环状低聚糖α-环糊精在薄层色谱中的应用

将环状低聚糖α-环糊精(α-CD)应用于薄层色谱,以国产聚酰胺膜为固定相,研究了同分异构体邻、间、对苯二酚的薄层色谱行为及影响分离的因素;建立了苯二酚异构体的分析方法;探讨了苯二酚化合物与α-CD的键合常数,并提出了可能的包接模型.     

具有大开孔接管结构的椭圆封头边界效应

通过理论计算分析了椭圆封头大开孔结构的一般情况，即两个相互干涉的边界对封头结构性能的影响问题．发现当开孔率达到90％（即r／R=0．9）时，尽管两个干涉的边界相距很近，但开孔边界的应力集中问题仍然可以按接管边界单独存在的情况进行处理．这一发现表明，开孔率较大的情况下，边界效应的相互干涉和影响应当加以考虑的传统观点需要加以修改，从而为提供更简洁的工程设计方法打下了基础．     

含纳米硅氧化硅薄膜的光致发光特性

利用射频磁控溅射复合靶技术,通过调节复合靶的百分比制得富硅的氧化硅薄膜,并在不同的温度下退火,制得含纳米硅的氧化硅薄膜.通过Raman谱的测量,计算出800℃退火的薄膜中纳米硅晶粒的平均尺寸为5.6 nm,用X射线衍射测量同样的样品得出其粒径为6.0 nm.在室温下测量光致发光(PL)谱,探测样品的峰位为360 nm,并结合光致发光激发谱(PLE),研究相应的激发与发光中心.     

Target tracking based on frequency spectrum amplitude

1 .INTRODUCTIONIn target tracking, attribute parameters can beused to i mprove the performance of data associa-tion. The probabilistic data association ( PDA)which employ the attribute enhance the capabilityof data association and i mprove the performancefor target tracking. The method of PDA is per-formedin the environment of high signal to noise(SNR) generally and the SNRis in excess of 10dB.But the SNRinthe actual environment is lowerthan 10 dB commonly . When SNRis below0 dB,…     

中国家族文化形成的宗教审视

家族观念是中国文化中极其重要的一部分,它的形成与政治历史地理等都有很大的关系,本文从宗教的角度,就祖先崇拜的层面剖析家族观念形成的原因,从而进一步明晰宗教在民族文化心理的生成过程中的重要作用.     

Eolian origin of the Miocene loess-soil sequence at Qin’an, China: Evidence of quartz morphology and quartz grain-size

Recent study revealed that the so-called Neogene Gansu System in the western Loess Plateau contains loess-soil sequences of Miocene age. A most complete sequence （QA-I） covers a time interval from ～22 to ～.6.2 Ma BP, consisting of more than 230 visually definable paleosols interbedded with loess layers. A loess-soil sequence of late Miocene-Pliocene age, synchronous with the Hipparian Red Clay in the eastern Loess Plateau, was also recognized, and extends the Miocene sequences into the Pliocene, ～3.5 Ma BP. Recently, Miocene eolian deposits were also reported from the high terraces near Xining.     

Seasonal variation of snow microbial community structure in the East Rongbuk glacier, Mt. Everest

Mt. Everest, the zenith of the world, plays an impor- tant role in the global climate change. During the lastdecade, some studies on glacier and snow have been undertaken in this region. The climate and environment changes in the past hundred years have b…     

Crystal structure determining of 7-ADCA based on X-ray powder diffraction

Traditionally, crystal structure data can be collected and determined from single-crystal X-ray diffraction. However, in the fields of organic and macromolecular crystallography, it is often difficult or impractical to grow single crystals with suitable sizes and purity. Therefore, it will be benefited from the newly growing analytical tool that combining X-ray powder diffraction based on polycrystalline samples and ab initio calcula- tion[1]. 7-ADCA is one of the most important intermediate…     

高职高专学生实验能力评价体系构建初探

科学地建立高职高专实验能力评价体系是高职高专实验教学改革的重点,以实验能力结构和评价标准构建的体系初探表明,该体系操作性好,有利于教学质量的提高,有利于高职高专学生综合能力的提高。     

分子印迹技术研究的新进展

分子印迹技术是制备对特定分子具有特异性识别能力的高分子聚合物的一种技术,本文就近些年来分子印迹技术在合成单体、合成方法以及应用领域等方面取得的新进展进行了综述.