用异淀粉酶改进淀粉膜的研究

用异淀粉酶可使淀粉中的支淀粉脱支而形成链淀粉,从而提高淀粉膜的成膜性能及强度。本文用正交试验法研究异淀粉酶对马铃薯淀粉脱支的作用条件,并描绘了异淀粉酶的作用时间与膜的抗张强度、伸长百分率、耐折度、透湿性、链淀粉含量的关系曲线,为制取性能好的食用淀粉膜提供依据。     

PVDF与海藻酸钠黏结剂对石墨负极电化学性能的影响

应用循环伏安和恒电流充、放电等电化学方法,并结合微观测试技术对比了油性黏结剂（PVDF）和水性黏结剂（海藻酸钠）对石墨负极电化学嵌脱锂性能的影响．结果表明,黏结剂的种类对电极的电容、库效率、倍率充、放电性能以及电化学循环性能均有影响．     

DSEM时域数值模型求解关键影响因素分析

人工材料阻尼系数与有限区域尺寸对以阻尼溶剂抽取法(DSEM)为基础的动力结构-地基相互作用分析的效率与精度影响显著.为研究这种影响,以弹性地基上半无限杆的波动理论为基础,在频域中推导了人工高阻尼条件下谐波幅值衰减的解析表达,进而结合对杆端交界面力的时域数值分析,给出了适于工程应用的关键因素参考取值.提出了基于加速度求解的DSEM隐式积分算法,克服了原位移求解模式中存在的结构-地基交界面显隐式积分步长协调性的问题,可方便地与结构侧的动力响应分析相结合.数值算例表明该算法具有良好的稳定性和计算效率,亦验证了关键因素参考取值的有效性.     

结构-地基相互作用的频域计算模型

基于比例边界有限元法（SBFEM）建立了结构-无限地基相互作用分析的频域透射边界,这种透射边界精确满足Sommerfeld辐射条件.该方法的特点是可以根据精度需要从低阶到高阶逐步递推计算无限域刚度矩阵,应用简单且十分方便.针对文献中比较常用的各种无限地基计算模型的适应性进行了一定的研究分析.结合无限地基上重力坝的地震响应,对无限地基迟滞效应的影响进行了对比分析,由对比结果可以看出考虑无限地基影响时的坝体最大拉应力分布比常用的无质量地基模型的计算结果约小15%;考虑迟滞效应时最大应力计算结果比不考虑迟滞效应时的计算结果增加了约25%.     

联结数与分数（k，n’）一临界消去图

设G是一个图,若删除G中任意n’个顶点的剩余子图依然是分数k-消去图,则称G为分数（k,n＇）-临界消去图．笔者证明了若k≥2,n,≥0,bind（G）≥^（n＇＋1）且6（G）≥k＋n＇＋1,则G是分数（k,n＇）-临界消去图．     

有向图和二部有向图的局部边连通性

笔者首先利用顶点的度和给出了有向图是超级局部边连通的一个最好可能的充分条件,然后提出了二部有向图为极大局部边连通和超级局部边连通的度序列条件.这些结果在网络可靠性分析中有一定应用.     

Re-emerging superconductivity at 48 kelvin in iron chalcogenides

Pressure has an essential role in the production and control of superconductivity in iron-based superconductors. Substitution of a large cation by a smaller rare-earth ion to simulate the pressure effect has raised the superconducting transition temperature T(c) to a record high of 55?K in these materials. In the same way as T(c) exhibits a bell-shaped curve of dependence on chemical doping, pressure-tuned T(c) typically drops monotonically after passing the optimal pressure. Here we report that in the superconducting iron chalcogenides, a second superconducting phase suddenly re-emerges above 11.5?GPa, after the T(c) drops from the first maximum of 32?K at 1?GPa. The T(c) of the re-emerging superconducting phase is considerably higher than the first maximum, reaching 48.0-48.7?K for Tl(0.6)Rb(0.4)Fe(1.67)Se(2), K(0.8)Fe(1.7)Se(2) and K(0.8)Fe(1.78)Se(2).     

靶向TTF-1的siRNA腺相关病毒载体组装验证

为了解决靶向TTF-1的siRNA导入肺腺癌细胞的问题,设计了3条靶向NCI-H1975细胞TTF-1基因的siRNA,并将其分别构建到腺相关病毒上.在293细胞中装配病毒,收获病毒原初液后进行超滤浓缩、层析柱纯化,测定病毒滴度.重组病毒感染肺腺癌细胞系NCI-H1975,通过Western-Blot实验检测siRNA效果,利用凋亡实验验证细胞生物学效应.Western-Blot实验测得siRNA有较好的干扰效果,凋亡实验测得肺腺癌细胞NCI-H1975产生了凋亡,从而证明具有感染性的靶向TTF-1的siRNA腺相关病毒载体组装成功.     

Theoretical study on stereodynamics of H + NeH+ (v = 0, j = 0) → H2 + + Ne reaction

Stereodynamics of reaction H + NeH+(v = 0,j = 0) → H2+ + Ne is investigated by quasi-classical trajectory method using a new potential energy surface constructed by Lv et al.The distributions of P(r),P(r) and PDDCSs are calculated at four different collision energies.The rotational polarization of product H2+ presents different characters at different collision energies.The product rotational angular momentum vector j’ is not only aligned,but also oriented along the direction perpendicular to the scattering plane.With the increase of collision energy,the rotation of product molecule has a preference of changing from the "in-plane" mechanism to the "out-of-plane" mechanism.Although the title reaction is mainly dominated by the direct reaction mechanism,the indirect mechanism plays a role when the collision energies are low.     

An engraved artifact from Shuidonggou, an Early Late Paleolithic Site in Northwest China

Cognition and symbolic thinking are viewed as important features of modern human behavior.Engraved objects are seen as a hallmark of cognition and symbolism,and even as evidence for language.Accumulated evidences including engraved bones,ochre,ostrich eggshells and stone artifacts were unearthed from Africa,Europe,Levant even Siberia Paleolithic sites.But the archaeological evidence for this,including beads,ornaments,burials,performed objects and engraved objects,is rarely discovered in the Pleistocene of East Asia.The present paper reports an engraved stone object unearthed in the Early Late Paleolithic levels about 30 ka BP at the Shuidonggou site(SDG) in northwestern China.It was unearthed in the 1980’s excavation from Lower culture unit of SDG1 but was identified in 2011 when the first author of this article observed the collection from the 1980’s excavations stored in the Institute of Archaeology of Ningxia Hui Autonomous Region for further detailed lithic analysis.This lithic artifact is the first engraved non-organic object of the Paleolithic period found in China.In order to clarify the details of the incisions and to document the human intentional modifications,we used a KEYENCE VHX-600 Digital Microscope to measure and observe all the incisions in 3-dimensional perspective.Comparing the natural cracks and analyzing many details of the incisions,we argue that incisions on this stone artifact are the result of intentional behaviors by ancient humans.Also,we exclude the possible other causes including animal-induced damages,post-depositional phenomenon and unintentional by-products.Combining all these features,we suggest that the incisions were made by an intentional behavior and were probably of a non-utilitarian character.Because the nature of most other engraved objects in China is debate,we cannot get a clear scenario of the emergence and progress of modern human behavior in North China.But we infer the possible existence of a counting or recording system,or other symbolic behaviors,which reflect considerably evolved cognitive capacities or modern human behavior in the Early Late Paleolithic of East Asia.