甲基丙烯酸叔丁酯的原子转移自由基聚合

分别以对氯甲基苯乙烯和α-溴代丙酸乙酯为引发剂,联二吡啶和N,N,N′,N″,N″-五甲基二亚乙基三胺为配位剂,在氯化亚铜的催化作用下,使甲基丙烯酸叔丁酯(tBMA)进行本体聚合.用凝胶渗透色谱跟踪聚合物的相对分子质量变化,发现不同引发剂与配位剂对聚合反应速率有明显的影响.根据体系中的ln([cM0]/[cM])变化与聚合反应时间成线形的关系,证明tBMA的聚合过程在实验范围内符合原子转移自由基聚合(ATRP)反应规律.利用ATRP的反应特点,改变引发剂与单体tBMA的配比,可将聚甲基丙烯酸叔丁酯(PtBMA)的相对分子质量控制在所需范围内,并保持PtBMA的相对分子质量分布≤1.2;同时用核磁共振氢谱对产物的结构进行表征,结果表明所得聚合物PtBMA的结构明确.     

信阳绿茶茶多酚含量及浸出率

本文采用酒石酸亚铁比色法对优质信阳毛尖和次等茶叶中茶多酚含量进行测定，并探讨冲泡水温和冲泡时间对茶多酚浸出率的影响。实验结果表明：优质毛尖和次等茶叶的ＴＰ含量分别为２１．９６％－２３．５２％和１７．９８％－１９．２６％。冲泡水温度和冲泡时间对ＴＰ浸出率均有显著影响。     

Development and characterization of interspecific hybrids between <Emphasis Type="Italic">Oryza sativa</Emphasis> and <Subscript>O. latifolia</Subscript> by <Subscript>in situ</Subscript> hybridization

Oryza sativa and O. latifolia belong to the AA and CCDD genomes of Oryza, respectively. In this study, interspecific hybrids of these species were obtained using the embryo rescue technique. Hybrid panicle traits, such as long awns, small grain, exoteric large purple stigma, grain shattering and dispersed panicles, resemble that of the paternal parent, O. latifolia, whereas there is obvious heterosis in such respects as plant height, tillering ability and vegetative vigor. Chromosome pairing and the genomic components of the hybrid were subsequently investigated using genomic in situ hybridization （GISH） and fluorescent in situ hybridization （FISH） analysis. Based on the mitotic metaphase chromosome numbers of the root tips investigated, the hybrid is a triploid with 36 chromosomes. The genomic constitution of the hybrid is ACD. In the meiotic metaphase Ⅰ of the hybrid pollen mother cell, poor chromosome pairing was identified and most of the chromosomes were univalent, which resulted in complete male sterility in the hybrid.     

玻璃钢井盖的研制

介绍了一种玻璃钢井盖从模具到成品的生产方法,采用独特的软模与硬模相结合,玻璃钢纤维与金属骨架互补、使工艺简化、成本降低。     

Immune Algorithm for Selecting Optimum Services in Web Services Composition

0 IntroductionInha rveec eenmte yregaerds a,sa t ghreo Iwnitnegrn neut mdbeverel oofps W aetb a S fearsvtic reast e( .W TSshe)Webis nowevolving into a distributed device of computationfroma collection of information resources[1]. But individualWeb services usually cannot satisfy some customers’require-ments ,so we always needtointegrate existingservices to cre-ate newvalue-added composed services .The process model underlying a composite identifies thefunctionalities required by the servic…     

超快速低功率光子晶体全光开关研究进展

本文介绍了光子晶体全光开关的原理,以及实现低功率光子晶体全光开关的方法,并详细介绍了北京大学在超快速低功率光子晶体全光开关方面的重要研究进展。     

多模型卡尔曼滤波器的研究

在深入研究卡尔曼滤波算法的基础上,提出模型卡尔曼滤波器的工程设计方法。分别针对二阶系统和船舶模型进行了大量的仿真研究,其结果表明,对参数突变的系统,应用该方法进行状态估计或参数辨人有很好的跟踪突变参数的效果,仿真结果展示,该方法具有广阔的工程应用前景。     

块三对角矩阵方程的追赶法及其应用

导出了块三对角矩阵方程追赶法的一套递推关系式，并编制出相应的计算机Ｃｏｄｅ。该Ｃｏｄｅ具有良好的实用价值，可供在实际问题中使用。     

神经网络TSP问题仿真分析

描述了Hopfield神经网络和自组织特征映射神经网络解决TSP问题时的求解过程和仿真算法.通过对两种算法的仿真比较,得出以下结论:对于较大规模的TSP问题,SOFM模型的寻优结果要优于HNN模型寻优结果;HNN对网络模型参数和初始条件具有很强的依赖性且调整参数组合非常困难,而SOFM的参数设置和调整相对要简单得多;SOFM算法对待解决问题的拓扑分布不敏感,而HNN算法的收敛性对待求解问题的自身分布有很强的依赖性;当待求解问题的数目增大时,SOFM算法的运算时间增加缓慢,而HNN算法的运算时间增加较快.因此,在解决TSP问题时,自组织特征映射神经网络比Hopfield神经网络的效率高,随着问题规模的增大,其优势更为明显.     

Shale gas exploitation with supercritical CO2 technology

This paper analyzes the physicochemical properties of supercritical CO2, the characteristic of shale gas and shale gas reservoirs. The technologies of drilling, production, fracturing using the supercritical CO2 in shale gas exploration are proposed, to increase the penetration rate, decrease the damage to formation while fracturing, and enhance the recovery of shale gas. It is believed that the huge economic benefits of shale gas exploration with the supercritical CO2 fluid will be obtained, and it also can initiate a new technology field of CO2 in the petroleum engineering.