花线切割的智能控制提供控制依据。试验表明,该方法能有效检测WEDM加工中放电间隙的状态,为进一步研究WEDM智能加工控制系统提供了可靠的控制依据。     

Science Letters: A new quantitative model of ecological compensation based on ecosystem capital in Zhejiang Province, China

Ecological compensation is becoming one of key and multidiscipline issues in the field of resources and environmental management. Considering the change relation between gross domestic product (GDP) and ecological capital (EC) based on remote sensing estimation, we construct a new quantitative estimate model for ecological compensation, using county as study unit, and determine standard value so as to evaluate ecological compensation from 2001 to 2004 in Zhejiang Province, China. Spatial differences of the ecological compensation were significant among all the counties or districts. This model fills up the gap in the field of quantitative evaluation of regional ecological compensation and provides a feasible way to reconcile the conflicts among benefits in the economic, social, and ecological sectors.     

国企中职务侵占犯罪认定初探

本文从职务侵占犯罪的概念入手，分析其基本特征与该犯罪行为的主观，客观，主体，客体等四大要素。阐述了此类犯罪的构成，通过与其他相关犯罪的比较，使读者能正确把握此类犯罪。     

PWR蒸汽发生器中一、二次汽水分离器加装挡水器研究

在水－空气实验台架上，对PWR蒸汽发生器中一次汽水分离器和一、二次水分离器加装挡水器进行了一系列实验研究，实验表明，在循环倍率不大的条件下，一、二次汽水分离器加装档水器，可降低汽水分离器的上携带，挡水器的集水效果与挡水器的轴向位置有关。     

谈市政工程施工管理工作的科学发展

市政工程是城市正常运转和社会经济发展的保障,所以市政工程施工的质量至关重要,用科学的方法管理市政工程施工是未来的发展方向。     

聚合物改性乳化沥青防水涂料在水泥砼桥面上的应用

随着高等级公路对路面质量要求的提高,桥面铺装的质量要求也相应提高.、在桥梁的正常使用期内需经常对面层进行维修或翻新,为保证在面层维修或翻新施工中不对桥梁造成损坏,有必要设置桥面防水层.文章主要从聚合物改性乳化沥青的概述、乳化沥青改性剂的选择、水泥砼桥面防水层的施工质量要求、桥面防水涂料防水层的施工及施工注意事项这几个方面进行阐述,以供参考.