Crystal structure determining of 7-ADCA based on X-ray powder diffraction

Traditionally, crystal structure data can be collected and determined from single-crystal X-ray diffraction. However, in the fields of organic and macromolecular crystallography, it is often difficult or impractical to grow single crystals with suitable sizes and purity. Therefore, it will be benefited from the newly growing analytical tool that combining X-ray powder diffraction based on polycrystalline samples and ab initio calcula- tion[1]. 7-ADCA is one of the most important intermediate…     

关于Killing方程及其物理意义

从变分原理和对称变换出发，讨论了Ｈｌｄｅｒ变分及ＣｙｃлｏＢ变分下的Ｋｉｌｌｉｎｇ方程，并简述其几何意义．     

高砷烟尘酸性氧化浸出砷和锌的试验研究

采用酸性氧化浸出工艺对某冶炼厂高砷烟尘进行湿法浸出砷、锌的试验研究。通过单因素试验确定最佳浸出工艺条件。结果表明,采用pH值为2的稀硫酸溶液,在浸出温度80℃、浸出时间105min、液固体积质量比10∶1、H2O2添加量1.75mL/g(烟灰)、搅拌速度705r/min的条件下,砷、锌浸出率分别达到78.25%和85.42%。     

Nitric oxide produced by cumulus cells stimulates maturation of mouse oocytes

The effect of sodium nitroprusside (SNP), a donor of nitric oxide, on meiotic maturation of mouse oocytes was studied by injecting N^w-nitro-L-arginine methyl ester (L-NAME) intra-peritoneal (ip), a nitric oxide synthase inhibitor, or culturing oocytes in the medium supplemented with L-NAME or hypoxanthine (HX) to arrest the spontaneous oocyte maturation in vitro. The results showed that the inhibitory effect of L-NAME by injecting 10 mg/kg ip on extrusion of the first polar body only could be reversed by injecting 2.5 mg/kg SNP with L-NAME simultaneously (P < 0.05). Half an hour later ten mice died when given 10 mg/kg SNP ip. The treatment of some concentrations of SNP (10^–7, 10^–6, 10^–5mol/L) significantly stimulated meiotic maturation to metaphase Ⅱ stages in cumulus enclosed oocytes in the presence of HX. However, other concentrations of SNP (10^–8, 10^–4, 10^–3 mol/L) had no effect on HX-arrested oocyte meiotic maturation. The optimal concentration of SNP on CEOs had no effect on DOs. The dose of 10^–3 mol/LL-NAME demonstrated a significant suppression in formation of PB₁, but not in GVBD. This inhibition was reversed by the addition of SNP. These results indicated that the physiological levels of NO produced by cumulus cells could stimulate meiotic maturation of mouse oocytes both in vivo and in vitro.     

最小二乘法在直线矢量化技术中的应用

由于在计算机中图象的存储和显示常常都是以离散的点阵方式进行的，因而给直线的识别带来了很大的困难。本文采用最小二乘法进行参数估计，以提取模式的特征，得到了比较简单的直线矢量化算法，该算法较好的克服了矢量化算法中存在的短线和畸变的缺陷。     

Rutile U-Pb age for the ultrahigh pressure eclogite from the Dabie Mountains,central China: Evidence for rapid cooling

The U-Pb isotope compositions of rutile, omphacite and garnet in the eclogite from the Jinheqiao area in the Southern Dabie ultrahigh-pressure metamorphic zone were analyzed. The consistent high precision U-Pb age (218 ± 1.2) Ma of rutile in eclogite from the Dabie Mountains was obtained by two ways of isochron and common Pb correction based on the composition of omphacite. This proves that the omphacite in eclogite has a U/Pb ratio (m = 2.8) low enough to be used for common Pb correction in the analyses of rutile. Under the rapid cooling condition (40℃/Ma) the closure temperature for U-Pb diffusion in rutile is about 470℃. Thus, this U-Pb age of rutile proves that 218 Ma should be the cooling age of eclogite at 470℃ instead of the peak metamorphic age.     

技术的人文关怀及人文的技术语境——试论哲学视域下的数字城市及其活力挑战

数字城市一方面作为信息技术产品而存在,另一方面也内植了深沉的人文情感与文化意蕴,影射着技术与人文、自然与社会、个体与群体之间的矛盾与冲突,预言着人类活动、社会存在与文明进步的实践基础、人性根基与精神源泉所面临的活力挑战。对其蕴涵的活力挑战与潜在机遇进行透彻剖析,无疑将有利于我们深刻理解数字空间与现实空间的互动与缠绕,有利于正确把握自然、社会、人三者之间的相互影响与相互依赖,催生并建构出新型的活力个体、活力城市与活力社会。     

谈小学作文教学

在小学作文教学中,树立正确的作文观,重视学生的人格教育;端正教师的角色现,影响学生的人格形成;优化作文训练,发展学生的人格教育,都是行之有效的教学法.     

浅谈寒冷地区大体积砼冬季施工技术

文章重点介绍了寒冷地区侯家沟大桥承台大体积砼施工技术方案及实施工艺.