Characterization and Preparation of Bimetallic Nanoparticles

1 Results Bimetallic particles in the nanometer size range are of substantial interest due to their vast applications in catalysis[1].The synthesis of bimetallic nanoparticles with definite size with a well-control over their nanostructure remains a challenging problem.Thus there exists a great demand for both synthesis and atomic level characterization of nanostructure of bimetallic nanoparticles (NPs).With the recent advent of high-intensity tunable sources of X-rays,now available at synchrotron radia...     

Preparation and electrochemical performance of double perovskite La_2CoMnO_6 nanofibers

Through electrospinning,La_2Co Mn O_6 nanofibers were prepared from a polyvinylpyrrolidone/lanthanum nitrate–cobalt acetate–manganese acetate(PVP/LCM)precursor and were used as electrode materials.The morphologies and structures of the samples were characterized by field-emission scanning electron microscopy(FE-SEM),transmission electron microscopy(TEM),X-ray diffraction(XRD),and Brunauer-Emmett-Teller(BET)specific surface area analysis.The results show that the prepared La_2Co Mn O_6 nanofibers are stable,one-dimensional structures formed from interconnected La_2Co Mn O_(6 )nanoparticles with a diamond-like crystal structure.The specific surface area of the fibers is 79.407 m~2·g~(-1).Electrochemical performance tests with a three-electrode system reveal the specific capacitance of the La_2Co Mn O_6 nanofibers as 109.7 F·g~(-1) at a current density of 0.5 A·g~(-1).After 1000 charge-discharge cycles at a current density of 1 A·g~(-1),the specific capacitance maintains 90.9%of its initial value,demonstrating a promising performance of the constraint capacitance and good cyclic stability.     

群组判断矩阵排序中的广义最小偏差方法

本文对群组判断矩阵排序提出一种新的广义最小偏差方法。鉴于不同专家所给判断矩阵质量上的差异, 广义最小偏差排序方法对群组判断矩阵进行不同程度的加权处理, 并进行群组一致性检验。     

大跨平屋盖结构风压分布特性的神经网络模型

影响大跨平屋盖结构风荷载分布特性的因素很复杂，且具有不确定性，仅靠风洞试验难以完整的描述其风荷载分布的整体特性，针对这种情况，本文中提出用改进的BP神经网络和模糊神经网络两种方法来建立反映大跨平屋盖结构风压分布特性的模型，并用试验数据进行了验证．结果表明，这两种模型都能很好的逼近和预测大跨平屋盖结构风压分布的特性，相比之下，改进的BP神经网络稳定性较好，但逼近速度慢，精度也不高；而模糊神经网络由于结合了模糊系统和神经网络的优点，其稳定性好，逼近速度快，且精度高，这表明模糊神经网络方法是预测大跨平屋盖结构风压分布特性的有效途径，在结构风工程中具有广阔的应用前景。     

不同屋面雨水径流中PAHs污染特性对比分析

对南京市典型沥青屋面、瓦屋面径流中PAHs含量进行了9场降雨事件的现场取样监测,对比分析了2种不同屋面径流中PAHs的EMC值及其各组分的浓度,并对其初期效应及影响因素进行了分析和探讨.结果表明,沥青屋面径流PAHs污染较严重,其平均浓度为4 261.7 ng/L,而瓦屋面径流PAHs平均浓度仅为351.2 ng/L.沥青屋面、瓦屋面径流中PAHs均以4环组分为主,沥青屋面径流中3环组分占较大含量,而瓦屋面径流中5环和6环PAHs浓度仅次于4环PAHs.大多数降雨事件中总PAHs及各组分均存在较显著的初期效应;前期晴天数对PAHs在屋面的累积影响最大,瓦屋面径流PAHs含量受降雨强度影响较大,而沥青屋面径流PAHs含量受降雨量影响较大.     

关于深化教育学教学中理论思维的认识

深化高师教育学教学的重要途径在于提高学生的理论思维水平。应从两个方面加强理论思维：一是从理论联系实际的宗旨入手，强调理论思维对于实践的批判反思和能动把握；二是从分析理论“经验化”的误区出发，强调理论思维对于克服“经验化”倾向的重要性。     

用于舞台布景的微机激光图形扫描系统

本文描述了一个为舞台布景而设计的微机激光图形扫描系统。该系统由后援微机、RS—232异步通信接口、单板微机控制器、激光源及其反射偏转执行装置等组成。在系统软件支持下,能用光笔进行图形设计与编辑。在激光源及其编转振镜的支持下,可对少于四路的各种类型的激光束进行控制,以显示二维图形。其偏转角度为士7~0、定位精度为0.5％,还可用于广告宣传及工艺雕刻等方面。     

关于思想政治教育目的的确立依据及当代启示

思想政治教育的目的是思想政治教育中的一个根本性问题,它不仅为思想政治教育活动的开展提供基本依据和目标指向,而且为衡量和检验思想政治教育效果提供基本尺度。结合时代变迁对思想政治教育目的进行科学、合理的定位,对于保证思想政治教育的方向,促进人的自由全面发展具有重要意义。     

一种快速计算Zernike矩的混合算法

提取傅里叶-梅林矩作为Zernike矩的公共项,将Zernike矩表示为该公共项的线性组.通过研究Zerni-ke核多项式与傅里叶函数的对称性,将图像区域分成8个区域,只以一个区域的Zernike基函数的值代替其他7个区域基函数的值.而且Zernike多项式的系数具有迭代性.综合这3项技术,本文提出了一种快速计算Zernike矩的混合算法.根据对256 bit色灰度图像的实验结果表明该方法明显优于现有方法.     

Cloning,sequencing of the HSC70 gene in Ctenopharyngodon idella

A cDNA encoding heat shock cognate protein 70(HSC70)was cloned from liver of grass carp(Ctenopharyngodon idella)(GenBank JF436930).This cDNA was found out to contain2 346 bp in length,including 1 950 bp of complete coding sequence encoding 649 amino acids(aa),plus 89 bp of 5′-UTR and 307 bp of3′-UTR.Analysis of its genomic structure revealed that its corresponding gene contained seven exons and six introns.Homology analysis indicated that it shared 99%of identity with HSC70 of breams and 86%of identity with HSP70 of Drosophila.Fluorescent RT-PCR analysis revealed that at 28℃,this gene was expressed in abdominal fat,muscle,intestines,brain,middle kidney,head kidney,gonads,swim bladder,liver,heart,spleen,gills,and fins with expression level in liver being the highest(p0.05),followed by that in the gonads;at 36℃,its mRNA expression level was increased at first but then decreased thereafter under heat shock stress,indicating that its expression can be regulated by heat shock.In conclusion,cloning and expression analysis identified a cDNA encoding a constitutive HSP70 gene that is expressed in many tissues of Ctenopharyngodon idella and its expression was down-regulated by heat shock.